ALD Technology Transfer – Progress Update LAPPD2 Godparent Review Aileen O’Mahony 5 th April 2013.

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Presentation transcript:

ALD Technology Transfer – Progress Update LAPPD2 Godparent Review Aileen O’Mahony 5 th April 2013

Incom ALD Coating Technology Transfer and Facility Prepare specifications for facility and ALD coating hardware and thin film diagnostic instrumentation needed for electrode and ALD coating systems – ongoing Receive quotations to purchase equipment and establish facility at Incom Inc. – ongoing Documentation of the ANL ALD process technology – to be completed Initiate purchase orders for equipment to ensure availability for Phase II – to be completed STTR Task #3

ALD System Beneq ALD System Updated quote received for Beneq TFS500 ALD system Safety concerns expressed by Beneq with the gas precursors required for Chem1 Conference call with Beneq on 3 rd March to review Meeting at Incom on 11 th April to discuss safety and facilities requirements to have these precursors on-site

ALD System Beneq ALD System Option to order from Beneq in the US? Possible to purchase other components (pump, chilller etc.) from US vendors? Showerhead configuration required for processing of MCPs – cost for system customization ~$5,000 Preference for U. Chicago to fabricate showerhead for Incom Beneq system Final showerhead configuration TBD for batch processing of MCPs

ALD System Estimated cost of Beneq TFS500 system Base price including: €309,500 = $397,000 Reaction chamber (ANL design) €31,500 = $40,000 Precursor lines - 2 x liquid (TMA, H 2 O) precursor lines & 200 ml containers - 2 x hot precursor lines (300 o C) & 580 ml containers - 2 x gas lines Foreline trap, shipping and packing Additional Components Alcatel ADS 602H pump €29,700 = $38,000 Huber H chiller €6,200 = $8,000 Showerhead configuration (TBD) ~$5,000 = $450,000 Additional modifications TBD – gas lines for Chem1 precursors and showerhead

Additional Equipment Evaporator Veeco system from U. Chicago to ANL to be shipped to Incom Being coordinated by Mike Lefebvre (Incom) with Jeff Williams (ANL) To be assessed and refurbished by Yeagle Technology, Inc., CT Ellipsometer Final quote received from Woollam Ordering fixed angle base, calibration wafers and software (~$10,000) Evaluation/refurbishment may be required on-site at Incom Annealing oven Oven purchased and modified for ANL, to be installed Incom plan to purchase same oven from U. Chicago with approximate cost $10,000 Additional equipment: resistance and gain measurement, scribing/dicing equipment, fumehood, glovebox, chemical storage, MCP storage (desiccators), MCP racks etc.

R&D Lab Facilities Planning Facilities layout at Incom R&D lab (Rte. 20 location) Cleanroom planning in initial stages To be determined: › Square footage of cleanroom and location › Class of cleanroom required › Equipment to be located in cleanroom or chase › Facilities requirements – house N 2, air, H 2 O, chemical storage, gas lines, power supply, extraction/ventilation, fumehood, glovebox etc. › Funding and timeline for outfitting of cleanroom Safety review meeting on 11 th April at Incom regarding handling of hazardous precursors required for Beneq system Proposal for $200,000 START Phase II funding from MassVentures earmarked for cleanroom layout planning unfortunately unsuccessful Estimated cost of complete cleanroom for MCP processing ~$1,500,000

Personnel: Engineer Job Spec Job spec for engineer to be hired by Incom for MCP coating and characterization Vacuum deposition equipment – hands on experience with pumps, vacuum/pressure gauges, etc. – most important criteria Deposition experience – process optimization, film characterization; ellipsometry, electrical characterization Experience with LabVIEW and SolidWorks Troubleshooting vacuum systems – leak checking etc. Chemical handling – familiar with changing gas cylinders, precursor bottles Resistance and gain measurements – experience with design, assembly and operation of equipment for resistance and gain measurement advantageous

What is the status of the STTR Phase I? STTR Phase I is in the early stages of the technology transfer process. Equipment vendors have provided quotes Initial plans and safety reviews at Incom for the floor-plan and facilities required for the cleanroom → Dependent upon STTR Phase II funding? Are there concerns about the interaction of the LAPPD MCP development and the STTR work? Not from the perspective of the technology ANL hired additional ALD personnel Incom has plans to hire a graduate engineer Thank you – Incom team, Argonne, U. Chicago Questions