04/06/2010 Production of Dimethyl Sulfoxide from Lignin Team Bravo is: Stan Das, Jeff Umbach, Russ Boyer, Krista Sutton, Mike Czepizak Project Lead: Jake.

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Presentation transcript:

04/06/2010 Production of Dimethyl Sulfoxide from Lignin Team Bravo is: Stan Das, Jeff Umbach, Russ Boyer, Krista Sutton, Mike Czepizak Project Lead: Jake Biberstein

04/06/2010 Team Bravo: Presentation 4 2 Project Outline Design Basis Block Flow Diagram Constraints Review Material and Energy Balances Applicable Standards Annotated Equipment List Distribution and End Use Utilities Conceptual Control Scheme General Arrangement Economic Evaluation Process Flow Diagram Calculations Project Communications File Information Sources and References

04/06/2010 Team Bravo: Presentation 4 3 Presentation Outline PFD Initial Control Scheme General Plant Layout Hand Calculations and Material Balances Economic Evaluation

04/06/2010 Team Bravo: Presentation 4 4 Block Flow Diagram

04/06/2010 Team Bravo: Presentation 4 5 PFD: Lignin Reaction

04/06/2010 Team Bravo: Presentation 4 6 Block Flow Diagram

04/06/2010 Team Bravo: Presentation 4 7 PFD: NO 2 Creation/Regeneration

04/06/2010 Team Bravo: Presentation 4 8 Block Flow Diagram

04/06/2010 Team Bravo: Presentation 4 9 PFD: DMS Oxidation

04/06/2010 Team Bravo: Presentation 4 10 General Plant Layout Plant is to be adjacent to paper mill to obtain a cheaper source of black liquor Plant Dimensions 250 x 185(285) x 40

04/06/2010 Team Bravo: Presentation 4 11 Calculations: Lignin Reactor Mass In (lbs/hr) Mass Waste Stream (lbs/hr) Mass Reactor Product (lbs/hr) Black Liquor NaOH17 0 Sulfur Water Tall Oil12 0 Dimethyl Sulfide Total  Reactor Size  Diameter = 7 ft  Height = 20 ft  Volume = 5700 gallons Heat Duty = 830,000 BTU/hr Total Cost of Unit = $1,340,000

04/06/2010 Team Bravo: Presentation 4 12 Calculations: Distillation Column Mass Feed (lbs/hr) Mass Impurit ies (lbs/hr) Mass Bottom Product (lbs/hr) Dimethyl Sulfide 66.2 TRACE Water Other Impurit ies 15.1 TRACE DMSO Total  Column Size  Number of Trays = 9  Diameter = 1.5 ft  Height = 30 ft  Volume = 400 gallons Reboiler Heat Duty = 420,000 BTU/hr Condenser Heat Duty = -47,000 BTU/hr Total Cost of Unit = $410,000

04/06/2010 Team Bravo: Presentation 4 13 General Economic Evaluation Capital Costs  $22,500,000 Utilities  $642,000/year Raw Materials  $14,900,000/year Labor and Maintenance  $1,900,000/year Other Costs  $3,440,000/year Total Operating Costs  $20,800,000/year Total Product Sales  $30,400,000/year Profit per Year  $9,550,000/year Payback Period (x)  2 > x > 3 Years

04/06/2010 Team Bravo: Presentation 4 14 Summary Block flow and process flow diagrams are nearly finalized. Basic control schemes have been added to the process flow diagrams. Our payback period is between 2 to 3 years. We have drafted the general arrangement of our DMSO plant. Further details and higher-detail drawings are available on our Wiki. 

04/06/2010 Team Bravo: Presentation 4 15 Future Goals Pinch analysis and heat integration. Utility optimization. Waste processing. Pumps and compressor adjustments. More detailed control scheme. P&ID Applicable standards, environmental regulations, OSHA requirements.

04/06/2010 Team Bravo: Presentation 4 16 Questions? For more information, please visit our Wiki! 