Distillation Column By Jesse Reeves. Outline Where we are, where we want to be. How to get there. What we used and what we got. The trouble. The model.

Slides:

Advertisements

Similar presentations

Batch Distillation.

Advertisements

Absorption and Stripping

Jonathan Peters Miguel Bagajewicz.  Conventional Distillation  Pre-flash Fractionation  Previous Work  Mission Statement  Optimization  Results:

Mass Transfer for 4 th Year Chemical Engineering Department Faculty of Engineering Cairo University.

Multistage Distillation

Plate efficiencies 1. Types of plate efficiency

Process Modeling using Aspen Plus

Team 3: Robert Clifford, Patricia Firmin, Gen Liang, Rooma Raza

4/14/ ChE 382 Group 5.  Binary distillation involves only 2 components  It works by using the differences in boiling points for separation › Methanol.

“Chemical Engineering Equilibrium Separations” Lectures 12 & Oct 2012.

Distillation of Binary Mixture

“Chemical Engineering Equilibrium Separations” Lectures Oct 2012.

IDEAL STAGE Feed F, x F Distillate D, x D Bottom Product B, x B SINGLE-STAGE (FLASH) DISTILLATION UNECONOMICAL.

TEAM X Steady State Data Analysis Distillation Column By: Dr. Jim Henry 7 Oct 2003.

Batch Distillation John Ozbek Murat Ozkaya 11/25/08.

1 Acetone, 2-Propanol H 2 Acetone 2-Propanol L2 Acetone, 2-Propanol L201 L101L1 L3 L4 L10 L9 Condenser Reboiler Distillation Column Endothermic Reactor.

TEAM X Steady State Data Analysis Distillation Column

Batch Distillation Gavin Duffy School of Electrical Engineering Systems DIT Kevin St.

Ethanol Production from Wastepaper Ben DaltonMarie Labrie Cassia DavisAlex Saputa John OzbekSteve Wild Murat Ozkaya4/15/09.

ENGINEERING 536 MASS TRANSFER OPERATIONS FALL 1997 TEAM MEMBERS: Dr. Jim Henry, P.E. Sean Cunningham Mark Koss, P.E. Sandy Koss Tara Ostrander, E.I. Nittaya.

Methanol-Water Batch Distillation Prepared by: Jason Hixson Don Scott Michael Hickey September 20, 2005 UTC ENCH 435.

EXAMPLES. UBAID UR REHMAN 2008-CHEM-19 ANAM ASIF 2008-CHEM-107 PRESENTED BY 2 CHEMICAL ENGINEERING DEPARTMENT, UET.

Distillation Column ENGR 435 Team Members James Linder Marc Moss Corita Suber Brian Vandagriff December 1, 1998.

Final Stages NGL Separation

Unit Operations Lecture 19

USE OF HEAT INTEGRATED DISTILLATION TECHNOLOGY IN CRUDE FRACTIONATION Su Zhu, Stephanie N. English, Miguel J. Bagajewicz The University of Oklahoma Department.

Controller Design Using CHEMCAD

ERT 313 BIOSEPARATION ENGINEERING DISTILLATION

ERT 313 BIOSEPARATION ENGINEERING TUTORIAL 2 - DISTILLATION

1 (16) Use of Murphree efficiency 默弗里板效率 /Determining the number of actual plates 实际板 [pp ] When the Murphree efficiency is known, it can readily.

LPPD Jamie Polan, LPPD ◦ Chicago, Illinois ◦ REU, Summer 2006 Separation Systems Design Under Uncertainty Final Presentation for REU program August 3,

University of Texas at AustinMichigan Technological University 1 Module 5: Process Integration of Heat and Mass Chapter 10 David R. Shonnard Department.

Lecture 15: Batch Distillation 1 Batch Distillation Total condenser Overhead vapor Boilup N 2 1 Distillation Reflux drum Rectifying section stages Stripping.

Redesign Analysis of a Distillation Column Presented By: Michael Hoepfner University of Utah 2006.

Internal Column Balances Feed tray F V V L L Feed Equation: y = -{(L - L)/(V - V)}x + Fz f /(V-V) y = -(L f /V f )x + (F/V f )z f y = {q/(q-1)}x.

SEQUENCING OF AZEOTROPIC DISTILLATION COLUMNS

CHEMICAL HEAT PUMP SAND TEAM

Chemstations, Inc – Houston, TX – – Short Cut - Fenske-Underwood-Gilliland - Limited design, Rating Tower - Rigorous.

McCabe Thiele Graphical Equilibrium-Stage

ERT 313 BIOSEPARATION ENGINEERING DISTILLATION Prepared by: Miss Hairul Nazirah Abdul Halim.

Distillation of Ethyl Alcohol Alexander Saputa ENCH 435 September 23, 2008.

“Chemical Engineering Equilibrium Separations”

Other Sources of Enthalpy Data Specific heats tabulated (see Appendix of thermodynamic textbook) and graphical data Riedel Equation  H n /RT n = 1.092(InP.

The Production of Ethanol from Syngas

CBE 417 “Chemical Engineering Equilibrium Separations” 1 Lecture: 7 17 Sep 2012.

Dr Saad Al-ShahraniChE 201: Introduction to Chemical Engineering  Separation operations are subject to the conservation of mass  Separation of components.

Last Week of Project Terry A. Ring. Project Schedule.

Tower Design in ProMax ChEN 4253 Design II Chapter 19 S,S&L Terry A. Ring University of Utah.

McCabe Thiele Part Two Today we will discuss:

Chemical Engineering Department Government Engineering College Bhuj Prepared By: ( to ) B.E. Sem-III(Chemical) Guided By:

Unit 1 Mix and Flow of Matter Topic 3 Separating Earth’s Mixtures Remember to name and date your notes!

John Edwards, P&I Design Ltd

CHEMCAD User Meeting Berlin, September 2015

Unit Operations Laboratory Distillation Analysis Seminar Super Team 2005 Monday, December 5, :30 PM.

John Edwards, P&I Design Ltd

Natural Gas Processing I Chapter 9 Fractionation

Experiment 300: Distillation

A Review of Separation Topics

Process Equipment Design Distillation Columns

Terry A. Ring Chemical Engineering University of Utah

Team 3: Robert Clifford, Patricia Firmin, Gen Liang, Rooma Raza

ChEN 5253 Design II Chapter 13 Terry A. Ring University of Utah

SEQUENCING OF AZEOTROPIC DISTILLATION COLUMNS

Distillation Column – External Balance

1 INTERNATIONAL MARITIME COLLEGE OMAN PROCESS TECHNOLOGY & SYSTEMS (TPTS & PT-TPTS) PE (TPTS & PT-TPTS) (Chapter-3) Chapter - 3 Distillation Systems Textbook.

Terry A. Ring Chemical Engineering University of Utah

Limiting Conditions – Reflux Ratios

Integration of Heat and Power

Separation Columns (Distillation, Absorption and Extraction)

Presentation transcript:

Distillation Column By Jesse Reeves

Outline Where we are, where we want to be. How to get there. What we used and what we got. The trouble. The model.

What we have 12 tray bubble-cap distillation column Isoproply alcohol water separation

What we want Same distillation column Ethanol water separation

How to get there Operate column at total reflux Determine stage efficiency Model the column in Aspen Compare Aspen model to real IPA separation results Apply the Aspen model to an Ethanol separation

Theory to get there Equilibrium curveStripping operating line Rectifying operating lineMurphree-vapor efficiency

Theory in a graph

The Column

The Data Calibration StageStateMethodMass%IPAErrory* Mass% AveErrorEmv eqError 2LiquidPycnometer LiquidPycnometer LiquidPycnometer LiquidPycnometer LiquidPycnometer LiquidPycnometer LiquidPycnometer LiquidPycnometer LiquidRI LiquidRI LiquidRI

The Trouble

The IPA separation

The ETOH separation

The model The IPA Aspen model -4.7% at the top +8.4% at the bottom The three important stages 7, 9, and 10 Murphree- vapor efficiencies were %, %, % Overall column efficiency 8.3% Stage efficiency did not matter

The Aspen model for ETOH Max flow rate: 2.13 GPM Steam flow rate: 1.67 kg/min Condenser heat duty: kJ/min Feed composition: 2.5 wt% ETOH Distillate composition: 40 wt% ETOH ETOH recovery: 99.4%

Recomendations Replace the automatic control valve for the steam flow to the reboiler. Replace the leaky manual steam valve. Refine the ETOH model with steady state data.

Special thanks to team-J Jaron Stanley: Team Leader James Gardner: Operator Jesse Reeves: Team player

References Seader, J. D., Henley, Ernest J., Separation Process Principles, John Wiley & Sons, Inc. pp. 44, 301, (1998). Distillation Column Manual, unpublished printed notes, Univ. of Utah, Salt Lake City, Utah 1997.

Questions ?