M. M. Khalil, S. M. Mostafa, and A. A. Masoud Scholars Report

Slides:

Advertisements

Similar presentations

Chapter 1 Introduction Analytical Chemistry deals with methods for determining the chemical composition of samples. Qualitative Analysis (identification)

Advertisements

OMICS International Contact us at: OMICS Group International through its Open Access Initiative is committed to make genuine.

Copper Ion Analysis Cory Sennett November 15, 2006 CH EN 4903.

1 MSU, Laboratory of Macrocyclic Receptors Carboxylated Adamantylcalixarenes Moscow State University Chemistry Department V. Kovalev.

Table 5. Summary of electroanalytical methods found in literature survey Alankar Shrivastava et al. Various Analytical Methodologies for Determination.

POSTER TEMPLATE BY: om New spectrophotometric method for determination of cephalosporins in pharmaceutical formulations Shazalia.

ELECTROCHEMICAL DETERMINATION OF URANIUM IN SALINE SOLUTIONS Matthew Kirby, 1 Pascal Salaun, 2 Jonathan Watson, 1 and Dominik Weiss. 1 1 Department of.

1 Analytical Chemistry II Somsak Sirichai Lectures: Tuesday p.m. Friday a.m. C

From: Cost of Antibiotic Resistance and the Geometry of Adaptation

Novel Modified Carbon Paste Sensors for Determination of Benzydamine Hydrochloride in Pharmaceutical Formulations and Biological Fluids Research Article

Fig. 8 The two cases for the terminal edge e<sub>0</sub>

Spectrophotometric determination of Zn(II)) by quantitative displacement with copper(II) from diethyldithiocarbamate (DDTC) complex Md. Amzad Hossain,

Figure 3: MetaLIMS sample input.

The Reasons Behind Prevalence of Captagon Addiction in Jeddah and Community Awareness: A Questionnaire-Based Study Survey Article Author: Esraa Adel.

Table 1. Summary of spectrophotometry methods

Fabrication of glass/ITO/PANI-LS Electrodes

From: Shadows of Teichmüller Discs in the Curve Graph

From: Introducing the PRIDE Archive RESTful web services

Notes: Household survey-based Gini and p90/p10 measures use the same definitions as employed by the UK’s official income distribution statistics (source:

Joy Qiu ♦ Dr. Greg Swain ♦ HSHSP 2014

Toxic Exposure to Methyl bromide, a Case Study and a Review

Volume 84, Issue 4, Pages (April 2003)

e Stimuli images obtained from:

Chapter 23 Potentiometry.

Toxic Exposure to Methyl bromide, a Case Study and a Review

Serum Cholesterol levels mg/dl Frequency P

Figure 1. Circular taxonomy tree based on the species that were sequenced in our study. Unless provided in the caption above, the following copyright applies.

ANALYTICAL METHOD VALIDATION

Figure 2. Effect of gradually decreasing photoperiod on PHA response in Siberian hamsters. Asterisk (*) indicates statistical significance at P﹤0.05, determined.

Figure 1. Schematic illustration of CSN and NDM construction and our statistic model. (A) CSN and NDM construction. (i) ... Figure 1. Schematic illustration.

Figure 1. Ratios of observed to expected numbers of exon boundaries aligning to boundaries of domain and disorder ... Figure 1. Ratios of observed to expected.

Figure 4. The mean of spermatocyte of various treatment groups

Fig. 1 Kaplan-Meier plot of cumulative incidence of cancer onset following dermatomyositis diagnosis stratified ... Anti-TIF1-Ab: anti-transcriptional.

Figure 1. Chemical structures of DNA and tc-DNA

Toxic Exposure to Methyl bromide, a Case Study and a Review

Fig. 1 Mean change from baseline in ANC ± s. e

Introduction to Analytical Chemistry

Figure 1. A, Crude incidence rates per 100 person-years of follow-up and 95% confidence intervals for each solid organ ... Figure 1. A, Crude incidence.

M. M. Khalil, S. M. Mostafa, and A. A. Masoud Scholars Report

Fig. 1. iS-CellR pipeline overview

Figure 4. RLS spectra of (A) TMPipEOPP and (B) OMHEPzEOPP in the presence of different concentrations of KRAS. The RLS ... Figure 4. RLS spectra of (A)

Figure 1. Uncertainty reduction, value creation, and appropriation in two case studies. Unless provided in the caption above, the following copyright applies.

M. M. Khalil, S. M. Mostafa, and A. A. Masoud Scholars Report

M. M. Khalil, S. M. Mostafa, and A. A. Masoud Scholars Report

M. M. Khalil, S. M. Mostafa, and A. A. Masoud Scholars Report

M. M. Khalil, S. M. Mostafa, and A. A. Masoud Scholars Report

Polymeric based (SC-µ-ISEs) Established Equilibrium

Figure 3. A basic scheme of a part of the cross-section of the experimental setup implemented for the measurements of asymmetric reduction of weight of.

© The Author(s) Published by Science and Education Publishing.

Fig. 5 Correlation of RNA expression and protein abundance.

In vivo release of doxycycline hyclate from the GRS in a swine model

Fig. 2 Fluidic and electrical characteristics of the wireless optofluidic system. Fluidic and electrical characteristics of the wireless optofluidic system.

© The Author(s) Published by Science and Education Publishing.

Fig. 1 Mean and median RCR (Relative Citation Ratio) of Roadmap Epigenomics Program research articles for each year. Mean and median RCR (Relative Citation.

Fig. 5 Analytical performance of the wearable cortisol sensor.

Figure 1. Prevalence of parasitic infection and anemia among the children. Unless provided in the caption above, the following copyright applies to the.

Fig. 1 Phase diagram and FS topologies.

Fig. 3 Characteristics of UV and temperature sensors.

Financial Development

Intensified vegetation water use under acid deposition

Figure 1 Mechanisms of mitral regurgitation.

by Jacqueline Austermann, Jerry X

Fig. 1. Generic metabolic pathway and its corresponding adjacency matrices. The graph of a static network (A) is ... Fig. 1. Generic metabolic pathway.

Table 4. Summary of electroanalytical methods

Fig. 3 Electrochemical performances of symmetric cells using control Li and composite Li electrodes. Electrochemical performances of symmetric cells using.

Fig. 4 Mapping of abundance of the most dominant bacterial and archaeal phyla across France. Mapping of abundance of the most dominant bacterial and archaeal.

Research, 2016, Vol. 4, No. 6, doi: /jfnr-4-6-2

Fig. 1. A graphical representation of the GGDNA workflow used to identify each single expressed TE transcript from ... Fig. 1. A graphical representation.

Fig. 3 Underwater adhesion performance of adhesive coatings made of mammalian LC domain proteins. Underwater adhesion performance of adhesive coatings.

Education, 2016, Vol. 4, No. 1, doi: /wjce-4-1-4

Presentation transcript:

A Novel Coated Graphite Sensor for Potentiometric Determination of Hydroxychloroquine Sulfate M. M. Khalil, S. M. Mostafa, and A. A. Masoud Scholars Report Volume 1, Issue 2 ( July-Dec 2016) ScholReps-V1-I2-000004 Copyright © 2016 Policy

Fig. 1: The chemical structure of hydroxychloroquine sulfate. Khalil MM, Mostafa SM, and Masoud AA (2016) 'A novel coated graphite sensor for potentiometric determination of hydroxychloroquine sulfate', ScholReps, 1(2). http://www.scholarsreport.com/articles/vol_1/issue_2/ScholReps-V1-I2-000004.html Copyright © 2016 Policy

Fig. 2: Calibration curve of HCQS coated graphite sensor Khalil MM, Mostafa SM, and Masoud AA (2016) 'A novel coated graphite sensor for potentiometric determination of hydroxychloroquine sulfate', ScholReps, 1(2). http://www.scholarsreport.com/articles/vol_1/issue_2/ScholReps-V1-I2-000004.html Copyright © 2016 Policy

IPA: Ion-pair agent; LOD: Limit of detection; LR: Linear range. Table 1. Optimization of membrane composition (w/w %) for hydroxychloroquine sulfate sensor Sensor Composition % w/w Slope LR LOD IPA PVC DBP mV/ decade±SD mol L-1 CGS PTA 1 1.0 49.5 27,0 8.79x10-4-1.0x10-2 1.2x10-6 0.9177 2* 3.0 48.5 28.5 9.3x10-5-1.0x10-2 4.7x10-5 0.9997 3 5.0 47.5 22.0 7.39x10-5-1.0x10-2 1.9x10-5 0.9999 IPA: Ion-pair agent; LOD: Limit of detection; LR: Linear range. Khalil MM, Mostafa SM, and Masoud AA (2016) 'A novel coated graphite sensor for potentiometric determination of hydroxychloroquine sulfate', ScholReps, 1(2). http://www.scholarsreport.com/articles/vol_1/issue_2/ScholReps-V1-I2-000004.html Copyright © 2016 Policy

Fig. 3: The dynamic response time of CGS for step changes in concentrations of HCQS from low to high and vice versa Khalil MM, Mostafa SM, and Masoud AA (2016) 'A novel coated graphite sensor for potentiometric determination of hydroxychloroquine sulfate', ScholReps, 1(2). http://www.scholarsreport.com/articles/vol_1/issue_2/ScholReps-V1-I2-000004.html Copyright © 2016 Policy

Fig. 4: Representative concentration distribution diagram for HCQ species Khalil MM, Mostafa SM, and Masoud AA (2016) 'A novel coated graphite sensor for potentiometric determination of hydroxychloroquine sulfate', ScholReps, 1(2). http://www.scholarsreport.com/articles/vol_1/issue_2/ScholReps-V1-I2-000004.html Copyright © 2016 Policy

Fig.5: Effect of pH of the test solutions on the potential response of CGS a) 1.0 × 10−3 and b) 1.0 × 10−4 mol L−1 of HCQS solution Khalil MM, Mostafa SM, and Masoud AA (2016) 'A novel coated graphite sensor for potentiometric determination of hydroxychloroquine sulfate', ScholReps, 1(2). http://www.scholarsreport.com/articles/vol_1/issue_2/ScholReps-V1-I2-000004.html Copyright © 2016 Policy

Fig. 6: Calibration graphs of some inorganic cations, sugars and amino acids using CGS Khalil MM, Mostafa SM, and Masoud AA (2016) 'A novel coated graphite sensor for potentiometric determination of hydroxychloroquine sulfate', ScholReps, 1(2). http://www.scholarsreport.com/articles/vol_1/issue_2/ScholReps-V1-I2-000004.html Copyright © 2016 Policy

RSD: Relative standard deviation (four determinations) Table 2. Determination of hydroxychloroquine sulfate in pure solution applying the standard addition method Sample Standard addition method Taken mg Found mg Mean Recovery % RSD % CGS Pure solution 0.22 0.21 99.00 0.35 2.17 2.12 97.72 0.51 21.69 21.26 98.00 0.71 RSD: Relative standard deviation (four determinations) Khalil MM, Mostafa SM, and Masoud AA (2016) 'A novel coated graphite sensor for potentiometric determination of hydroxychloroquine sulfate', ScholReps, 1(2). http://www.scholarsreport.com/articles/vol_1/issue_2/ScholReps-V1-I2-000004.html Copyright © 2016 Policy

r2: Correlation coefficient P.W: Present work Table 3. Comparison of the proposed HCQS ion-selective electrode method with published methods Method LR mol L-1 LOD r2 RSD % Ref Spectrophotometry 4.0×10-6–2.0×10-5 2.3×10-5 0.9999 0.36 [23] Pulse differential voltammetry 2.0×10-5–5.0×10-4 2.6×10-5 0.46 Potentiometric sensor CGS 9.3x10-5-1.0x10-2 4.7x10-5 0.9997 0.49 [P.W] r2: Correlation coefficient P.W: Present work Khalil MM, Mostafa SM, and Masoud AA (2016) 'A novel coated graphite sensor for potentiometric determination of hydroxychloroquine sulfate', ScholReps, 1(2). http://www.scholarsreport.com/articles/vol_1/issue_2/ScholReps-V1-I2-000004.html Copyright © 2016 Policy

M. M. Khalil1*, S. M. Mostafa1, A. A. Masoud1 Thank You  A Novel Coated Graphite Sensor for Potentiometric Determination of Hydroxychloroquine Sulfate M. M. Khalil1*, S. M. Mostafa1, A. A. Masoud1 About the Authors 1Chemistry Department, Faculty of Science, Beni-Suef University, Beni-Suef, Egypt *Corresponding Author: M. M. Khalil magdy_mmagdy@yahoo.com mohamed.mahmoud@science.bsu.edu.eg Editor: Dr. Alessandra A. Correa Center for Engineering, Modeling and Applied Social Sciences (CECS), Federal University of ABC (UFABC), 09210-170, Santo André, SP, Brazil. Citation and Copyrights Citation: Khalil MM, Mostafa SM, and Masoud AA (2016) 'A novel coated graphite sensor for potentiometric determination of hydroxychloroquine sulfate', ScholReps, 1(2). Copyright: © 2016 Khalil MM et. al. This is an open access article distributed under the terms of the Creative Commons Attribution 4.0, which permits unrestricted use, distribution, and reproduction in any medium, provided the original author and source are credited Publication Details Received: Sept 25, 2016 Accepted: Nov 05, 2016 Published: Nov 19, 2016 Funding: None. Subject Section: Analytical Chemistry Conflict of interest: The authors have read the journal’s policy and have the following conflicts: Construction and analytical application of novel potentiometric sensors for determination of selected pharmaceutical drugs. Funding: Nonehttp://www.scholarsreport.com/articles/vol_1/issue_2/ScholReps-V1-I2-000004.html Copyright © 2016 Policy