Two fatal intoxication cases with imidacloprid: LC/MS analysis

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Two fatal intoxication cases with imidacloprid: LC/MS analysis Paula Proença, Helena Teixeira, Fernando Castanheira, João Pinheiro, Paula V. Monsanto, Estela P. Marques, Duarte Nuno Vieira Forensic Science International Volume 153, Issue 1, Pages 75-80 (October 2005) DOI: 10.1016/j.forsciint.2005.04.015 Copyright © 2005 Elsevier Ireland Ltd Terms and Conditions

Fig. 1 Metabolic pathways for imidacloprid [6]. Forensic Science International 2005 153, 75-80DOI: (10.1016/j.forsciint.2005.04.015) Copyright © 2005 Elsevier Ireland Ltd Terms and Conditions

Fig. 2 UV spectra of imidacloprid (A) (Rt 8.777), 5-hydroxyimidacloprid (B) (Rt 5.903), 6-chloronicotinic acid (C) (Rt 6.896) and ethirimol (IS) and (D) (Rt 2.603). Forensic Science International 2005 153, 75-80DOI: (10.1016/j.forsciint.2005.04.015) Copyright © 2005 Elsevier Ireland Ltd Terms and Conditions

Fig. 3 SIR mass chromatograms and mass spectrum in scan mode (m/z 256) of imidacloprid detected in blood sample (case 1). Forensic Science International 2005 153, 75-80DOI: (10.1016/j.forsciint.2005.04.015) Copyright © 2005 Elsevier Ireland Ltd Terms and Conditions