Chemical characterization of synthetic cannabinoids by electrospray ionization FT-ICR mass spectrometry  Jade B. Kill, Izabela F. Oliveira, Lilian V.

Slides:



Advertisements
Similar presentations
The most efficient STR loci in forensic genetics in population of central Poland R. Jacewicz, M. Jedrzejczyk, J. Berent Forensic Science International:
Advertisements

Analysis of deteriorated rubber-based pressure sensitive adhesive by pyrolysis-gas chromatography/mass spectrometry and attenuated total reflectance Fourier.
Illa Tea, Ingrid Antheaume, Ben-Li Zhang 
The forensic analysis of office paper using carbon isotope ratio mass spectrometry. Part 3: Characterizing the source materials and the effect of production.
The importance of Guthrie cards and other medical samples for the direct matching of disaster victims using DNA profiling  D. Hartman, L. Benton, L. Morenos,
DNA profiling of trace DNA recovered from bedding
Right heart ischemia in cases of sepsis
Cyanide quantification in post-mortem biological matrices by headspace GC–MS  Brigitte Desharnais, Geneviève Huppé, Martine Lamarche, Pascal Mireault,
Buprenorphine and major metabolites in blood specimens collected for drug analysis in law enforcement purposes  Stephanie Oechsler, Gisela Skopp  Forensic.
Analysis of Indian blue ballpoint pen inks tagged with rare-earth thenoyltrifluoroacetonates by inductively coupled plasma–mass spectrometry and instrumental.
The ideal subject distance for passport pictures
Volatile organic compounds in polyethylene bags⿿A forensic perspective
Two fatal intoxication cases with imidacloprid: LC/MS analysis
The effect of sodium fluoride on the stability of cyanide in postmortem blood samples from fire victims  J.L. McAllister, R.J. Roby, Barry Levine, David.
Piotr Adamowicz, Dariusz Zuba, Karolina Sekuła 
A snapshot on NPS in Italy: Distribution of drugs in seized materials analysed in an Italian forensic laboratory in the period 2013–2015  Sara Odoardi,
A snapshot on NPS in Italy: Distribution of drugs in seized materials analysed in an Italian forensic laboratory in the period 2013–2015  Sara Odoardi,
Determination of ketamine and norketamine in hair by micropulverized extraction and liquid chromatography–high resolution mass spectrometry  Donata Favretto,
Simultaneous determination of mushroom toxins α-amanitin, β-amanitin and muscarine in human urine by solid-phase extraction and ultra-high-performance.
Detection of 3-methylmethcathinone and its metabolites 3-methylephedrine and 3- methylnorephedrine in pubic hair samples by liquid chromatography–high.
Purple discoloration of the colon found during autopsy: Identification of betanin, its aglycone and metabolites by liquid chromatography–high-resolution.
Direct analysis in real time high resolution mass spectrometry as a tool for rapid characterization of mind-altering plant materials and revelation of.
Simultaneous analysis of six amphetamines and analogues in hair, blood and urine by LC-ESI-MS/MS  Marjorie Chèze, Marc Deveaux, Claire Martin, Michel.
Effective injection in pulsed splitless mode for impurity profiling of methamphetamine crystal by GC or GC/MS  Tetsuro Sasaki, Yukiko Makino  Forensic.
The homogeneity testing of EtG in hair reference materials: A high-throughput procedure using GC–NCI–MS  Bettina Mönch, Roland Becker, Christian Jung,
Yun Sik Nam, Il Keun Kwon, Yeonhee Lee, Kang-Bong Lee 
Forensic Science International
Development of a GC–MS method for methamphetamine detection in Calliphora vomitoria L. (Diptera: Calliphoridae)  Paola A. Magni, Tommaso Pacini, Marco.
Profiling counterfeit Cialis, Viagra and analogs by UPLC–MS
Rapid screening for detection and differentiation of detergent powder adulteration in infant milk formula by LC–MS  Manjun Tay, Guihua Fang, Poh Ling.
UPLC-MS/MS determination in blood of a mixed-drug fatal intoxication: A case report  Paula Proença, João Miguel Franco, Carla Mustra, Carla Monteiro, Joana.
Gowri Vijay Reesu, Nathan Lee Brown  Forensic Science International 
Inhwan Han  Forensic Science International 
Comparing ballistic wounds with experiments on body simulator
Identification, extraction and quantification of the synthetic cannabinoid JWH-018 from commercially available herbal marijuana alternatives  Sage J.B.
Cuiling Zhang, Joost van de Weijer, Jingxu Cui 
Suspected clozapine poisoning in the UK/Eire, 1992–2003
Suspected clozapine poisoning in the UK/Eire, 1992–2003
Elemental analysis of glass by laser ablation inductively coupled plasma optical emission spectrometry (LA-ICP-OES)  Emily R. Schenk, José R. Almirall 
Reliability of the Suchey-Brooks method for a French contemporary population  Frédéric Savall, Camille Rérolle, Fabrice Hérin, Fabrice Dédouit, Daniel.
Instability of calcium channel antagonists during sample preparation for LC–MS–MS analysis of serum samples  Ana B. Baranda, Rosa M. Alonso, Rosa M. Jiménez,
The discrimination of automotive clear coats by pyrolysis-gas chromatography/mass spectrometry and comparison of samples by a chromatogram library software 
Forensic Science International
Comparison of latex body paint with wetted gauze wipes for sampling the chemical warfare agents VX and sulfur mustard from common indoor surfaces  Laura.
Some pyridine derivatives as “route-specific markers” in 4-methoxyamphetamine (PMA) prepared by the Leuckart method  Dariusz Błachut, Krystyna Wojtasiewicz,
The characterisation of two halogenated cathinone analogues: 3,5- Difluoromethcathinone and 3,5-dichloromethcathinone  Sean Davis, Karen Rands-Trevor,
Forensic analysis of biodiesel
Evidence of mephedrone chronic abuse through hair analysis using GC/MS
Evidence of mephedrone chronic abuse through hair analysis using GC/MS
Forensic classification of counterfeit banknote paper by X-ray fluorescence and multivariate statistical methods  Hongling Guo, Baohua Yin, Jie Zhang,
Simultaneous determination of creatinine and uric acid in urine by liquid chromatography–tandem mass spectrometry with polarity switching electrospray.
Simultaneous determination of creatinine and uric acid in urine by liquid chromatography–tandem mass spectrometry with polarity switching electrospray.
Natalija Novokmet, Zlatko Pavčec  Forensic Science International 
A. Barbaro, P. Cormaci, G. Falcone 
Multiplex PCR electrospray-ionization mass spectrometry (ESI-MS): Application to forensic mitochondrial DNA examinations  Leslie D. McCurdy, Lora J. Gioeni,
Probabilistic modelling for DNA mixture analysis
Naoto Iizuka, Ryo Kobayashi, Yukio Itoh 
A comparative study between muscle, cartilage and swab from inside the urinary bladder samples for DNA typing of severely burnt bodies in disaster victim.
Establishment of Italian national DNA database and the central laboratory: Some aspects  R. Biondo, F. De Stefano  Forensic Science International: Genetics.
Human autosomal SNP profiling using fully automated electrospray ionization time of flight mass spectrometry  Thomas A. Hall, Christine V. Marzan, Sandy.
Population data for SE33 locus in United Arab Emirates Arab population
P. Dario, A. R. Oliveira, T. Ribeiro, M. J. Porto, J. Costa Santos, D
Human autosomal SNP profiling using fully automated electrospray ionization time of flight mass spectrometry  Thomas A. Hall, Christine V. Marzan, Sandy.
Analysis of forensic samples in Banco Nacional de Datos Genéticos
M. Hara, T. Masuda, A. Takada, T. Miyazaki, H. Suzuki, A. Kido, K
Application of less primer method to commercial kits
Human being eaten by his own dogs: Genetic confirmation through analysis of bones recovered in a dog's stomach content  A. Serra, J. Pinheiro, L. Batista,
Effects of the most common methods for the enhancement of latent fingerprints on DNA extraction from forensic samples  S. Gino, M. Omedei  Forensic Science.
M. Lurdes Pontes, M. Fátima Pinheiro 
A.M. Ölçen, G. Filoğlu, H. Altunçul, S. Erdem, Ö. Bülbül 
Presentation transcript:

Chemical characterization of synthetic cannabinoids by electrospray ionization FT-ICR mass spectrometry  Jade B. Kill, Izabela F. Oliveira, Lilian V. Tose, Helber B. Costa, Ricardo M. Kuster, Leandro F. Machado, Radigya M. Correia, Rayza R.T. Rodrigues, Géssica A. Vasconcellos, Boniek G. Vaz, Wanderson Romão  Forensic Science International  Volume 266, Pages 474-487 (September 2016) DOI: 10.1016/j.forsciint.2016.07.007 Copyright © 2016 Elsevier Ireland Ltd Terms and Conditions

Fig. 1 Examples of SCs samples that are popularly known as bong basic or extremely. Forensic Science International 2016 266, 474-487DOI: (10.1016/j.forsciint.2016.07.007) Copyright © 2016 Elsevier Ireland Ltd Terms and Conditions

Fig. 2 ESI(+)-FT-ICR mass spectra of the nine herbal extracts samples containing the 11 SCs. Forensic Science International 2016 266, 474-487DOI: (10.1016/j.forsciint.2016.07.007) Copyright © 2016 Elsevier Ireland Ltd Terms and Conditions

Fig. 3 ESI(+)MS/MS spectra for the ions at m/z 372 (JWH-081), 328 (JWH-073), 360 (AM-2201), 356 (JWH-122), 370 (JWH-210), 312 (UR-144) and 330 (XLR-11). Forensic Science International 2016 266, 474-487DOI: (10.1016/j.forsciint.2016.07.007) Copyright © 2016 Elsevier Ireland Ltd Terms and Conditions

Fig. 4 Possible fragmentation pathways of the synthetic cannabinoids by ESI-MS/MS. Forensic Science International 2016 266, 474-487DOI: (10.1016/j.forsciint.2016.07.007) Copyright © 2016 Elsevier Ireland Ltd Terms and Conditions

Fig. 5 ESI(⿿)-FT-ICR mass spectra of the nine herbal extract samples, with which 44 new substances were identified. Forensic Science International 2016 266, 474-487DOI: (10.1016/j.forsciint.2016.07.007) Copyright © 2016 Elsevier Ireland Ltd Terms and Conditions

Fig. 6 Diagrams of classes from ESI(⿿)-FT-ICR MS data. Forensic Science International 2016 266, 474-487DOI: (10.1016/j.forsciint.2016.07.007) Copyright © 2016 Elsevier Ireland Ltd Terms and Conditions

Forensic Science International 2016 266, 474-487DOI: (10. 1016/j Forensic Science International 2016 266, 474-487DOI: (10.1016/j.forsciint.2016.07.007) Copyright © 2016 Elsevier Ireland Ltd Terms and Conditions