Headspace-GC/MS detection of TATP traces in post-explosion debris

Slides:

Advertisements

Similar presentations

The most efficient STR loci in forensic genetics in population of central Poland R. Jacewicz, M. Jedrzejczyk, J. Berent Forensic Science International:

Advertisements

The importance of Guthrie cards and other medical samples for the direct matching of disaster victims using DNA profiling D. Hartman, L. Benton, L. Morenos,

DNA profiling of trace DNA recovered from bedding

Right heart ischemia in cases of sepsis

Headspace-GC/MS detection of TATP traces in post-explosion debris

Analysis of the headspace composition of smokeless powders using GC–MS, GC-μECD and ion mobility spectrometry Monica Joshi, Kia Rigsby, Jose R. Almirall

Cyanide quantification in post-mortem biological matrices by headspace GC–MS Brigitte Desharnais, Geneviève Huppé, Martine Lamarche, Pascal Mireault,

Buprenorphine and major metabolites in blood specimens collected for drug analysis in law enforcement purposes Stephanie Oechsler, Gisela Skopp Forensic.

The ideal subject distance for passport pictures

Volatile organic compounds in polyethylene bags⿿A forensic perspective

Two fatal intoxication cases with imidacloprid: LC/MS analysis

Could NF-κB and caspase-3 be markers for estimation of post-interval of human traumatic brain injury? Luyang Tao, Xiping Chen, Zhenghong Qin, Shizhong.

The effect of sodium fluoride on the stability of cyanide in postmortem blood samples from fire victims J.L. McAllister, R.J. Roby, Barry Levine, David.

Detecting and collecting traces of semen and blood from outdoor crime scenes using crime scene dogs and presumptive tests A.G. Skalleberg, M.M. Bouzga

Piotr Adamowicz, Dariusz Zuba, Karolina Sekuła

A snapshot on NPS in Italy: Distribution of drugs in seized materials analysed in an Italian forensic laboratory in the period 2013–2015 Sara Odoardi,

A snapshot on NPS in Italy: Distribution of drugs in seized materials analysed in an Italian forensic laboratory in the period 2013–2015 Sara Odoardi,

Determination of ketamine and norketamine in hair by micropulverized extraction and liquid chromatography–high resolution mass spectrometry Donata Favretto,

Simultaneous determination of mushroom toxins α-amanitin, β-amanitin and muscarine in human urine by solid-phase extraction and ultra-high-performance.

Simultaneous analysis of six amphetamines and analogues in hair, blood and urine by LC-ESI-MS/MS Marjorie Chèze, Marc Deveaux, Claire Martin, Michel.

Optimization of an analytical method for detecting paraphenylenediamine (PPD) by GC/MS-iontrap in biological liquids A. Stambouli, M.A. Bellimam, N.

Effective injection in pulsed splitless mode for impurity profiling of methamphetamine crystal by GC or GC/MS Tetsuro Sasaki, Yukiko Makino Forensic.

The homogeneity testing of EtG in hair reference materials: A high-throughput procedure using GC–NCI–MS Bettina Mönch, Roland Becker, Christian Jung,

Forensic Science International

Development of a GC–MS method for methamphetamine detection in Calliphora vomitoria L. (Diptera: Calliphoridae) Paola A. Magni, Tommaso Pacini, Marco.

Gowri Vijay Reesu, Nathan Lee Brown Forensic Science International

Inhwan Han Forensic Science International

Is the assessment of bone age by the Greulich–Pyle method reliable at forensic age estimation for Turkish children? Bora Büken, Alp Alper Şafak, Burhan.

Comparing ballistic wounds with experiments on body simulator

Identification, extraction and quantification of the synthetic cannabinoid JWH-018 from commercially available herbal marijuana alternatives Sage J.B.

Cuiling Zhang, Joost van de Weijer, Jingxu Cui

Suspected clozapine poisoning in the UK/Eire, 1992–2003

Suspected clozapine poisoning in the UK/Eire, 1992–2003

Elemental analysis of glass by laser ablation inductively coupled plasma optical emission spectrometry (LA-ICP-OES) Emily R. Schenk, José R. Almirall

The discrimination of automotive clear coats by pyrolysis-gas chromatography/mass spectrometry and comparison of samples by a chromatogram library software

Forensic Science International

Nopporn Song-im, Sarah Benson, Chris Lennard

Forensic analysis of biodiesel

Relationship between methamphetamine use history and segmental hair analysis findings of MA users Eunyoung Han, Sangeun Lee, Sanghwan In, Meejung Park,

Evidence of mephedrone chronic abuse through hair analysis using GC/MS

Evidence of mephedrone chronic abuse through hair analysis using GC/MS

Natalija Novokmet, Zlatko Pavčec Forensic Science International

Methods for analyzing the uncertainty of a reconstructed result in a traffic accident with interval and probabilistic traces Tiefang Zou, Xulong Peng,

Performance of the RapidHIT™200

A. Barbaro, P. Cormaci, G. Falcone

C. Davies, J. Thomson, F. Kennedy

DNA typing of trace DNA recovered from different areas of sandals found at a homicide crime scene investigation: A comparative study Samuel T.G. Ferreira,

Establishment of Italian national DNA database and the central laboratory: Some aspects R. Biondo, F. De Stefano Forensic Science International: Genetics.

Sabine Michel, Anne De Bast, Isabelle Vandenbroere, Olivier Froment

Yan Liu, Li Li, Chengtao Li, Zhenmin Zhao

A custom software solution for forensic mtDNA analysis of MiSeq data

Population data for SE33 locus in United Arab Emirates Arab population

Confessions of a journal junkie

False homozygosity at D12S391 locus: A case report

Evaluating DNA profiles using peak heights, allowing for dropin, dropout and stutters Roberto Puch-Solis Forensic Science International: Genetics Supplement.

A review of low template STR analysis in casework using the DNA SenCE post-PCR purification technique T. Gross, J. Thomson, S. Kutranov Forensic Science.

Is it always possible to avoid exhumation in particular defective paternity cases by increasing autosomal STRs number? E. Carnevali, L. Caenazzo, N.

Analysis of forensic samples in Banco Nacional de Datos Genéticos

Determination of siblings: A special case report from Halle

C.J. Bruijning-van Dongen, K. Slooten, W. Burgers, W. Wiegerinck

N. Scaramozzino, P. Terrenoire, L. Baron

Testing the behavior of GlobalFiler® PCR amplification kit with degraded and/or inhibited biological samples V. Bogas, M. Carvalho, F. Corte-Real, M.J.

Semen detection: A retrospective overview from 2010

Application of less primer method to commercial kits

Eye colour and SNPs in Danes

Antoinette A. Westen, Titia Sijen

Influence of the luminol chemiluminescence reaction on the confirmatory tests for the detection and characterization of bloodstains in forensic analysis

Effects of the most common methods for the enhancement of latent fingerprints on DNA extraction from forensic samples S. Gino, M. Omedei Forensic Science.

Statistical aspects of familial searching

A.M. Ölçen, G. Filoğlu, H. Altunçul, S. Erdem, Ö. Bülbül

Presentation transcript:

Headspace-GC/MS detection of TATP traces in post-explosion debris A. Stambouli, A. El Bouri, T. Bouayoun, M.A. Bellimam Forensic Science International Volume 146, Pages S191-S194 (December 2004) DOI: 10.1016/j.forsciint.2004.09.060 Copyright © 2004 Elsevier Ireland Ltd Terms and Conditions

Fig. 1 GC/MS profile obtained from the injection of 1000μl of headspace explosion debris conditioned at 90°C, 30min (Tinj=270°C; Ttransferline=280°C; Tsource=180°C; Toven=40°C (2min), 5°C/min; 100°C (6min). Forensic Science International 2004 146, S191-S194DOI: (10.1016/j.forsciint.2004.09.060) Copyright © 2004 Elsevier Ireland Ltd Terms and Conditions

Fig. 2 Mass spectrum of triperoxide triacetone TATP I and diperoxide diacetone DADP II. Forensic Science International 2004 146, S191-S194DOI: (10.1016/j.forsciint.2004.09.060) Copyright © 2004 Elsevier Ireland Ltd Terms and Conditions

Fig. 3 HS-GC/MS chromatogram thermal decomposition of TATP; Tinj=270°C. Forensic Science International 2004 146, S191-S194DOI: (10.1016/j.forsciint.2004.09.060) Copyright © 2004 Elsevier Ireland Ltd Terms and Conditions

Fig. 4 HS-GC/MS chromatogram thermal decomposition of TATP avoided. Forensic Science International 2004 146, S191-S194DOI: (10.1016/j.forsciint.2004.09.060) Copyright © 2004 Elsevier Ireland Ltd Terms and Conditions

Fig. 5 Results of optimization of the heating zones temperature. Forensic Science International 2004 146, S191-S194DOI: (10.1016/j.forsciint.2004.09.060) Copyright © 2004 Elsevier Ireland Ltd Terms and Conditions

Fig. 6 Limit of the TATP detection (.1ng). Forensic Science International 2004 146, S191-S194DOI: (10.1016/j.forsciint.2004.09.060) Copyright © 2004 Elsevier Ireland Ltd Terms and Conditions