Rapid screening for detection and differentiation of detergent powder adulteration in infant milk formula by LC–MS  Manjun Tay, Guihua Fang, Poh Ling.

Slides:



Advertisements
Similar presentations
The most efficient STR loci in forensic genetics in population of central Poland R. Jacewicz, M. Jedrzejczyk, J. Berent Forensic Science International:
Advertisements

Illa Tea, Ingrid Antheaume, Ben-Li Zhang 
The importance of Guthrie cards and other medical samples for the direct matching of disaster victims using DNA profiling  D. Hartman, L. Benton, L. Morenos,
DNA profiling of trace DNA recovered from bedding
Headspace-GC/MS detection of TATP traces in post-explosion debris
Analysis of the headspace composition of smokeless powders using GC–MS, GC-μECD and ion mobility spectrometry  Monica Joshi, Kia Rigsby, Jose R. Almirall 
Cyanide quantification in post-mortem biological matrices by headspace GC–MS  Brigitte Desharnais, Geneviève Huppé, Martine Lamarche, Pascal Mireault,
Buprenorphine and major metabolites in blood specimens collected for drug analysis in law enforcement purposes  Stephanie Oechsler, Gisela Skopp  Forensic.
M. Gallidabino, C. Weyermann, R. Marquis 
Flávia de Souza Lins Borba, Ricardo Saldanha Honorato, Anna de Juan 
The ideal subject distance for passport pictures
Forensic Science International
Volatile organic compounds in polyethylene bags⿿A forensic perspective
Two fatal intoxication cases with imidacloprid: LC/MS analysis
Chemical characterization of synthetic cannabinoids by electrospray ionization FT-ICR mass spectrometry  Jade B. Kill, Izabela F. Oliveira, Lilian V.
The effect of sodium fluoride on the stability of cyanide in postmortem blood samples from fire victims  J.L. McAllister, R.J. Roby, Barry Levine, David.
Detecting and collecting traces of semen and blood from outdoor crime scenes using crime scene dogs and presumptive tests  A.G. Skalleberg, M.M. Bouzga 
Piotr Adamowicz, Dariusz Zuba, Karolina Sekuła 
Gregory McLaughlin, Vitali Sikirzhytski, Igor K. Lednev 
Előd Hidvégi, Péter Fábián, Zsuzsa Hideg, Gábor Somogyi 
A snapshot on NPS in Italy: Distribution of drugs in seized materials analysed in an Italian forensic laboratory in the period 2013–2015  Sara Odoardi,
A snapshot on NPS in Italy: Distribution of drugs in seized materials analysed in an Italian forensic laboratory in the period 2013–2015  Sara Odoardi,
Determination of ketamine and norketamine in hair by micropulverized extraction and liquid chromatography–high resolution mass spectrometry  Donata Favretto,
Detection of 3-methylmethcathinone and its metabolites 3-methylephedrine and 3- methylnorephedrine in pubic hair samples by liquid chromatography–high.
Purple discoloration of the colon found during autopsy: Identification of betanin, its aglycone and metabolites by liquid chromatography–high-resolution.
Direct analysis in real time high resolution mass spectrometry as a tool for rapid characterization of mind-altering plant materials and revelation of.
Simultaneous analysis of six amphetamines and analogues in hair, blood and urine by LC-ESI-MS/MS  Marjorie Chèze, Marc Deveaux, Claire Martin, Michel.
Optimization of an analytical method for detecting paraphenylenediamine (PPD) by GC/MS-iontrap in biological liquids  A. Stambouli, M.A. Bellimam, N.
Headspace-GC/MS detection of TATP traces in post-explosion debris
The homogeneity testing of EtG in hair reference materials: A high-throughput procedure using GC–NCI–MS  Bettina Mönch, Roland Becker, Christian Jung,
A high-throughput urinalysis of abused drugs based on a SPE-LC–MS/MS method coupled with an in-house developed post-analysis data treatment system  Wing-Chi.
Yun Sik Nam, Il Keun Kwon, Yeonhee Lee, Kang-Bong Lee 
Development of a GC–MS method for methamphetamine detection in Calliphora vomitoria L. (Diptera: Calliphoridae)  Paola A. Magni, Tommaso Pacini, Marco.
Profiling counterfeit Cialis, Viagra and analogs by UPLC–MS
UPLC-MS/MS determination in blood of a mixed-drug fatal intoxication: A case report  Paula Proença, João Miguel Franco, Carla Mustra, Carla Monteiro, Joana.
Evidence evaluation in fingerprint comparison and automated fingerprint identification systems—Modelling within finger variability  Nicole M. Egli, Christophe.
Gowri Vijay Reesu, Nathan Lee Brown  Forensic Science International 
Inhwan Han  Forensic Science International 
Comparing ballistic wounds with experiments on body simulator
An investigation into the behaviour of air rifle pellets in ballistic gel and their interaction with bone  G. Wightman, J. Beard, R. Allison  Forensic.
Identification, extraction and quantification of the synthetic cannabinoid JWH-018 from commercially available herbal marijuana alternatives  Sage J.B.
LC–MS method development and comparison of sampling materials for the analysis of organic gunshot residues  Anne-Laure Gassner, Céline Weyermann  Forensic.
Cuiling Zhang, Joost van de Weijer, Jingxu Cui 
Elemental analysis of glass by laser ablation inductively coupled plasma optical emission spectrometry (LA-ICP-OES)  Emily R. Schenk, José R. Almirall 
Előd Hidvégi, Péter Fábián, Zsuzsa Hideg, Gábor Somogyi 
The discrimination of automotive clear coats by pyrolysis-gas chromatography/mass spectrometry and comparison of samples by a chromatogram library software 
Forensic Science International
Comparison of latex body paint with wetted gauze wipes for sampling the chemical warfare agents VX and sulfur mustard from common indoor surfaces  Laura.
Fluorescence imaging of petroleum accelerants by time-resolved spectroscopy with a pulsed Nd-YAG laser  Naoki Saitoh, Shigeki Takeuchi  Forensic Science.
Automated region segmentation on cartridge case base
Nopporn Song-im, Sarah Benson, Chris Lennard 
Forensic analysis of biodiesel
Evidence of mephedrone chronic abuse through hair analysis using GC/MS
Evidence of mephedrone chronic abuse through hair analysis using GC/MS
Forensic classification of counterfeit banknote paper by X-ray fluorescence and multivariate statistical methods  Hongling Guo, Baohua Yin, Jie Zhang,
Martina Skenderović Božičević, Andreja Gajović, Igor Zjakić 
Simultaneous determination of creatinine and uric acid in urine by liquid chromatography–tandem mass spectrometry with polarity switching electrospray.
Simultaneous determination of creatinine and uric acid in urine by liquid chromatography–tandem mass spectrometry with polarity switching electrospray.
Natalija Novokmet, Zlatko Pavčec  Forensic Science International 
A. Barbaro, P. Cormaci, G. Falcone 
Evaluation of heteroplasmy detection in the Ion Torrent PGM
Establishment of Italian national DNA database and the central laboratory: Some aspects  R. Biondo, F. De Stefano  Forensic Science International: Genetics.
J.P. Pamplona, F. Freitas, L. Pereira 
Analysis of forensic samples in Banco Nacional de Datos Genéticos
Introducing a latent variable approach for finding populations in a forensic DNA database  Maarten Kruijver  Forensic Science International: Genetics.
Application of less primer method to commercial kits
Antoinette A. Westen, Titia Sijen 
Effects of the most common methods for the enhancement of latent fingerprints on DNA extraction from forensic samples  S. Gino, M. Omedei  Forensic Science.
M. Lurdes Pontes, M. Fátima Pinheiro 
Development of a 24-plex Y chromosomal STR loci typing system
Presentation transcript:

Rapid screening for detection and differentiation of detergent powder adulteration in infant milk formula by LC–MS  Manjun Tay, Guihua Fang, Poh Ling Chia, Sam Fong Yau Li  Forensic Science International  Volume 232, Issue 1, Pages 32-39 (October 2013) DOI: 10.1016/j.forsciint.2013.06.013 Copyright © 2013 Elsevier Ireland Ltd Terms and Conditions

Fig. 1 PCA score plots (centering) of 0–20% D1 adulterated in M2 samples acquired by LC-Qtrap in 12min LC run time under (a) negative electrospray ionization with R2(cum) and Q2(cum) values of 0.990 and 0.958 respectively], (b) positive electrospray ionization with R2(cum) and Q2(cum) values of 0.954 and 0.903 respectively. The numbers represent % adulteration level and ‘R’ represents samples for inter-day reproducibility test. Forensic Science International 2013 232, 32-39DOI: (10.1016/j.forsciint.2013.06.013) Copyright © 2013 Elsevier Ireland Ltd Terms and Conditions

Fig. 2 PCA score plots (centering) of M1 samples adulterated with 20% of various detergent brands by LC-Qtrap, 25min LC run time under (a) negative electrospray ionization and (b) positive electrospray ionization. Forensic Science International 2013 232, 32-39DOI: (10.1016/j.forsciint.2013.06.013) Copyright © 2013 Elsevier Ireland Ltd Terms and Conditions

Fig. 3 Contribution plot of the difference between adulterated and pure M3 samples analyzed by negative electrospray ionization LC-Qtrap, 25min LC run time. Forensic Science International 2013 232, 32-39DOI: (10.1016/j.forsciint.2013.06.013) Copyright © 2013 Elsevier Ireland Ltd Terms and Conditions

Fig. 4 (a) 3D PCA score plot (centering) and (b) zoomed-in image of the boxed up region (left) of pure M1 and adulterated M1 samples with 20% various detergent brands analyzed by negative electrospray ionization LC-QTOF–MS in 25min LC run time. Forensic Science International 2013 232, 32-39DOI: (10.1016/j.forsciint.2013.06.013) Copyright © 2013 Elsevier Ireland Ltd Terms and Conditions

Fig. 5 Total ion chromatograms of pure M1 and adulterated samples containing 20% of various detergent brands by negative electrospray ionization LC-QTOF–MS, 25min run time. Forensic Science International 2013 232, 32-39DOI: (10.1016/j.forsciint.2013.06.013) Copyright © 2013 Elsevier Ireland Ltd Terms and Conditions

Fig. 6 MS/MS spectrum of m/z 325.1843 ion in M1 sample adulterated with 20% D1 analyzed by negative electrospray ionization LC-QTOF–MS, 25min LC run time. Forensic Science International 2013 232, 32-39DOI: (10.1016/j.forsciint.2013.06.013) Copyright © 2013 Elsevier Ireland Ltd Terms and Conditions

Feedback: Privacy Policy Feedback
Do Not Sell My Personal Information
About project: SlidePlayer Terms of Service

© 2025 SlidePlayer.com. Inc. All rights reserved.