Evidence of mephedrone chronic abuse through hair analysis using GC/MS

Slides:



Advertisements
Similar presentations
The most efficient STR loci in forensic genetics in population of central Poland R. Jacewicz, M. Jedrzejczyk, J. Berent Forensic Science International:
Advertisements

Analysis of deteriorated rubber-based pressure sensitive adhesive by pyrolysis-gas chromatography/mass spectrometry and attenuated total reflectance Fourier.
Illa Tea, Ingrid Antheaume, Ben-Li Zhang 
The importance of Guthrie cards and other medical samples for the direct matching of disaster victims using DNA profiling  D. Hartman, L. Benton, L. Morenos,
DNA profiling of trace DNA recovered from bedding
Right heart ischemia in cases of sepsis
Gua Sha a traditional Chinese healing technique that could mimick physical abuse: A potential issue with forensic implications. A case study  A. Aprile,
Headspace-GC/MS detection of TATP traces in post-explosion debris
Validation of a headspace solid-phase microextraction–GC–MS/MS for the determination of ethyl glucuronide in hair according to forensic guidelines  Ronald.
Cyanide quantification in post-mortem biological matrices by headspace GC–MS  Brigitte Desharnais, Geneviève Huppé, Martine Lamarche, Pascal Mireault,
Buprenorphine and major metabolites in blood specimens collected for drug analysis in law enforcement purposes  Stephanie Oechsler, Gisela Skopp  Forensic.
The ideal subject distance for passport pictures
Volatile organic compounds in polyethylene bags⿿A forensic perspective
Fast LC–MS/MS method for the determination of amphetamine, methamphetamine, MDA, MDMA, MDEA, MBDB and PMA in urine  Marta Concheiro, Susana Maria dos.
Two fatal intoxication cases with imidacloprid: LC/MS analysis
High-performance combination method of electric network frequency and phase for audio forgery detection in battery-powered devices  Maryam Savari, Ainuddin.
The effect of sodium fluoride on the stability of cyanide in postmortem blood samples from fire victims  J.L. McAllister, R.J. Roby, Barry Levine, David.
Piotr Adamowicz, Dariusz Zuba, Karolina Sekuła 
Előd Hidvégi, Péter Fábián, Zsuzsa Hideg, Gábor Somogyi 
A snapshot on NPS in Italy: Distribution of drugs in seized materials analysed in an Italian forensic laboratory in the period 2013–2015  Sara Odoardi,
A snapshot on NPS in Italy: Distribution of drugs in seized materials analysed in an Italian forensic laboratory in the period 2013–2015  Sara Odoardi,
Determination of ketamine and norketamine in hair by micropulverized extraction and liquid chromatography–high resolution mass spectrometry  Donata Favretto,
Simultaneous determination of mushroom toxins α-amanitin, β-amanitin and muscarine in human urine by solid-phase extraction and ultra-high-performance.
Detection of 3-methylmethcathinone and its metabolites 3-methylephedrine and 3- methylnorephedrine in pubic hair samples by liquid chromatography–high.
Simultaneous analysis of six amphetamines and analogues in hair, blood and urine by LC-ESI-MS/MS  Marjorie Chèze, Marc Deveaux, Claire Martin, Michel.
Optimization of an analytical method for detecting paraphenylenediamine (PPD) by GC/MS-iontrap in biological liquids  A. Stambouli, M.A. Bellimam, N.
Effective injection in pulsed splitless mode for impurity profiling of methamphetamine crystal by GC or GC/MS  Tetsuro Sasaki, Yukiko Makino  Forensic.
Headspace-GC/MS detection of TATP traces in post-explosion debris
The homogeneity testing of EtG in hair reference materials: A high-throughput procedure using GC–NCI–MS  Bettina Mönch, Roland Becker, Christian Jung,
A high-throughput urinalysis of abused drugs based on a SPE-LC–MS/MS method coupled with an in-house developed post-analysis data treatment system  Wing-Chi.
Yun Sik Nam, Il Keun Kwon, Yeonhee Lee, Kang-Bong Lee 
Forensic Science International
Development of a GC–MS method for methamphetamine detection in Calliphora vomitoria L. (Diptera: Calliphoridae)  Paola A. Magni, Tommaso Pacini, Marco.
Fatal intoxication due to ackee (Blighia sapida) in Suriname and French Guyana. GC– MS detection and quantification of hypoglycin-A  Yvan Gaillard, Jérémie.
UPLC-MS/MS determination in blood of a mixed-drug fatal intoxication: A case report  Paula Proença, João Miguel Franco, Carla Mustra, Carla Monteiro, Joana.
Cathinone preservation in khat evidence via drying
Gowri Vijay Reesu, Nathan Lee Brown  Forensic Science International 
Inhwan Han  Forensic Science International 
Comparing ballistic wounds with experiments on body simulator
An investigation into the behaviour of air rifle pellets in ballistic gel and their interaction with bone  G. Wightman, J. Beard, R. Allison  Forensic.
Identification, extraction and quantification of the synthetic cannabinoid JWH-018 from commercially available herbal marijuana alternatives  Sage J.B.
Cuiling Zhang, Joost van de Weijer, Jingxu Cui 
Suspected clozapine poisoning in the UK/Eire, 1992–2003
Suspected clozapine poisoning in the UK/Eire, 1992–2003
Elemental analysis of glass by laser ablation inductively coupled plasma optical emission spectrometry (LA-ICP-OES)  Emily R. Schenk, José R. Almirall 
Reliability of the Suchey-Brooks method for a French contemporary population  Frédéric Savall, Camille Rérolle, Fabrice Hérin, Fabrice Dédouit, Daniel.
Előd Hidvégi, Péter Fábián, Zsuzsa Hideg, Gábor Somogyi 
The discrimination of automotive clear coats by pyrolysis-gas chromatography/mass spectrometry and comparison of samples by a chromatogram library software 
Forensic Science International
Comparison of latex body paint with wetted gauze wipes for sampling the chemical warfare agents VX and sulfur mustard from common indoor surfaces  Laura.
Some pyridine derivatives as “route-specific markers” in 4-methoxyamphetamine (PMA) prepared by the Leuckart method  Dariusz Błachut, Krystyna Wojtasiewicz,
The characterisation of two halogenated cathinone analogues: 3,5- Difluoromethcathinone and 3,5-dichloromethcathinone  Sean Davis, Karen Rands-Trevor,
Forensic analysis of biodiesel
Estimation of the measurement uncertainty of methamphetamine and amphetamine in hair analysis  Sooyeun Lee, Yonghoon Park, Wonkyung Yang, Eunyoung Han,
Relationship between methamphetamine use history and segmental hair analysis findings of MA users  Eunyoung Han, Sangeun Lee, Sanghwan In, Meejung Park,
Development and validation of a liquid chromatography–tandem mass spectrometry assay for hair analysis of atomoxetine and its metabolites: Application.
Evidence of mephedrone chronic abuse through hair analysis using GC/MS
Development and validation of a liquid chromatography–tandem mass spectrometry assay for hair analysis of atomoxetine and its metabolites: Application.
Forensic classification of counterfeit banknote paper by X-ray fluorescence and multivariate statistical methods  Hongling Guo, Baohua Yin, Jie Zhang,
Natalija Novokmet, Zlatko Pavčec  Forensic Science International 
A. Barbaro, P. Cormaci, G. Falcone 
Establishment of Italian national DNA database and the central laboratory: Some aspects  R. Biondo, F. De Stefano  Forensic Science International: Genetics.
Population data for SE33 locus in United Arab Emirates Arab population
Efficient DNA extraction from hair shafts
Analysis of forensic samples in Banco Nacional de Datos Genéticos
M. Hara, T. Masuda, A. Takada, T. Miyazaki, H. Suzuki, A. Kido, K
Application of less primer method to commercial kits
Effects of the most common methods for the enhancement of latent fingerprints on DNA extraction from forensic samples  S. Gino, M. Omedei  Forensic Science.
M. Lurdes Pontes, M. Fátima Pinheiro 
S. Cardoso, M. C. González-Fernández, A. Odriozola, L. Valverde, M. M
Presentation transcript:

Evidence of mephedrone chronic abuse through hair analysis using GC/MS M. Martin, J.F. Muller, K. Turner, M. Duez, V. Cirimele  Forensic Science International  Volume 218, Issue 1, Pages 44-48 (May 2012) DOI: 10.1016/j.forsciint.2011.10.016 Copyright © 2011 Elsevier Ireland Ltd Terms and Conditions

Fig. 1 Structures of mephedrone (1), methcathinone (2), cathinone (3) and amphetamine (4). Forensic Science International 2012 218, 44-48DOI: (10.1016/j.forsciint.2011.10.016) Copyright © 2011 Elsevier Ireland Ltd Terms and Conditions

Fig. 2 Gas chromatogram and full-scan mass spectrum of the heptafluorobutyric anhydride derivative of mephedrone. Forensic Science International 2012 218, 44-48DOI: (10.1016/j.forsciint.2011.10.016) Copyright © 2011 Elsevier Ireland Ltd Terms and Conditions

Fig. 3 Gas chromatograms of the heptafluorobutyric anhydride derivative of mephedrone (A–C) and MDMA-d5 (D) extracted from hair sample in selected ion monitoring. Forensic Science International 2012 218, 44-48DOI: (10.1016/j.forsciint.2011.10.016) Copyright © 2011 Elsevier Ireland Ltd Terms and Conditions