X-Ray Facility Overview

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Presentation transcript:

X-Ray Facility Overview IMB X-Ray Diffraction Facility 410-413 Kasha Laboratory www.sb.fsu.edu/~xray 850-644-6448 9/20/2018 © 2006 Thayumanasamy Somasundaram

X-Ray Facility Overview The Facility The Usage XRF-Amenities XRF-Services 9/20/2018 © 2006 Thayumanasamy Somasundaram

Cu Rotating Anode Generators Rigaku H2R 5.4kW High Brilliance Well Maintained Two Generators Four Ports 1.541 Å Wavelength www.rigaku.com 9/20/2018 © 2006 Thayumanasamy Somasundaram

Area Detector 1 (Image Plate) R-Axis IIc Two IPs Variable IP Distance Variable 2-Theta Eight Min. Read-out Digital Data Workhorse Unit www.rigaku.com 9/20/2018 © 2006 Thayumanasamy Somasundaram

© 2006 Thayumanasamy Somasundaram Area Dectector 2 (CCD) MarCCD165 Variable CCD Distance 3 s Read-out 80 um Resolution Quick Results www.mar-usa.com 9/20/2018 © 2006 Thayumanasamy Somasundaram

Osmic Blue/Purple Mirrors Easy Alignment Monochromatic Higher Flux Symmetric Focus www.osmic.com 9/20/2018 © 2006 Thayumanasamy Somasundaram

© 2006 Thayumanasamy Somasundaram Cryo Systems Oxford Cryo Systems 80 - 400 ± 0.1 K Programmable Two Systems One Auto-Refill www.oxfordcryosystems.co.uk 9/20/2018 © 2006 Thayumanasamy Somasundaram

© 2006 Thayumanasamy Somasundaram XRF Usage Averages 14 Users / Year 6 Groups / Year 3 Papers / Year 5 SyncDays / Year 9/20/2018 © 2006 Thayumanasamy Somasundaram

© 2006 Thayumanasamy Somasundaram XRF Yearly Usage 3 Main Groups (70%) 3 Other Groups (20%) XRF Usage (10%) 9/20/2018 © 2006 Thayumanasamy Somasundaram

Usage Efficiency Work Hours Max. 109% (2001-02) Min. 13% (1994-95) 38% (1993-1999) 79% (1999-2005) 9/20/2018 © 2006 Thayumanasamy Somasundaram

© 2006 Thayumanasamy Somasundaram Amenities 700 ft2 Main Lab 270 ft2 Crystal Room 170 ft2 Cold Room Crystal Chamber SER-CAT @ APS 9/20/2018 © 2006 Thayumanasamy Somasundaram

© 2006 Thayumanasamy Somasundaram Amenities Linux/Windows O/S Software License Data Archival Sample Set-up Sample Storage 9/20/2018 © 2006 Thayumanasamy Somasundaram

© 2006 Thayumanasamy Somasundaram Services Data Collection Data Processing Data Retrieval Sample Storage Sample Transport Synchrotron Help 9/20/2018 © 2006 Thayumanasamy Somasundaram

© 2006 Thayumanasamy Somasundaram Accessories Stereo Microscopes Digital Imaging Cryo Tools Stereo Desktops Portable Storage 9/20/2018 © 2006 Thayumanasamy Somasundaram