What did I learn in school today?

Slides:



Advertisements
Similar presentations
X-ray Diffraction and EBSD
Advertisements

Chap 8 Analytical Instruments. XRD Measure X-Rays “Diffracted” by the specimen and obtain a diffraction pattern Interaction of X-rays with sample creates.
Do it with electrons ! II.
Crystal diffraction Laue Nobel prize Max von Laue
Experimentally, the Bragg law can be applied in two different ways:
What is diffraction? Diffraction – the spreading out of waves as they encounter a barrier.
IPC Friedrich-Schiller-Universität Jena Contrast modes in light microscopy: Bright field.
CHAPTER 3: CRYSTAL STRUCTURES X-Ray Diffraction (XRD)
Are your X-ray powder diffraction patterns any good? Are your X-ray powder diffraction patterns any good?
Lecture 8b X-Ray Diffraction. Introduction I History 1895 Wilhelm Conrad R ӧ ntgen discovered X-rays 1905 Albert Einstein introduces the concept of photons.
X-ray powder diffractometer X-ray powder diffractometer.
Chem Single Crystals For single crystals, we see the individual reciprocal lattice points projected onto the detector and we can determine the values.
Atomic X-Ray Spectroscopy Chapter 12 X-ray range  Å to 100 Å Used  0.1Å to 25 Å.
IPCMS-GEMME, BP 43, 23 rue du Loess, Strasbourg Cedex 2
TEM- What is it?. Diffraction in the Transmission Electron Microscope Vidhya Sagar Jayaseelan.
X-Ray Diffraction ME 215 Exp#1. X-Ray Diffraction X-rays is a form of electromagnetic radiation having a range of wavelength from nm (0.01x10 -9.
Ge 116 Module 1: Scanning Electron Microscopy
Do it with electrons !. Microscopy Structure determines properties We have discussed crystal structure (x-ray diffraction) But consider now different.
Diffraction Basics II: Intensities
Chapter 7 X-Ray diffraction. Contents Basic concepts and definitions Basic concepts and definitions Waves and X-rays Waves and X-rays Crystal structure.
Chapter 12 Atomic X-Ray Spectroscopy
1 Refinement parameters What are the parameters to be determined? atom positional parameters atom thermal motion parameters atom site occupancy parameters.
Peak intensities Peak widths
X-Ray Diffraction Dr. T. Ramlochan March 2010.
PHYS 430/603 material Laszlo Takacs UMBC Department of Physics
Diffraction Basics Coherent scattering around atomic scattering centers occurs when x-rays interact with material In materials with a crystalline structure,
Microscopes Compound Bright-Field Light Microscope
Interference in Thin Films, final
Reminders for this week Homework #4 Due Wednesday (5/20) Lithography Lab Due Thursday (5/21) Quiz #3 on Thursday (5/21) – In Classroom –Covers Lithography,
~ Crystallography ~ Prof. Yu Wang Office: A507 Telephone: ~
1 Data Acquisition What choices need to be made?.
Electron Microcopy 180/ Useful info – many websites. Images here from
Lecture 6: Microscopy II PHYS 430/603 material Laszlo Takacs UMBC Department of Physics.
X-ray powder diffractometer X-ray powder diffractometer.
Least squares & Rietveld Have n points in powder pattern w/ observed intensity values Y i obs Minimize this function: Have n points in powder pattern w/
Page 1 Phys Baski Diffraction Techniques Topic #7: Diffraction Techniques Introductory Material –Wave-like nature of electrons, diffraction/interference.
The Muppet’s Guide to: The Structure and Dynamics of Solids XRD.
Diffraction: Intensity (From Chapter 4 of Textbook 2 and Chapter 9 of Textbook 1) Electron  atoms  group of atoms or structure  Crystal (poly or single)
The probe Some material used from:. EPMA - electron probe microanalysis Probe signals.
IPCMS-GEMME, BP 43, 23 rue du Loess, Strasbourg Cedex 2
复习 What did I learn in school today? 复习 What did I learn in school today?
ENGINEERING PHYSICS.
THE X-RAY DIFFRACTOMETER AND OTHER XRD INSTRUMENTATION Precession Camera.
Do it with electrons !. Microscopy Structure determines properties We have discussed crystal structure (x-ray diffraction) But consider now different.
X-ray powder diffraction
X-RAY METHODS FOR ORIENTING CRYSTALS
Presentation on.  There are many methods for measuring of fiber structure. Such as:  The absorption of infrared radiation  Raman scattering of light.
X-ray Crystallography - The Beginning
CHARACTERIZATION OF THE STRUCTURE OF SOLIDS
What do X-ray powder diffraction
Ch.4 Atomic Structure of Solid Surfaces.
Other imaging techniques
3.3 Other types of microscopy
Diffraction Literature:
TEM (Transition Electron Microscope)
X-ray Scattering from Thin Films
X-ray diffraction.
Chem5410 Q1 2/20 & 2/27/’06 1. What is so-called a single-crystal?
X-ray powder diffractometer.
Lecture 2.1 Crystalline Solids.
X-ray Neutron Electron
Institut Laue-Langevin
Do it with electrons !.
X-ray powder diffractometer.
Diffraction T. Ishikawa Part 1 Kinematical Theory 1/11/2019 JASS02.
Chap 8 Analytical Instruments
Crystal and X-ray Diffraction
Factors that affect the diffracted intensity
Chapter 16: Electron Diffraction
What if you use a capillary, small specimen or transmission technique
Presentation transcript:

What did I learn in school today? 复习 What did I learn in school today?

Must-know terms Crystallography symmetry operation - translation, rotation lattice, Bravais lattice unit cell crystal system point group, space group stereographic projection equipoint lattice plane, lattice direction

Must-know terms X-rays continuous radiation characteristic radiation synchrotron radiation mass attenuation coefficient absorption edge fluorescence

Must-know terms Diffraction Braggs' law reciprocal lattice Ewald construction Debye rings

Must-know terms Powder diffractometer focusing Soller slit divergence slit receiving slit monochromator detector deadtime

Must-know terms Powder diffraction patterns indexing extinction rule atomic scattering factor structure factor intensity multiplicity Lorentz polarization temperature factor peak breadth

Must-know terms Powder diffraction procedures diffractometer alignment calibration standards specimen displacement preferred orientation front fill, back fill, side drift zero background plate step size dwell time

Must-know terms Powder diffraction applications PDF Hanawalt search method quantitative analysis crystallite size microstrain Scherrer equation Williamson-Hall method

Must-know terms SEM microstructure matrix and precipitates backscattered electrons composition contrast secondary electrons topographic contrast depth of focus Wehnelt cup tunneling and field emission interaction volume

Must-know terms TEM back focal plane jet thinning ion milling camera constant relrods bright field dark field lattice imaging diffraction contrast

Must-know terms Optical microscopy index of refraction numerical aperture depth of field depth of focus etching

Must-know terms AFM contact and non-contact modes constant height constant force tapping mode force-distance plot