1H, 13C NMR, IR and MS Spectral data for Benzoin

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Presentation transcript:

1H, 13C NMR, IR and MS Spectral data for Benzoin

Disappears on addition of D2O

Nothing below 75 ppm

Mass spectrum of benzoin 27.0 3.7 29.0 3.0 39.0 5.1 50.0 8.9 51.0 30.4 52.0 4.5 53.0 2.7 63.0 2.9 74.0 2.3 76.0 2.9 77.0 75.8 78.0 11.9 79.0 48.1 80.0 3.2 105.0 100.0 106.0 11.1 107.0 63.6 108.0 4.9 165.0 1.5 212.0 (m/z)3.2 Peak data mass intensity m/z = 212

1H and 13C NMR Spectroscopic Data for the Grignard addition product of the reaction of benzoin with CH3MgI (you will get a mass spectrum and will obtain your own IR)

1H NMR Spectrum expansion Disappears on addition of D2O

13C NMR Spectrum CDCl3 product CDCl3 CDCl3