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CONSEQUENCES OF E-H TRANSITIONS IN IMPEDANCE MATCHING OF PULSED INDUCTIVELY COUPLED PLASMAS* Chenhui Qua), Steven Lanhama), Peng Tiana), Carl Smithb), Kristopher Fordb), Joel Brandonb), Steven Shannonb), and Mark J. Kushnera) 71st Gaseous Electronics Conference Portland, Oregon USA November 2018 * Work supported by the US Dept. of Energy Office of Fusion Energy Science, National Science Foundation, Lam Research and Samsung Electronics a) University of Michigan Ann Arbor, MI USA mjkush@umich.edu b) North Carolina State University Raleigh, NC USA schanno@ncsu.edu 1 1

University of Michigan Institute for Plasma Science & Engr. AGENDA Impedance matching in ICPs E-H Transition Description of Model CW: E-H transition Perfect matching Choosing a match point Experiment: Match point during pulse Duty cycle and IEDs Concluding Remarks Application for atm discharges University of Michigan Institute for Plasma Science & Engr. GEC_2018

POWER INTO ICP: LOAD ON TRANSMISSION LINE Inductively coupled plasmas (ICPs) are typically sustained by power from an RF generator through a cable transmission line (TL) – the plasma is the load at the end of the TL. Power delivered to the plasma reactor is  is the “reflection coefficient”. Since Z0 = 50  (usually) and, for example, ZP = 10 - i100 ,  can be close to 1 and little power gets into the plasma. pictures University of Michigan Institute for Plasma Science & Engr. GEC_2018

POWER INTO PLASMA: MATCHING NETWORK To trick the generator into thinking ZL = Z0 and  =0, an impedance matching circuit is used. C1, C2 and L (this is a -network) are chosen so that Zmatch = ZL = Z0. With pulsed plasmas, ZP changes during the pulse – difficult to match power into plasma during entire pulse. pictures University of Michigan Institute for Plasma Science & Engr. GEC_2018

E-H TRANSITION DURING PULSED ICPs Two modes of power deposition from RF antenna in pulsed inductively coupled plasmas: H-mode: EM waves launched from antenna are absorbed by plasma EM skin depth must be short compared to depth of plasma Dominates at high power and high plasma density Power dominantly dissipated by electron collisions. E-mode: Electrostatic coupling to plasma due to high voltage on antenna. Dominates at low power, low plasma density, thick sheaths Power dominantly dissipated by ion acceleration. During pulsing, E-H mode transition can occur further complicating matching. University of Michigan Institute for Plasma Science & Engr. GEC_2018 5

University of Michigan Institute for Plasma Science & Engr. DESCRIPTION OF MODEL Hybrid Plasma Equipment Model (HPEM) Transmission line representation of antenna (coil) with match box model. Capacitive coupling results from coil voltage in Poisson solution and capacitive impedance in Circuit Module University of Michigan Institute for Plasma Science & Engr. GEC_2018 6

University of Michigan Institute for Plasma Science & Engr. MATCH BOX AND COIL Capacitive coupling is natural outcome of including voltage on coil in solving Poisson’s equation. Coil voltage and current obtained by representing coil as transmission line (TL) with physical and transformed plasma impedance, ZTL. Capacitive plasma impedance ZP from Fourier from analysis of (r,z) coil displacement current and voltage. ZTL and ZP provide ZL. University of Michigan Institute for Plasma Science & Engr. GEC_2018 7

University of Michigan Institute for Plasma Science & Engr. CW E-H MODES With CW perfect match, smooth transition between E- (capcitive power) to H- (inductive power) modes. E-mode power mostly ion acceleration in sheaths. Ar/Cl2 = 65/35, 25 mTorr, Rcoil = 0.1 , LP = 100 nH, LT = 5 nH, CT = 100 nF University of Michigan Institute for Plasma Science & Engr. GEC_2018

University of Michigan Institute for Plasma Science & Engr. CW E-H MODES Increase in plasma density with power: Shorter skin-depth improves inductive coupling. Thinner sheath reduces capacitive power transfer. Less ion acceleration improves ionization efficiency ([e]/power) Ar/Cl2 = 65/35, 25 mTorr, Rcoil = 0.1 , LP = 100 nH, LT = 5 nH, CT = 100 nF University of Michigan Institute for Plasma Science & Engr. GEC_2018

E-H TRANSITION DURING PULSED ICP E-Mode Power H-Mode Power Pulsed ICPs in halogen gases have small electron densities at the start of the pulse. The plasma starts in “E- mode” (capacitive) and transitions to “H-mode” (inductive). Large change in ZLoad further complicates matching. Ar/Cl2 = 65/35, 25 mTorr, PRF = 13.3 kHz, Duty Cycle = 35%, Forward Power = 250 W. 0-50 s University of Michigan Institute for Plasma Science & Engr. Animation Slide GEC_2018

PERFECT MATCH WITH E-H TRANSITION Calculate CP and CS to provide a perfect match vs time. ZL has positive reactance from coil. Initial E-mode operation requires smaller CS as to match generator, ZG. Decrease in ZL reactance during pulse due to capacitive coupling that contributes negative reactance. Ar/Cl2 = 65/35, 25 mTorr, PRF = 13.3 kHz, Duty Cycle = 35%, Forward Power = 250 W. University of Michigan Institute for Plasma Science & Engr. GEC_2018

PERFECT MATCH WITH E-H TRANSITION Calculate CP and CS to provide a perfect match vs time. E-mode indicated by initial capacitive power dissipation resulting from initial low electron density. Initial E-mode accompanied by large coil voltage, large oscillation in plasma potential. H-mode starts with power dominated by inductive coupling. Steady state has 5-10% capacitive power. Ar/Cl2 = 65/35, 25 mTorr, PRF = 13.3 kHz, Duty Cycle = 35%, Forward Power = 250 W. University of Michigan Institute for Plasma Science & Engr. GEC_2018

EARLY MATCH WITH E-H TRANSITION Choose CP and CS to provide a perfect match to ZG at t = 3 s near E- to H-mode transition. Reflection coefficient  = 0 at match time enables rapid increase in delivered power. Mismatch at later time during dominantly H-mode operation produces  = 0.25. Ar/Cl2 = 65/35, 25 mTorr, PRF = 13.3 kHz, Duty Cycle = 35%, Forward Power = 250 W. University of Michigan Institute for Plasma Science & Engr. GEC_2018

University of Michigan Institute for Plasma Science & Engr. MATCHING WITH E-H TRANSITION Choose “perfect match” values of CP,S at different times. Early match emphasizes capacitive coupling. Later matches reduces capacitive coupling and delays inductive power with better overall match. Ar/Cl2 = 65/35, 25 mTorr, PRF = 13.3 kHz, Duty Cycle = 35%, Forward Power = 250 W. University of Michigan Institute for Plasma Science & Engr. GEC_2018

MATCHING PULSED PLASMAS Reflection Coefficient (Z0=50 ohm) During a pulsed ICP period, ZLoad changes. Must choose values of C1 and C2 to match ZLoad at some point during pulsed period. Demonstrate with Ar, pulsed ICP University of Michigan Institute for Plasma Science & Engr. GEC_2018 15

PULSED ICP, FIXED MATCHBOX Power: Yellow: Forward Blue: Reflected Match early in pulsed ( = 0), plasma density rises quickly but mismatch late in pulse when power is high – lower electron density. Match late in pulse, plasma density rises slowly but higher [e] due to better match when power is high. Ar, 5 mTorr Match point as indicator of degree of mismatch. Scaling of plasma properties with different mismatch conditions-delayed match points. University of Michigan Institute for Plasma Science & Engr. GEC_2018

MATCHING WITH E-H TRANSITION: DUTY CYCLE Plasma Potential Small duty cycle results in low electron density at start of next pulse, producing dominant E-mode, high impedance, large coil voltage. Large oscillation in plasma potential with low duty cycle. Large duty cycle – higher electron density at start of pulse and smoother transition to H-mode. Ar/Cl2 = 65/35, 25 mTorr, PRF = 13.3 kHz, Forward Power = 250 W. University of Michigan Institute for Plasma Science & Engr. GEC_2018

University of Michigan Institute for Plasma Science & Engr. IEDs ONTO WINDOW The transient and large sheath voltage during the E-H transition produces energetic ion bombardment onto the dielectric window. Ar/Cl2 = 65/35, 25 mTorr, 13.3 kHz, 25% Duty Cycle, Forward: 250 W. University of Michigan Institute for Plasma Science & Engr. GEC_2018

University of Michigan Institute for Plasma Science & Engr. CONCLUDING REMARKS Power delivery to inductively coupled plasmas (ICPs) is challenged by impedance matching for operation in either E-mode or H-mode. During pulsed operation in attaching gases, low electron density at start of pulse translates to initial E-mode. As plasma density increases, transition occurs to H-mode. Must typically choose match values Impedance matching network for some point in pulse. Early matches emphasize capacitive power – poor H-mode match. Late matches prevent power transfer early in pulse – better H- mode match. E-mode producing large amplitude oscillations in plasma potential, producing ion acceleration into windows. Some form of real-time impedance matching required during pulse – frequency tuning? University of Michigan Institute for Plasma Science & Engr. GEC_2018