Fig. 5 ATR-FTIR spectra supporting the assignment of band B to an oxo structure. ATR-FTIR spectra supporting the assignment of band B to an oxo structure.

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Fig. 5 ATR-FTIR spectra supporting the assignment of band B to an oxo structure. ATR-FTIR spectra supporting the assignment of band B to an oxo structure. (A) Time profiles of integrated IR bands during curing of LO/Zn at 190°C on the ATR crystal. The disappearance of the C═CH stretch vibration band at 3009 cm−1 is a measure for the extent of polymerization, while the reduction of the band at 530 cm−1 is attributed to a loss of symmetry in the central Zn4O unit (see also fig. S3). (B) Time profiles of absorbance at the frequencies corresponding to the components A, B, and C of the broad carboxylate band envelope during curing. (C) IR spectra under dry conditions (150°C) of LO/Zn with decreasing neutralization, demonstrating the correlation between the concentration of COOH groups and the relative concentration of chain and oxo complex. Joen. J. Hermans et al. Sci Adv 2019;5:eaaw3592 Copyright © 2019 The Authors, some rights reserved; exclusive licensee American Association for the Advancement of Science. No claim to original U.S. Government Works. Distributed under a Creative Commons Attribution NonCommercial License 4.0 (CC BY-NC).