Fig. 1 Precursor suspensions for spin coating and the obtained monolayer films. Precursor suspensions for spin coating and the obtained monolayer films.

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Fig. 1 Precursor suspensions for spin coating and the obtained monolayer films. Precursor suspensions for spin coating and the obtained monolayer films. (A) Typical precursor DMSO nanosheet suspensions for spin coating: Bottles i to v contain the suspensions of Ti0.87O20.52− (large, 0.3 wt %), Ti0.87O20.52− (small, 0.36 wt %), Ca2Nb3O10− (1.38 wt %), GO (0.072 wt %), and rGO (0.045 wt %), respectively. (B) SEM image of the monolayer film obtained by spin coating the suspension of i. A single nanosheet is highlighted by a red polygon. (C to G) AFM images of the monolayer films via spin coating of the suspensions of i to v. The thickness of the nanosheets in (C) to (G) was ~1.4, 1.0, 2.3, 1.1, and 1.0 nm, respectively, which is consistent with the values reported for the unilamellar nanosheets. On the other hand, the average lateral size was ~10, 0.3, 2, 2, and 1 μm, respectively, which is compatible with the textural appearance of the suspensions. Kazuaki Matsuba et al. Sci Adv 2017;3:e1700414 Copyright © 2017 The Authors, some rights reserved; exclusive licensee American Association for the Advancement of Science. No claim to original U.S. Government Works. Distributed under a Creative Commons Attribution NonCommercial License 4.0 (CC BY-NC).