Archaeometry using Ion Beams

Slides:

Advertisements

Similar presentations

The 26g Al(p, ) 27 Si Reaction at DRAGON Heather Crawford Simon Fraser University TRIUMF Student Symposium July 27, 2005.

Advertisements

Equipe Couches Nanométriques : Formation, Interfaces, Défauts

Dan Gabriel Ghiţă IFIN-HH

High-Speed PIXE A spatially resolved PIXE setup at the

Ion beam Analysis Joele Mira from UWC and iThemba LABS Tinyiko Maluleke from US Supervisor: Dr. Alexander Kobzev Dr. Alexander Kobzev.

Ion Beam Analysis techniques:

Professor: Scott M. LaBrake Course: Physics 300 – Spring 2013 Office: NWSE N308, N008b Phone: & 6562 Office Hours: MWF.

AMCF Materials Characterization School 2012 X-Ray Photoelectron Spectroscopy Tim Morgan.

A.Lagoyannis I.N.P.P. NCSR “Demokritos” Nuclear Physics Applications at the Institute of Nuclear and Particle Physics A. Lagoyannis Institute of Nuclear.

ERDA, for measurement of hydrogen in PV applications

Study of sputtering on thin films due to ionic implantations F. C. Ceoni, M. A. Rizzutto, M. H. Tabacniks, N. Added, M. A. P. Carmignotto, C.C.P. Nunes,

Ion Beam Analysis Part 1 Henri I. Boudinov

Setup for large area low-fluence irradiations with quasi-monoenergetic 0.1−5 MeV light ions M. Laitinen 1, T. Sajavaara 1, M. Santala 2 and Harry J. Whitlow.

BYU Ion Beam Analysis Facility Particle accelerators are used for materials analysis Jointly operated by Physics and Astronomy and Chemistry and Biochemistry.

The Work Being Done at the Ion Beam Laboratory at Texas A&M University Van D. Willey Columbia High School Under the Direction of Lin Shao Assistant Professor.

Istituto Nazionale Fisica Nucleare

Cross section measurements for analysis of D and T in thicker films Liqun Shi Institute of Modern Physics, Fudan University, Shanghai, , People’s.

Seminar Author: Bojan Hiti Mentor: doc. dr. Matjaž Kavčič Determination of trace impurities on Si wafers with x-ray fluorescence.

Precise neutron inelastic cross section measurements A.Negret 1 1 “Horia Hulubei” National Institute for Physics and Nuclear Engineering, Bucharest, ROMANIA.

The 1 st Research Coordination Meeting Reference Database for PIGE Van de Graaff Lab in Tehran activities.

PHYSICAL SCIENCE VOCABULARY WEEK 10. 1) HYDROGEN Symbol – H Atomic Number – 1 Combines with oxygen to form water.

Radiation Detection and Measurement, JU, 1st Semester, (Saed Dababneh). 1 Radiation Sources Heavy nuclei are unstable against spontaneous emission.

Centre de Toulouse Radiation interaction with matter 1.

Ion Beam Analysis Dolly Langa Physics Department, University of Pretoria, South Africa Blane Lomberg Physics Department, University of the Western Cape,

Korea Institute of Geoscience and Mineral Resources (KIGAM) Thin Film Analysis by Ion Beam Techniques W. Hong, G. D. Kim, H. J. Woo, H. W.

FRANK LABORATORY OF NEUTRON PHYSICS ION BEAM ANALYSIS STANCIU-OPREAN LIGIA SUPERVISOR DR. KOBZEV ALEXANDER.

Depth Profiling with Low-Energy Nuclear Resonances H.-W. Becker, IAEA May 2011 CRP: Reference Database for Particle Induced Gamma-ray Emission (PIGE) Ruhr-University.

Water infusion and drug effusion in drug release polymers and drug diffusion in mucosae and muscle A S Clough, F E Gauntlett, M S Rihawy University of.

Nuclear and Radiation Physics, BAU, First Semester, (Saed Dababneh). 1 Nuclear Reactions Sample.

FRANK LABORTORY OF NEUTRON PHYSICS ION BEAM ANALYSIS

Introduction Montelupo Fiorentino is a little town about 20 km west of Florence, characterised by the presence of a large number of ceramic and glass factories.

Tshepo Mahafa P-LABS Necsa 1 CHARGED PARTICLE IRRADIATION EFFECTS ON ZIRCALOY-4 Necsa_Wits Workshop, 10 – 11 September 2015, Necsa, Pelindaba.

NATIONAL TECHNICAL UNIVERSITY OF ATHENS DEPARTMENT OF PHYSICS A Detailed Study of the 10,11 B(d,α) and 10,11 B(d,p) Reactions at Detector Angles between.

Detection of trace elements in meteorites using PIXE Presented by: Sasha dos-Santos.

Duncan Weathers Department of Physics University of North Texas.

2. RUTHERFORD BACKSCATTERING SPECTROMETRY Basic Principles.

1 A. Kitamura, H. Iwai, R. Nishio, R. Satoh, A. Taniike and Y. Furuyama Department of Environmental Energy Science, Graduate School of Science and Technology,

Characterization of nuclear transmutations by 638 nm laser beams ( ¹ ) STMicroelectronics, via Tolomeo, Cornaredo Milano-I ( ² ) Applied Electronics.

NATIONAL TECHNICAL UNIVERSITY OF ATHENS DEPARTMENT OF PHYSICS NRA studies at the INP Tandem: Present status and perspectives M. Kokkoris 1, C. T. Papadopoulos.

Daniela Adriana LĂCĂTUŞ1 Supervisor: Alexander Pavlovich KOBZEV

Accelerator Physics, JU, First Semester, (Saed Dababneh). 1 Electron pick-up. ~1/E What about fission fragments????? Bragg curve stochastic energy.

UL UNIVERSIDADE DE LISBOA CENTRO DE FÍSICA NUCLEAR People: Senior Researchers (responsible for activity lines): Eduardo Alves (Head of Lab) Adelaide Pedro.

Physics Colloquium Ⅱ Shibata Laboratory OKA, Hiroki Nucleosyntheses studied with a Van de Graaff Accelerator [Contents] 1. Objective.

Basics of Ion Beam Analysis

Rutherford Backscattering Spectrometry (RBS)

Questions/Problems on SEM microcharacterization Explain why Field Emission Gun (FEG) SEM is preferred in SEM? How is a contrast generated in an SEM? What.

Karolina Danuta Pągowska

Rita Ramos IBA RCM, Nov 2005 MEASUREMENT OF PROTON ELASTIC SCATTERING CROSS SECTIONS FOR LIGHT ELEMENTS – VALIDATION OF A “BULK SAMPLE”

Accelerator Based Techniques for Air Pollution Studies Across Asia David Cohen, ANSTO, Sydney, Australia

Overview of Tandem Accelerator Facility and related R&D Work at NCP Ishaq Ahmad

Neutron production and iodide transmutation studies using intensive beam of Dubna Phasotron Mitja Majerle Nuclear Physics Institute of CAS Řež, Czech republic.

Shuya Ota: Japan Atomic Energy Agency, Rutgers University H. Makii, T. Ishii, K. Nishio, S. Mitsuoka, I. Nishinaka : Japan Atomic Energy Agency M. Matos,

Non-destructive compositional investigation of historical enamels by combining portable alpha-PIXE and XRF imaging techniques H.C. Santos, C. Caliri, L.

Potku – A New Analysis Software for Heavy Ion Elastic Recoil Detection Analysis K. Arstila 1, J. Julin 1, M.I. Laitinen 1, J. Aalto 2, T. Konu 2, S. Ka.

Chandrayaan-2 Large Area Soft X-ray Spectrometer (CLASS)

22nd International Conference on Ion Beam Analysis, June , 2015- Opatija, Croatia Characterization and source apportionment of fine particulate.

Young Researchers Session in IFIN-HH 2016

Roger Webb University of Surrey Ion Beam Centre

Department of Tandem Accelerators

PIXE measurements of heavy metals of Tsunami sediment samples

Chapter 3 History of the Atom.

Direct measurements for nuclear

Technogical transfer department

Bucharest-Magurele, Romania M. BOROMIZA - Trieste, October, 2017

ASSESSMENT OF CONCRETE USING NUCLEAR TECHNIQUES

ION BEAM ANALYSIS.

Elastic alpha scattering experiments

Chapter 5 - Interactions of Ionizing Radiation

Thin Film Analysis by Ion Beam Techniques

Ion Beam Analysis (IBA)

Presentation transcript:

Archaeometry using Ion Beams Dragos Alexandru MIREA - Department of Tandem Accelerators dragos.mirea@nipne.ro IFIN-HH Days, 21 December 2016, Măgurele

Ion Beam Analysis Rutherford BackScattering Energy of scattered protons or He give light element composition and elemental depth profiles sample 1-4 MeV proton beam or 1-6 MeV He beam PIXE/PIGE Characteristic X-ray emission Simultaneous part-per-milion detection of trace elements from Li to U Elastic Recoil Detection Analysis Foreward recoil of target atoms (particulary good for H profiling) Nuclear Reaction Analysis Nuclear reactions give characteristic gamma rays and particles from light nuclei 17 September 2019

PIXE Analysis Collaboration with A. Dragoman from Vasile Pârvan Institute of Archaeology In-Air PIXE preferred due to the sample’s dimensions 3 axis positioning system with sample holding capacity used Proton beam used, 3MeV, ~10nA (IBA chamber) NIST? Nu, nu avem standarde cu aceeasi matrice. Am incercat un NIST 1412, erori mari. Necesar un standard cu aceeasi matrice. De ce elemente? Asa s-a cerut. Minimum 2 points on each surface. Maximum 6 on the same sample 2 points on each identified pigment – Red, White and Black 17 September 2019

Archaeological site Căscioarele (CL) Călărași county, Căscioarele Archaeological site dated to Neolithic Age (~1500 – 1800 BC) Photo source: Google Maps Photo source: Google Maps Multiple artefacts discovered. 35 samples sent to IFIN-HH for PIXE analysis Pigment and ceramic paste characterisation 17 September 2019

Pottery samples analyzed 17 September 2019 Photo credits: A. Dragoman

Pottery samples results percentage Photo credits: A. Dragoman percentage percentage 17 September 2019

Pottery samples results white red paste percentage Photo credits: A. Dragoman percentage percentage 17 September 2019

Results overview White pigment Beam penetrated Concentration (%) the pigment layer Concentration (%) Red pigment Elements 17 September 2019

Conclusions A succesfull test for the In-Air PIXE system developped at IFIN-HH A new opportunity for collaboration opened Samples analyzed in safe conditions, returned to owner undamaged Two types of pigments identified. White mainly implies calcite and other calcium white compounds, quartz varieties, kaolinite, even monohidrated calcium oxalates. Red is dominated by iron oxides (hematite in a possible mixture with magnetite, denoting a specific thermal treatment), and by silicon dioxide varieties Results presented at 5BSA in Sinaia, September 2016 by A. Dragoman 17 September 2019

Perspectives A good resolution obtained, but Si-PIN detector unable to separate Si from Al Si + Al ?? 2 new SDD X-ray detectors to be installed for IN-AIR PIXE analysis resolution 130 eV resolution 127 eV Photo credits: 3MV Tandetron Team 17 September 2019

Perspectives The current laser positioning system for samples needs improvement New laser positioning system to be installed Photo credits: 3MV Tandetron Team Photo credits: 3MV Tandetron Team 17 September 2019

Perspectives The current video survailance system New IP 3MP video camera to be installed Photo credits: 3MV Tandetron Team Photo credits: 3MV Tandetron Team 17 September 2019

In-air Particle Induced X-ray Emission Presented in 2015 IFIN-HH Young Researcher’s Annual Session (actual presented slide) Desired experimental setup: 2 new X-ray detectors a plexiglass ermetic chamber an ultra fast valve a He flow system (homemade) a high resolution video camera for microPIXE experiments a Faraday cup for in-air beam current measurment 17.12.2015

THANK YOU FOR YOUR ATTENTION ! The 3MV Tandetron Team Andrei Radu, Burducea Ion, Chelărescu Dana, Mirea Dragoș, Morărescu Cezar, Ravar Mădălina, Rugină Andrei and Straticiuc Mihai Wish you Merry Christmas and Happy New Year! Contact & Collaboration: dragos.mirea@nipne.ro Beam Time: pac.bucharest@tandem.nipne.ro 17 September 2019

17 September 2019

Pottery samples results - Back-up Photo credits: A. Dragoman 17 September 2019

Pottery samples results – Back-up white red paste Photo credits: A. Dragoman 17 September 2019