Fig. 3 Double-resonance solid-state NMR data of ceria nanoparticles.

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Fig. 3 Double-resonance solid-state NMR data of ceria nanoparticles. Double-resonance solid-state NMR data of ceria nanoparticles. (A, top to bottom) 17O MAS NMR spectra of ceria nanoparticles adsorbed with 17O water followed by thermal treatment under vacuum at 373 K at 14.1 and 9.4 T; difference spectrum in 17O-1H REDOR experiments; and 1H-17O CP MAS NMR spectrum with a contact time of 100 μs. (B) The peak intensity in CP MAS NMR experiment as a function of contact time. Spectra were obtained at both 9.4 and 14.1 T under MAS rates of 13 to 14 kHz. One thousand to 40,000 scans were averaged, and recycle delays from 0.2 to 1 s were used. Asterisks denote spinning sidebands. Meng Wang et al. Sci Adv 2015;1:e1400133 Copyright © 2015, The Authors