Mapping the Free Energy Landscape of HIV-1 TAR RNA with Metadynamics Tyler J. Mulligan 1, Harish Vashisth 2 1 M.S. Student, Department of Chemical Engineering,

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Mapping the Free Energy Landscape of HIV-1 TAR RNA with Metadynamics Tyler J. Mulligan 1, Harish Vashisth 2 1 M.S. Student, Department of Chemical Engineering, University of New Hampshire, Durham NH 2 Advisor, Department of Chemical Engineering, University of New Hampshire, Durham NH ABSTRACT INTRODUCTION HIV-1 trans-activated response element (TAR) RNA is the RNA molecule located in the human form of the immunodeficiency virus. This TAR RNA molecule plays an essential role in the reproduction of viral proteins, and ultimately the reproduction of virions themselves. Through the use of molecular simulation methods such as steered molecular dynamics (SMD) and Metadynamics, the free energy landscape of this RNA is to be mapped. SMD will allow for a quantitative analysis of the force required to break the nucleotide interactions of TAR RNA, while Metadynamics will allow for quantitative analysis of the free energy barriers between the various low energy conformations that TAR RNA encounters on its way to the folded native state. HIV affects Human T-Cells 50,000 infected yearly in the US Globally over 35 million people have HIV 36 million have died as a result of the virus TAR RNA assists in reproduction of viral proteins (ribozyme) TAR RNA has multiple metastable conformations that give yield to multiple functions HIV-1 TAR RNA References Steered MD of TAR RNA HIV-1 TAR RNA (right) molecule rendered using VMD [1] The Hairpin loop can be seen in yellow The 3-nucleotide bulge in green Both structures play an important role Orange (Cytosine) Yellow (Guanine) Blue (Adenine) Green (Cytosine) RNA Hairpin Loop 3-nucleotide bulge SMD Parameters Cell size (angstroms) X: 58 Y: 47 Z: 188 2fs timestep NPT ensemble SMD k constant: 7 SMD vel.: 0.05 A/ps SMD dir: X(0) Y(0) Z(1) Minimize 100 steps Ran for 4 ns 216,000 atoms Ions: Mg Cl Aqueous, not implicit solvent. [1] Humphrey, W., Dalke, A. and Schulten, K., "VMD - Visual Molecular Dynamics", J. Molec. Graphics, 1996, vol. 14, pp [2] Knightly, Russell. “HIV AIDS Virus Replication (viral Life Cycle).” Diagram by Russell Knightly Media. Web. Oct [3] Cheng, Bingqing. "Quora." How Does Metadynamics Calculate the Potential Mean Force (PMF) or the Free Energy Profile of a Reaction Coordinate? June Web. 4 Oct [4] James C. Phillips, Rosemary Braun, Wei Wang, James Gumbart, Emad Tajkhorshid, Elizabeth Villa, Christophe Chipot, Robert D. Skeel, Laxmikant Kale, and Klaus Schulten. Scalable molecular dynamics with NAMD. Journal of Computational Chemistry, 26: , Force vs. Time averaged over 10 identical SMD runs Pulling velocity 0.05 A/ps The dashed line represents 0pN of force Black line shows the averaged force Average of about 100pN of force Elongated RNA resolvated and used as starting molecule for Metadynamic simulations Pulling force analysis for 10 averaged SMD simulations for HIV-1 TAR RNA. METADYNAMICS Metadynamics is a method to explore the free energy landscape in a large collective coordinate space. The height and width of the energy gaussians are manipulated and added at a certain frequency to explore the depth of the free energy wells. This allows for the RNA molecule to explore metastable states that it may not be able to reach in a standard simulation. [2] Diagram by Russell Knightly Media. The two graphs below show the molecules free energy in kcal/mol (Z) ΔG= 1.5 Kcal/mol ΔG= 2.5 Kcal/mol ΔG= 4 Kcal/mol ΔG= 1 Kcal/mol ΔG= 2 Kcal/mol Acknowledgements All images were produced using VMD [1] All simulations were run using NAMD [4]. We would also like to thank the University of New Hampshire for allowing our group access to the Trillian Supercomputer. Simulation Parameters: Box Dimensions 59x64x168 (A) NPT Ensemble 1.0 fs timestep Colvar width 2.0 Hill Weight 0.1 Hill Frequency ,644 atoms Red: Bulge Green: Hairpin t= 0pst= 267pst= 533pst= 800pst= 1.1nst= 1.4ns Pulling Velocity: 0.05 A/ps