EPA’s Revised Minimum Quantification Levels Scott Wilson.

Slides:



Advertisements
Similar presentations
Laurie Eng Water Quality Standards Group Jill Csekitz Surface Water Quality Monitoring Team Guidance Advisory Workgroup Meeting June 16, 2011.
Advertisements

Watershed Staff Videoconference October 17, 2012.
National Air Quality Conference -- Addison, Texas – March 2, Analysis Methods for Lead in TSP and PM 10 ICP-MS ICP-AES/OES ED-XRF.
© Copyright 2014 Loveland Tech4good T4G Arsenic Detection Techniques Loveland Tech4good Luke Whitaker / May 27, 2014.
1 Atomic Absorption Spectroscopy Atomic Emission Spectroscopy Lecture 18.
AAS and FES (Ch 10, 7th e, WMDS)
1 Atomic Absorption Spectroscopy. 2 Atomic Transitions: Excitation and Emission.
Emission Spectroscopy Based upon Plasma, Arc, and Spark Atomization Arc Arc Higher Temperature Higher Temperature Lower interelement interference Lower.
Outcome of Federal Actions on WA Water Quality Standards.
Using the Clean Water Act to Reduce Mercury in the Northeast Susy King September 8, 2010.
Instrumental Chemistry Chapter 11 Atomic Mass Spectrometry.
Atomic spectra are a result of energy level diagrams - quantum theory.
Evaluation of Several Field Test Kits for Determining Concentrations of Arsenic in Drinking Water J. Mitchell Spear, You “Mark” Zhou Charles A. Cole and.
A L B I O N E N V I R O N M E N T A L U.S. EPA REGION SIX & OKLAHOMA & ARKANSAS DEPARTMENTS OF ENVIRONMENTAL QUALITY 24 th ANNUAL PRETREATMENT ASSOCIATION.
Chapter 8 – Mass Spectrometry. Mass Spectrometry The mass spectrometer can be used for: – Quantitative analysis – as a sophisticated and very sensitive.
Implementation of Antidegradation Policies for Indiana Waters.
Impaired and TMDL Waterbody Listings Impacts on DoD Facilities Bill Melville, Regional TMDL Coordinator
2012 Determination of RRVs for DEQ-7. What is an RRV? “The RRV (Required Reporting Value) is the detection level that must be achieved in reporting surface.
in tin pest and pest free Monika Leodolter-Dvorak and Ilse Steffan
Mass spectrometry Ions are analyzed on the basis of their m/z Chlorine has 2 isotopes, 35 Cl and 37 Cl, in the approximate ratio of 3 :1. Electrons are.
Mercury Sources to Water and Associated Impacts Chris Piehler.
VIRGINIA’S TMDL PROCESS.
Water Quality Planning Division Monitoring & Assessment Section Surface Water Quality Monitoring Program (SWQM)
2015 Environmental Trade Fair and Conference Jill Csekitz Technical Specialist TCEQ Monitoring & Assessment Section Devils River State Natural Area Image.
1 IDEM Overview of March 14, 2008 Draft Antidegradation Rule Presented at the April 29, 2008 Antidegradation Stakeholder Meeting.
Florida Numerical Nutrient Criteria Southwest Florida Water Resources Conference Scott I. McClelland Vice President November 20, 2009.
Update on EPA Underground Injection Control (UIC) Program Activities: Presentation at the KDHE Geology Section’s Fall 2012 Seminar David Garrett, Environmental.
ANALYTICAL CHEMISTRY CHEM 3811 CHAPTER 20
COMPARISON OF DIFFERENT ANALYTICAL TECHNIQUES FOR ENVIRONMENTAL MONITORING OF CONTAMINATED SOILS Metodi Mladenov, Daria Ilieva University of Chemical Technology.
California Measure SB375: Linking Greenhouse Gas Emissions Reductions to Metropolitan Transportation Planning Presentation to the National Capital Region.
EPA REGION VI MINIMUM QUANTIFICATION LEVELS (MQLs) WHAT THE “L” IS GOING ON? 25 th EPA Annual Pretreatment Workshop Addison, TX 8/5/09 Allen Gilliam ADEQ.
Benefits of the Redesigned RMP to Regional Board Decision Making Karen Taberski Regional Water Quality Control Board San Francisco Bay Region.
ATOMIC SPECTROMETRY 1. Flames 2. Electrothermal Atomizers 3. Plasmas.
1 Analytical Methods for Perchlorate: Current Technology and Possibilities for the Future David J. Munch Daniel P. Hautman Office of Ground Water and Drinking.
Combining and Choosing Analytical Techniques Chapter 8.
Notebook Ref Summary of the Issue Part of a Tier II antidegradation review should incorporate the consideration of feasible alternatives, some of.
Is There a Link Between Epizootic Lobster Shell Disease and Contaminants? Lawrence A. LeBlanc 1, L. Brian Perkins, and Deanna Prince 1 1 School of Marine.
IMPROVE Algorithm for Estimating Light Extinction Draft Recommendations to the IMPROVE Steering Committee.
William Telliard U.S. EPA Office of Science and Technology
Detecting Aluminum in Drinking Water Erica Sandoval.
Review of Annex 1 - GLWQA Doug Spry Workshop convened by the Parties Implementation Work Group of the Science Advisory Board of the International Joint.
1 Water Quality Antidegradation: Guidance to Implement Tier II Summary of Discussion: Review the Tier II Rule requirements. Clarify what feedback we are.
Is Your Analytical Result Accurate? Presented By: James S. Smith, Ph.D. Trillium, Inc. GSA North-Central Section 39 th Annual Meeting Minneapolis, Minnesota.
Covalent Bonding in hydrogen chloride Click to continue.
SWRCB Public Workshop for Periodic Review January 10-12, 2005 Slide 1 Issue 4c New Objectives Greg Gartrell Assistant General Manager Contra Costa Water.
Connie Brower NC DENR Division of Water Resources.
George E. Detsis Manager, Analytical Services Program United States Department of Energy Office of Health, Safety and Security Office of Sustainability.
SAFE DRINKING WATER GENERAL UPDATE TO CHAPTER 109 June 19, 2007 Bureau of Water Standards and Facility Regulation.
Texas Surface Water Quality Standards Update Joe Martin Water Quality Standards Work Leader Joe Martin Water Quality Standards Work Leader.
Toxic Metals in Mine Tailings Dust Presented by: Paul Rheinheimer Acknowledgements: NASA Space Grant Consortium Susan Brew Susan Brew Brian Barbaris Brian.
The Method Update Rule Does this affect me? HOW?
Specialists in environmental solutions
Submittal And Review Of New And Revised Water Quality Standards
Overview of EPA Method 1631, Revision E By Roy W
Water Quality Standards Submittal & Review Process
Water Quality Planning Division Monitoring & Assessment Section
Sources of the PM10 aerosol in Flanders, Belgium, and re-evaluation of the contribution from wood burning Willy Maenhaut1,2, Reinhilde Vermeylen2, Magda.
RPA and the DEQ Drive for Lower Detection Limits
Homework #5 1. a) What are the EPA standards dealing with air quality in terms of particulate matter? b) How are they being revised? c) Give the rationale.
Biogeochemical Cycle of Mercury (Hg)
التعلم بالإكتشاف المراجع:
Spencer Bohaboy Policy Development Specialist Water Quality Policy
Request for Approval to Proceed to Public Hearing on the Triennial Review of Surface Water Quality Standards.
Adopt an Element By:.
Water Quality Planning Division Monitoring & Assessment Section
Atomic Math Challenge.
Marco island water quality monitoring
Water Quality Planning Division Monitoring & Assessment Section
2019 AWOP National Meeting Office of Ground Water and Drinking Water
2018 State Implementation Plan for the Imperial County 12 ug/m3 PM2
Presentation transcript:

EPA’s Revised Minimum Quantification Levels Scott Wilson

MQL Background First developed in 1992 Adopted by EPA Region 6 states and most other EPA Regions Based on –Atomic Adsorption –Furnace –Gas Chromatography/Mass Spectrometry

Revised MQLs In 2004, examined MQLs which were greater than water quality criteria (37) Examined newer methods and MQLs commonly achieved by labs Issues with Mercury

Revised MQLs Concentrated review on routinely achievable levels Routine levels were lower than previous MQLs for 33 of the 37 parameters Routine levels were lower than criteria for 13 parameters

Revised MQLs Based on: –Inductively Coupled Plasma Mass Spectrometry for metals (EPA method 200.8) –Gas Chromatography/Mass Spectrometry for most organics (EPA Method 624/625) –Gas Chromatography with Electron Capture Detector for pesticides (EPA Method 608) –Spectrophotometric Method for Chlorine (EPA Method 330.5)

Revised MQLs Mercury –Priority due to numerous fish advisories nationally –Choice of EPA Methods 1631 or 245.7

Revised MQLs EPA has implemented in permits for New Mexico Specific Methods are not required –Required to meet the MQL –May use any EPA approved methods –May obtain approval for alternative methods Other States are in the process of implementing revised MQLs

Scott Wilson EPA Region 6 telephone: