From the Amino Acid Structures to Metal Hydrides: Four Decades of Single-Crystal Neutron Diffraction Thomas F. Koetzle Suffolk Community College Selden,

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Presentation transcript:

From the Amino Acid Structures to Metal Hydrides: Four Decades of Single-Crystal Neutron Diffraction Thomas F. Koetzle Suffolk Community College Selden, New York ACA Honolulu July 20-24,2013 Bau Award Lecture AW.01 Work at Brookhaven and Argonne National Laboratories was Supported by the Office of Science, U. S. Department of Energy.

Single-Crystal Neutron Diffractometers at the Brookhaven High Flux Beam Reactor

SCD Instrument at Argonne IPNS 3 Figures, dated circa 2005, courtesy of Arthur Schultz

4 Neutron and X-Ray Scattering Amplitudes Adapted from Bacon, G. E., “Neutron Diffraction”; 3 rd Ed.; Oxford University Press: London, 1975.

Discrimination of Hydrogen from Deuterium in a Neutron Fourier Map 5 Determination of the Absolute Configuration for + Neopentyl-1-d alcohol (S) Yuan, H.S. et al. Proc. Natl. Acad. Sci. U.S.A. 1994, 91,

Modeling Disorder in a Type II Gas Hydrate: 3.5Xe·8CCl 4 ·136D 2 O 6 CCl 4 chlorine scattering densityCCl 4 encapsulated in 16-hedron McMullan, R.K.; Kvick, Å. Acta Crystallogr., Sect. B 1990, B46,

Pittsburgh Diffraction Conference, Photo courtesy of J. S. Ricci, Jr.

Air-Sensitive Crystal Sealed in a Quartz Tube Ready for Neutron Data Collection at IPNS 8 Large Crystal Size! Photo, dated circa 2006, courtesy of Paula Piccoli and Arthur Schultz

Amino Acids 9 Lehmann, M. S.; Koetzle, T. F.; Hamilton, W. C. J. Am. Chem. Soc. 1972, 94,