Industrialization of Electropolishing (EP) D.Proch, DESY EP is the preferred cleaning method for superconducting Nb resonators (besides Buffered Chemical.

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Presentation transcript:

Industrialization of Electropolishing (EP) D.Proch, DESY EP is the preferred cleaning method for superconducting Nb resonators (besides Buffered Chemical Polishing, BCP) There are experimental type EP installations in several laboratories Worldwide there was only one industrial EP facility at Japan (Nomura plating) EP activities in CARE: –Optimize EP parameters (DESY, Saclay, INFN Legnaro) –Transfer EP technology to industry –Develop quality assurance methods (QA) for EP

Electro-chemistry of EP Oxidation 2 Nb + 5 SO H2O  Nb2 O H+ + 5 SO e- Reduction Nb2 O5 + 6 HF  H2 NbOF5 + Nb O2 F 0.5 H2 O H2 O Nb O2 F 0.5 H2 O + 4 HF  H2 Nb O F H2 O Important: –HF is a very toxic acid!!! –Hydrogen gas is produced

Principle arrangement of EP

New EP electrode at DESY EP Al cathode Acid injection hole on top of the cavity equator Teflon insulator covering the electrode in the beam tube area PE spacer holding the TEFLON Nitrogen overlay tube PTFE net covering the electrodes

Details of the EP mechanical frame Figure 4 Details of the EP mechanical frame at DESY. timing belt disc, disk for sliding current transmitter) Timing belt disc Disks for sliding current transmitter Current leads

Cathode feed trough at the beam pipe flange current leads alumina electrode Nitrogen overlay inlet pipe disc for sliding current transmitter Gas outlet towards exhaust cleaner ( nitrogen, hydrogen and evaporated HF)

EP installation at DESY

EP Installation at Henkel,1

EP installation at Henkel,2

EP installation at ACCEL

Best candidates for EP electrolyte quality assurance (Henkel Study) Titration ICP-OES (inductively coupled plasma- optical emission spectroscopy) IC (ionic-chromatography) TOC (total organic carbon) NMR (nuclear magnetic resonance) FTIR-ATR-probe (Fourier transformation infrared spectroscopy –attenuated total reflection)

Overview QA methods for EP electrolyte (Henkel study)

Summary EP industrialization,1 The goal of this task was to explore and optimize the important operating parameters of the DESY EP system and to transfer this technology to industry. At DESY 176 EP treatments of 9-cell cavities have been carried out The EP technology has been successfully transferred to industry. Two companies (ACCEL and Henkel) have designed, built, installed and operated EP installations based on the experience with electropolishing at DESY.

Summary EP industrialization,2 Up to now ACCEL and Henkel have treated 24 cavities in total In addition a QA strategy for the EP electrolyte has been worked out by Henkel company Electropolishing infrastructure & expertise at two companies is available now in Europe for EP cleaning of TTF type multi-cell Nb resonators

Hazard of HF Repair of a leak in the heat exchanger