ECOLOGYCAL PURITY AND AUTHENTICITY OF BULGARIAN ORIENTAL TOBACCO World Tobacco North America– The Future Supply of Leaf Tobacco Richmond, Virginia, 05/12/2015.

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ECOLOGYCAL PURITY AND AUTHENTICITY OF BULGARIAN ORIENTAL TOBACCO World Tobacco North America– The Future Supply of Leaf Tobacco Richmond, Virginia, 05/12/2015

Krumovgrad 90, Region Petrich Krumovgrad 90, Region Gorna Dgumaia

Krumovgrad 58, Region Krumovgrad Krumovgrad 58, Region Krumovgrad

Tobacco and Tobacco Products Institute, Plovdiv, Bulgaria

Ecological Purity of Bulgarian Oriental Tabaco

№ Indicator Unit of measure Standard/ Validated method Results of the Analysis Indicator tolerance (CORESTA standard) (year) 1.Organochlorine pesticidesISO Sum of heptachlor and heptachlorepoxide μg/g n.d.* n.d.0,1 1.2Endosulfan alfa, beta μg/g n.d. 1,0 1.3Sum of aldrin and dieldrin μg/g n.d. 0,1 1.4Hexachlorobenzene μg/g n.d. 0,1 1.5Endrin μg/g n.d. 0,05 1.6HCH and isomers μg/g n.d. 0,5 1.7Sum of DDT and isomersq DDE and DDD μg/g n.d. 0,4 2.Dithiocarbamate pesticides, total estimated as CS 2 μg/g ISO 64660,40±0,010,970±0,0255,0 n.d.* - not detected Content of pesticide residues in the "Kabakulak" tobacco variety group, vintage 2006 and 2010.

No Indicator Unit of measure Standard/ Validated method Results of the Analysis Indicator Tolerance (CORESTA standard) (year) 1.Organochlorine pesticidesISO Sum of heptachlor and heptachlorepoxide μg/g n.d.* n.d.0,1 1.2Endosulfan alfa, beta μg/g n.d. 1,0 1.3Sum of aldrin and dieldrin μg/g n.d. 0,1 1.4Hexachlorobenzene μg/g n.d. 0,1 1.5Endrin μg/g n.d. 0,05 1.6HCH and isomers μg/g n.d. 0,5 1.7Sum of DDT and isomersq DDE and DDD μg/g n.d. 0,4 2.Dithiocarbamate pesticides, total estimated as CS 2 μg/g ISO 64660,20±0,020,710±0,015,0 n.d.* - not detected Content of pesticide residues in the "Basma" tobacco variety group, vintage 2006 and 2010.

No Indicator Unit of Measure Standard/Validated method Results of the Analysis Indicator Tolerance 1.Heavy metalsБДС Cooper (Cu)mg/kg16,90±1, Zinc (Zn)mg/kg45,50±3, Lead (Pb)mg/kg3,00±0, Cadmium (Cd)mg/kg2,50±0,25- 2.Specific activity of the radionuclidesIEC U 238Bq/kg9,0*- 2.2Ra 226Bq/kg5,2±2,1- 2.3Th 232Bq/kg2,0±0,8- 2.4K 40Bq/kg616± Pb 210Bq/kg ＜ 31* - 2.6Bi 214Bq/kg0,9±0,4- 2.7Pb 214Bq/kg0,8±0,4- 2.8Cs 137Bq/kg ＜ 0,32- *- less than the limit of determination Content of heavy metals and specific activity of natural and technogenic radionuclides in the "Kabakulak" tobacco variety group, vintage 2006

№ Indicator Unit of Measure Standard/Validated method Results of the Analysis Indicator Tolerance 1.Heavy metalsБДС Cooper (Cu)mg/kg10,58±0, Zinc (Zn)mg/kg42,25±3, Lead (Pb)mg/kg3,50±0, Cadmium (Cd)mg/kg1,65±0,16- 2.Specific activity of the radionuclidesIEC U 238Bq/kg9,1*- 2.2Ra 226Bq/kg9,0±1,9- 2.3Th 232Bq/kg11,3±1,0- 2.4K 40Bq/kg637± Pb 210Bq/kg34± Bi 214Bq/kg3,0±0,4- 2.7Pb 214Bq/kg3,1±0,4- 2.8Cs 137Bq/kg3,9±0,3- *- less than the limit of determination Content of heavy metals and specific activity of natural and technogenic radionuclides In the "Basma" tobacco variety group, vintage 2006