InfraCal Ethanol Blend Analyzer Ethanol in Gasoline Sample Analysis for Low Levels www.WilksIR.com.

Slides:



Advertisements
Similar presentations
Salk Institute Mobile Lab Gel Electrophoresis Teacher Instructions Edvotek Set Up 12 groups.
Advertisements

InfraCal TOG/TPH Analyzer, Model HATR-T2 Extraction Procedure.
DNA in My Food???. What is DNA ? Determines characteristics of all living organisms Composed of a four-letter nucleotide/molecule alphabet referred to.
Salk Institute Mobile Lab Gel Electrophoresis Teacher Instructions VWR Set Up 12 groups Mira Costa kit.
1 USDOC41 Rev 0 1/04 Training and Education Program ©2004 HemoCue, Inc. HemoCue ® Training and Education Program The HemoCue Hb System.
InfraCal TOG/TPH Analyzer, Model CVH Extraction Procedure.
Titration By Dr H W Winter.
Separation Techniques LSS 1 Term 3. Mixtures and Pure Substances Recap: How do we define mixture? A mixture contains two or more constituent substances.
1 Objective:The objective of this experiment is to determine the mass of acetylsalicylic acid (ASA) in an Aspirin tablet. Chemicals Potassium hydrogen.
Separation of Mixtures
LAB SAFETY! WHAT DO YOU DO? HOW SHOULD YOU DO IT? WHAT HAPPENS IF YOU DO IT WRONG?
Salk Institute Mobile Lab Gel Electrophoresis Teacher Instructions BioRad Set Up 8 groups Grossmont Kit.
1 | Vigyan Ashram | INDUSA PTI |. 1.Stainless steel knife 2.Stainless steel Pot 3.Mixer grinder 4.Stainless steel plates, etc. 5.Pan balance with weights.
Miscible or Immiscible
By Adam Wanetik, Spencer Olesky And also Daniel Broadie
Serial Dilutions. 0.2 g/mL NaCl Stock Solution NaCl STOCK solution Make a 0.2-g/mL NaCl STOCK solution - Add 2 g of sodium chloride to beaker and add.
InfraCal TOG/TPH Analyzer, Model CVH Calibration.
DNA Extraction Activity. Why extract DNA from a…….? Demonstrate that food actually has DNA in it! One study showed that some people think that traditionally.
 A mixture is two or more substances that have been combined without any chemical reaction. The substances can easily be separated by boiling or dissolving.
Chemical Energy Conversions Vanderbilt Student Volunteers for Science Spring 2015.
Using Laboratory Equipment Chapter 3
Performing a titration A bluffers guide! Preparing a standard solution 4 Accurately weigh a weighing bottle, recording the mass 4 Add approximately x.
Today: Quiz Thursday / Friday May 16/17 HW – Read pages Worksheet – Concentrations of solutions Worksheet - Molarity Problems 1.
Solutions.
Friday, Feb. 21 st : “A” Day Monday, Feb. 24 th : “B” Day Agenda  Collect chromatography labs  Begin Section 13.2: “Concentration and Molarity” 
Controlling Variables
DNA in My Food???. What is DNA ? Where do you find DNA?
Chapter 15 Solutions. Solution types & parts  Solutions can be: Solids – brass, dental fillings, chocolate bar Liquids – sodas, vinegar, salt water Gaseous.
How to get DNA from common food items.  A routine procedure to collect DNA for subsequent molecular or forensic analysis.DNAmolecularforensic  DNA is.
4.6 To prepare one enzyme immobilisation and examine its application
DETERMING CONCENTRATIONS OF SOLUTIONS. MOLAR Molar is mol solube/1 L solution Making molar solution 1)Add ½ of the total solvent 2)Add required amount.
Serial Dilutions Example!
Catalyst: 1.What is the solubility of potassium nitrate in 80 g of water at 60°? g KCl is dissolved in 100 g of water that is at 80°. What would.
InfraCal Ethanol Blend Analyzer Ethanol in Gasoline Calibration for High Levels
Layered Solutions: A Lab on Density. Observations/ Data: -The red solution was a little murky with some of the salt not settled. -Yellow and green seemed.
Saturation. Dissolving Does sodium chloride dissolve in water? Yes How do we know? It disappears into the water. It is still there because the sodium.
After completing this topic you should be able to : State to accurately neutralise an acid using a solution containing an alkali or a carbonate requires.
Unit 1- Matter and Measurement Chapter 1 in text book Day 1.
InfraCal Biodiesel Blend Analyzer Biodiesel in Diesel Calibration.
Solutions Chapter 14.
InfraCal Ethanol Blend Analyzer Ethanol in Gasoline Calibration for Low Levels
2001 Extension Annual Conference Communicating About Agricultural Biotechnology DNA IN MY FOOD??? Presented by Dr. Terri L. Lomax Director, Program for.
Fruit Cup DNA Extraction. Step 1 Into one of the 5 oz cups add 1 teaspoon of shampoo. Fruit Cup DNA Extraction.
DNA Isolation Lab.
InfraCal TOG/TPH Analyzer, Model HATR-T2 Calibration
Lab Instructions. Materials and Equipment Distilled Water Zinc metal Filter Paper Plastic Wash Bottle Copper II sulfate Tap water Pencil (not a pen) Plastic.
It’s Lab Day! Think back to middle school physical science class
Preparing Solutions.
Solubility Noadswood Science, 2012.
Solutions & Solubility Solution Preparation. Solution Preparation from a solid  Standard Solution = a solution for which the precise concentration is.
Analysis of fruit juices_2. Determination of saccharin Objective: To determine the amount of saccharine which may be added to fruit juice Introduction.
Solutions Mixtures (Varied Ratio) Homogeneous True Solutions (Soluble) Solubility – Ability to dissolve in solution (aq) See only 1 part Separated by.
Solutions Molarity = concentration term used to describe an amount of solute dissolved in a given amount of solvent. Concentrated solution = contains large.
Lab # 8. Key Terms Homogeneous Vs. Heterogeneous Saturated Vs. Unsaturated Solute Vs. Solvent Moles Vs Molarity Percent Weight and Percent Volume.
Solutions Investigation 8. Part 1 - Mixtures What is a Mixture? G:\ISTCS\School papers\Science\8th grade\Chemical Interactions\Media\Mixtures.wmv.
How to extract DNA from anything living
Extracting DNA from Green Peas
Lab 13 How Much Solute Dissolves in a Solvent
Calculating Concentrations
Calculating Concentrations
Experiment 2 RECRYSTALLIZATION.
Preparing Standard Solutions
Gel Electrophoresis Teacher Instructions BioRad Set Up 12 groups
Fruit Cup DNA Extraction.
Controlling Variables
Crystal Growing Experiment
Ethanol - Corn Mash and Distillation
Experiment 2 RECRYSTALLIZATION.
Year 7 multiple-choice main test: answers 7H Solutions
Ethanol - Corn Mash and Distillation
Presentation transcript:

InfraCal Ethanol Blend Analyzer Ethanol in Gasoline Sample Analysis for Low Levels

For the most accurate measurement, an ethanol free gasoline sample from the same stock as the ethanol/gas sample to be analyzed can be used to zero out any differences in gasoline makeup Zeroing on Gasoline: Background Measurement

Since ethanol free gasoline is not always available, the ethanol can be extracted from the gasoline in order to zero the analyzer Zeroing on Gasoline: Background Measurement

To extract the ethanol, the gasoline sample is mixed with a salt water solution which collects the ethanol, leaving ethanol free gasoline Zeroing on Gasoline: Background Measurement

If ethanol free gasoline of the same type to be measured is available, this step can be skipped. Note: If the gasolines to be analyzed are similar in chemical makeup, or if the measurement requirements allow up to a 1% error, zeroing can be done on a clean crystal without the base gasoline or the extraction step. Zeroing on Gasoline: Background Measurement

Salt Water for Extraction 1.Add 1 liter of distilled water to container. 2.Add 20g (1 tablespoon) of sodium chloride (table salt) to the water. The exact amount is not important. to the water. The exact amount is not important. 3. Stir the solution until all the salt is dissolved Note: This solution can be made in any quantity as long as the ratio of water to salt is kept similar. Background Measurement

Ethanol Extraction: 1. Add 2 parts salt water and 1 part gasoline of sample to be analyzed to glass container (~ 10 ml of salt water to 5 ml gasoline) 2. Cover the container and shake for 30 seconds 3. Allow the solution to settle (~ 30 seconds) There should now be two layers in the container. The top layer is ethanol free gasoline 4. There should now be two layers in the container. The top layer is ethanol free gasoline

Clean the crystal with a delicate task wipe cleaning from one end of the crystal to the other Background Measurement

Using a pipette, carefully remove approximately 2 ml of zero sample from the top layer of the extracted gasoline. Do not allow the pipette to come in contact with the bottom layer. Using a pipette, carefully remove approximately 2 ml of zero sample from the top layer of the extracted gasoline. Do not allow the pipette to come in contact with the bottom layer. Background Measurement

Apply the sample so that the entire crystal is wet and close the stainless steel cover Background Measurement

Press and hold the ZERO button until the display reads bAL Recall ZERO CAL RUN bAL Background Measurement

Recall ZERO CAL RUN A multiplier value to 3 decimal places will be displayed when zero is established The actual value is only of interest when reporting problems to the factory Background Measurement

Recall ZERO CAL RUN 0.0 Background Measurement Press RUN The display should read If not, repeat the zero process

Ensure that the gasoline sample to be analyzed is the same as the sample used in the background collection Sample Analysis

Apply approximately 2ml of the fuel sample ensuring that the entire crystal is wet Sample Analysis

Close cover to keep volatiles from evaporating Sample Analysis

Recall ZERO CAL RUN 0.0 Press RUN Sample Analysis

Recall ZERO CAL RUN 5.7 Sample Analysis After 15 seconds the result is displayed

Clean the crystal with a delicate task wipe cleaning from one end of the crystal to the other The InfraCal is ready for the next sample Sample Analysis

InfraCal Ethanol Blend Analyzer Ethanol in Gasoline Sample Analysis for Low Levels For questions please contact us at: or