Ethox Chemical, LLC Evaluation of Ethox Blended Lubes versus Standard EBS in MPIF F-0000 (Test #3) Product Assurance Services, Inc. PAS Job# 7195 JUN 2008.

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Ethox Chemical, LLC Evaluation of Ethox Blended Lubes versus Standard EBS in MPIF F-0000 (Test #3) Product Assurance Services, Inc. PAS Job# 7195 JUN 2008

Lubricant TypeHall Apparent Density, g/cc (*=assisted) Hall Flow Rate, sec./50g Mix CompositionAncorsteel 1000B+0.75% Lube Atomized Acrawax EAS EAS EAS EAS EAS Evaluation of Ethox Blended Lubes versus Standard EBS in MPIF F-0000 (Test #3) Hall Apparent Density and Flow Rate

Evaluation of Ethox Blended Lubes versus Standard EBS in MPIF F-0000 (Test #3) Green Properties Mix Composition 1000B % Lube Lubricant Type Green 50 TSI g/cc Green 50 TSI Psi 50 TSI Green Spring from Die 50 TSI, % from Die Atom. Acrawax Good0.19 EAS Good0.25 EAS Terrible0.32 EAS High0.24 EAS High0.45 EAS High0.44 EAS High0.52 EAS High0.58 EAS High0.54 EAS High0.57 EAS High0.28 EAS High0.29

Evaluation of Ethox Blended Lubes versus Standard EBS in MPIF F-0000 (Test #3) Green Properties Mix Composition 1000B % Lube Lubricant Type Green 50 TSI g/cc Green 50 TSI Psi 50 TSI Green Spring from Die 50 TSI, % from Die EAS High0.24 EAS Good0.19 EAS Good0.28 EAS High0.21 EAS Good0.22 EAS High0.23 EAS Good0.21 EAS High0.22 EAS Good0.21 EAS High0.19 EAS Good0.21

Evaluation of Ethox Blended Lubes versus Standard EBS in MPIF F-0000 (Test #3) Sintered Properties Compaction Tonnage, 50 TSI Lubricant Type Sintered Density g/cc Sintered TRS ksi Sintered DC from Die Size % in./in. Sintered Hardness, HRF Atomized Acrawax EAS EAS EAS EAS EAS F 95%N2/5% H2 3.5 in./min.

Evaluation of Ethox Blended Lubes versus Standard EBS in MPIF F-0000 (Test #3) Conclusions Samples 8-1, 8-4, 8-6, 8-8, 8-10 had comparable properties to EBS. 8-1 and 8-4 were unacceptable for sintering because of Low TRS strength. 8-6, 8-8, 8-10 showed similar hardness and density, but had higher sintered Dimensional Change, Lower TRS, and some evidence of residue on the surface. Based on the similarity of results between these three samples, they appear to be similar in composition. I think we should focus on these three samples, and try to figure out where the delubing issue is coming from. We may solve the other problems once we determine why we are having residue.