Kukolich Laboratory: Electronics, Inorganic Synthesis & Scientific Glassblowing Daniel A. Sánchez 04/17/10 NASA Space Grant: University of Arizona Chemistry.

Slides:

Advertisements

Similar presentations

FOURIER TRANSFORM EMISSION SPECTROSCOPY AND AB INITIO CALCULATIONS ON WO R. S. Ram, Department of Chemistry, University of Arizona J. Liévin, Université.

Advertisements

Development of a Reduced-Cost CP-FTMW Spectrometer Using Direct Digital Synthesis Ian Finneran Daniel Holland Brandon Carroll Geoffrey Blake California.

1 Extreme Ultraviolet Polarimetry Utilizing Laser-Generated High- Order Harmonics N. Brimhall, M. Turner, N. Herrick, D. Allred, R. S. Turley, M. Ware,

The Search is Over: Design and Applications of a Chirped Pulse Fourier Transform Microwave (CP- FTMW) Spectrometer for Ground State Rotational Spectroscopy.

MONITORING REACTION PRODUCTS USING CHIRPED-PULSE FOURIER TRANSFORM MICROWAVE SPECTROSCOPY Derek S. Frank, Daniel A. Obenchain, Wei Lin, Stewart E. Novick,

Charles Kime & Thomas Kaminski © 2008 Pearson Education, Inc. (Hyperlinks are active in View Show mode) Chapter 3 – Combinational Logic Design Part 1 –

2.4 Chemical Reactions and Enzymes Standard B.1.2

Fig 10: I-V characteristics of Au/PDNC/Al/Au junction. This shows that the molecule has rectification towards the positive bias. Current (A) M I A M I.

Optically Pumping Nuclear Magnetic Spin M.R.Ross, D.Morris, P.H. Bucksbaum, T. Chupp Physics Department, University of Michigan J. Taylor, N. Gershenfeld.

Sensors used in EFI (Electronic Fuel Injection)

Pulse Box Engineering Nikitha Ramohalli University of Arizona Advisor: Dr. Stephen Kukolich, Professor, Department of Chemistry and Biochemistry, University.

Power Converter Systems

X-Ray Diffraction Spectroscopy RAMAN Microwave. What is X-Ray Diffraction?

Introduction to Chemistry. Objectives What is chemistry and how is it part of everyday life What are the basic units of measurement in chemistry. What.

CHEMISTRY 2000 Topic #1: Bonding – What Holds Atoms Together? Spring 2010 Dr. Susan Lait.

Experience in a Microwave Spectroscopy Lab BRENDAN FRY ACKNOWLEDGMENTS: Dr. Stephen Kukolich Adam Daly Chandana Karunatilaka Space Grant Symposium April.

DELIVERING MICROWAVE SPECTROSCOPY TO THE MASSES: A DESIGN OF A LOW-COST MICROWAVE SPECTROMETER OPERATING IN THE GHZ FREQUENCY RANGE Amanda L. Steber.

Construction of a 480 MHz Chirped-Pulse Fourier-Transform Microwave Spectrometer: The Rotational Spectra of Divinyl Silane and 3,3-Difluoropentane Daniel.

ArXiv: Optical pulse-shaping for internal cooling of molecules Optical pulse-shaping for internal cooling of molecules Chien-Yu Lien, Scott Williams,

An Acoustic Demonstration Model for CW and Pulsed Spectroscopy Experiments Torben Starck, Heinrich Mäder Institut für Physikalische Chemie Christian-Albrechts-Universität.

Chirped Pulse Fourier Transform Microwave Spectroscopy of SnCl Garry S. Grubbs II and Stephen A. Cooke Department of Chemistry, University of North Texas,

A FABRY-PERÓT CAVITY PULSED FOURIER TRANSFORM W-BAND SPECTROMETER WITH A PULSED NOZZLE SOURCE. GARRY S. GRUBBS II, CHRISTOPHER T. DEWBERRY AND STEPHEN.

OSU – June – SGK1 STEVE KUKOLICH, ERIK MITCHELL ╬, SPENCER CAREY, MING SUN, AND BRYAN SARGUS, Dept. of Chemistry and Biochemistry, The University.

Galen Sedo, Jane Curtis, Kenneth R. Leopold Department of Chemistry, University of Minnesota The Dipole Moment of the Sulfuric Acid Monomer.

Laser Excitation and Fourier Transform Emission Spectroscopy of ScS R. S. Ram Department of Chemistry, University of Arizona, Tucson, AZ J. Gengler,

Chemical Reactions & Enzymes. I. Chemistry A. We already know that all living things are made up of chemical compounds. What are they again? Which give.

Sarah Newton University of Oregon Applied Physics.

Introduction to Chemistry. What did you do this summer? How Does this relate to Chemistry?

A New E-Band (60 – 90 GHz) Fourier Transform Millimeter-wave Spectrometer DeWayne T. Halfen and Lucy M. Ziurys Department of Chemistry Department of Astronomy.

Chaotic Robotics Callie Branyan Mechanical Engineering A Study of Analog Robots and their Nonlinear Behavior Arizona Space Grant Symposium April 18, 2015.

Electronic Transition of Ruthenium Monoxide Na Wang, Y. W. Ng and A. S.-C. Cheung Department of Chemistry The University of Hong Kong.

Design and Synthesis of Calixarene Scaffolds Bearing Hydrogen Bond Motifs Farzad Fani-Pakdel and Jason R. Telford Department of Chemistry, University of.

OSU RC10 Gas phase measurements and calculations of HCl and Ferrocene Adam Daly and Stephen Kukolich Chemistry Department University of Arizona.

Characterization of Laser Energy Deposition for Active Flow Control Clark Pederson University of Arizona Advisor: Dr. Jesse Little, Assistant Professor,

Elimination of the Vacuum Pump Requirement for High Resolution Rotational Spectroscopy Jennifer A. Holt Ryan Daly Christopher F. Neese Frank C. De Lucia.

June 18, rd International Symposium On Molecular Spectroscopy Gas-Phase Rotational Spectrum Of HZnCN (Χ 1 Σ + ) by Fourier Transform Microwave Techniques.

INTRODUCTION ~ PART 1 ~ Biomolecules. Chemistry of Life 1. Life requires about ____________naturally occurring chemical elements. A. _____________________________,

June 20, rd International Symposium On Molecular Spectroscopy Microwave Spectrum And Structure Determination Of the CCP ( X 2 П Ω ) Radical Ming.

First Principle Calculation of Nuclear Magnetic Resonance (NMR) chemical shift Kanchan Sonkar Center of Biomedical Magnetic Resonance SGPGIMS-Campus, Lucknow,

Fourier Transform Emission Spectroscopy of Some New Bands of ReN R. S. Ram Department of Chemistry, University of Arizona, Tucson, AZ and P. F. Bernath.

Extreme Ultraviolet Polarimetry Utilizing High-Order Harmonics Nicholas Herrick, Nicole Brimhall, Justin Peatross Brigham Young University.

The rod is continuously translated and rotated by a stepper motor Nd:YAG laser pulse vaporises the target rod Valve emits a helium pulse Fullerenes react.

The rod is continuously translated and rotated by a stepper motor Nd:YAG laser (532 nm, 3-5 ns, 5mj/pulse) vaporises the target rod by a single pulse/shot.

June 18, nd Symp. on Molec. Spectrosc. Activation of C-H Bonds: Pure Rotational Spectroscopy of HZnCH 3 ( 1 A 1 ) M. A. Flory A. J. Apponi and.

Extending the principles of the Flygare: Towards a FT-THz spectrometer Rogier Braakman Chemistry & Chemical Engineering California Institute of Technology.

Microwave Spectra of cis-1,3,5- Hexatriene and Its 13 C Isotopomers; An r s Substitution Structure for the Carbon Backbone Richard D. Suenram, Brooks H.

Fast Sweeping Double Resonance Microwave - (sub)Millimeter Spectrometer Based on Chirped Pulse Technology Brian Hays 1, Susanna Widicus Weaver 1, Steve.

Development of a Fluorescence Excitation Spectroscopy System Michael McDonnell ▪ Stephen Drucker Department of Chemistry ▪ University of Wisconsin – Eau.

Direct Observation of Rydberg–Rydberg Transitions in Calcium Atoms K. Kuyanov-Prozument, A.P. Colombo, Y. Zhou, G.B. Park, V.S. Petrović, and R.W. Field.

ACS - PRF1 MICROWAVE STRUCTURE MEASUREMENTS  Microwave spectroscopy measurements have yielded the first accurate gas- phase structural parameters for.

Digital Control System for Microwave Spectroscopy Data Collection Amanda Olmut Dr. Stephen Kukolich, Principle Investigator Dr. Adam Daly, Project Lead.

THE PURE ROTATIONAL SPECTRUM OF PERFLUOROOCTANONITRILE, C 7 F 15 CN, STUDIED USING CAVITY- AND CHIRPED-PULSED FOURIER TRANSFORM MICROWAVE SPECTROSCOPIES.

Fourier Transform Emission Spectroscopy of New Visible Systems of NbN R. S. Ram Department of Chemistry, University of Arizona, Tucson, AZ And P.

Probing Molecular Dynamics with Microwave Spectroscopy Adam Daly, Stephen G. Kukolich.

Chemical Reactions & Enzymes

A Chirped Pulse Fourier Transform Microwave (CP-FTMW) Spectrometer with Laser Ablation Source to Search for Actinide-Containing Molecules and Noble Metal.

STEPHEN G. KUKOLICH, MING SUN, ADAM M. DALY University of Arizona

Chemical Reactions & Enzymes

CHIRPED PULSE AND CAVITY FOURIER TRANSFORM MICROWAVE (CP-FTMW AND FTMW) INVESTIGATIONS INTO 3-BROMO-1,1,1,2,2-PENTAFLUOROPROPANE; A MOLECULE OF ATMOSPHERIC.

CHIRPED-PULSE FOURIER TRANSFORM MICROWAVE SPECTROSCOPY OF

Probing the Metal Activation of C-H Bonds Using High-Resolution Mid-infrared Laser Spectroscopy Timothy C. Steimle, Department of Chemistry and Biochemistry,

RH12, 70th International Symposium on Molecular Spectroscopy

Maintaining Microwave Spectrometer

Synthesis of Deuterocycloheptatrienyl-cyclopentadienyl-titanium

Fourier Transform Microwave Spectroscopy Of Sc13C2 and Sc12C13C: Establishing an Accurate Structure Of ScC2 (X2A1) ~ Sc C Mark A. Burton, DeWayne T. Halfen,

Modularity In Design for Microwave Spectroscopy Equipment

2.4 Chemical Reactions and Enzymes

Michal M. Serafin, Sean A. Peebles

THREE-PHASE INVERTERS

8.4 FOURIER SERIES ANALYSIS

Presentation transcript:

Kukolich Laboratory: Electronics, Inorganic Synthesis & Scientific Glassblowing Daniel A. Sánchez 04/17/10 NASA Space Grant: University of Arizona Chemistry Department

Project Overview 3 Projects Project #1 Part 1: Motor Circuit Part 2: Pulse Box Project #2- Synthesis of Trochrocene Project #3 Scientific Glassblowing

Microwave Spectroscopy Microwave Spectroscopy studies the structure of organic and inorganic compounds. Why is this important? Determines bond lengths and angles and model interactions.

Studied Complexes

Pulsed-Beam Fourier Transform Microwave Spectrometer Microwave Cavity Diffusion Pump Torr Fore pump

t=0 General Valve SCR Molecules in Ne +300V Pico Digital Oscilloscope HP 8673 Microwave Generator Pulse Sequence

+300V t~1ms HP 8673 Microwave Generator High Speed Microwave Switch Pico Digital Oscilloscope

+300V t`=1ms+10  s Mixer FID HP 8673 Microwave Generator Pico Digital Oscilloscope

Project #1: Part 1: Motor Control Circuit Objective –To control a DC motor at 12V/1Amp that will run at variable speeds, manually, or by computer. –Control of mirror movement –Using the NAND,555, One Shot, and Inverter

Final Design of Control Circuit When manual is in use computer is locked out and vice versa

Project #1: Part 1: Success! Project #1 Part 1 was a success and currently moves mirrors within the new spectrometer

Project #1: Part 2: Pulse Box construction for Spectrometer #3 Objective –To build a pulse box that could generate a sequences of pulses.

Circuit Design

Project #1: Part 2: Success TheoreticalExperimental

Project #2: Synthesis of Trochrocene Braunschweig, Holger; Kupfer, Thomas; Lutz, Matthias; Radacki, Krzysztof. Ansa [1]Trochrocenophanes and Their Related Unstrained 1,1'-Disubstituted Counterparts: Synthesis and Electronic Structure. Journal of the American Chemical Society (2007), 129(28),

Glassware Project: Cold Finger

Glassware Project: Sample Cell and Mixing System Neon Gas enters Sample Sample + Neon Gas exits Sample + Neon Gas enters Samples + Neon Gas exits Mixing occurs Neon Enters Sample

Acknowledgments Dr. Kukolich Adam Daly Laszlo Sarkozy Catherine Lavin NASA Space Program Susan Brew