1 LAPPD Team meeting 6/10/2010 Ossy Siegmund, Experimental Astrophysics Group, Space Sciences Laboratory, U. California at Berkeley Bialkali Photocathode Development GALEX M31

2 LAPPD Team meeting 6/10/2010 LAPD Photocathode Milestones Systematic characterization of Photo-electron Emission (PE) properties of materials for photocathode development. Demonstration of an operational 8”-square photo-cathode with a viable path to QE ≥ 15% for wavelengths between 300 and 450 nm. Associated Milestones - Dependencies:- Demonstration of the window-to-body seal solution. Design and costing of the vacuum-transfer/assembly facility for the 8”-square MCP module.

3 LAPPD Team meeting 6/10/2010 Cathode Bandpass and Windows Acceptable cutoff range Typical window transmission curves Nominal Cherenkov emission spectrum compared with bialkali

4 LAPPD Team meeting 6/10/2010 6* 10 9 Ohm/square 2*10 6 Ohm/square Bi-Alkali Cathode Characteristics QE and resistivity for various bialkalis we will use K 2 CsSb & Na 2 KSb Lyashenko, Chicago 7/09 Cathode Noise vs Temp

5 LAPPD Team meeting 6/10/2010 Photocathode Configuration Numerous processes affect the QE Bialkali is a few 100Å thick, and is compatible with deposition as semitransparent on the window, but is very difficult to achieve as an opaque cathode on the MCP surface.

6 LAPPD Team meeting 6/10/2010 Work Flow Program for Bialkali Cathode Development

7 LAPPD Team meeting 6/10/2010 Bialkali Photocathode QE Examples of SSL bialkali photocathode depositions with different wavelength optimizations (on fiber optics). Peak QEs 15% to 20% using Na 2 KSb. High efficiency Bialkali cathodes at Photonis. Clear room for improvement over standard bialkalis. Need to Establish enhancement techniques. Schyns, Clermont 2010

8 LAPPD Team meeting 6/10/2010 B33/B270 General Parameters B33 Composition Refractive B Air~1.0 Water~1.32 The cathode substrate, window or window coating, affects the photocathode performance. Quartz, fiber optics, 7056 glass are common. Borofloat B33 Borosilicate is not, and also has Tin diffused into one side from the float process, so we we need to test this. B270 is a soda-lime Crown glass and should be OK. Standard AR coating is bad for LAPD - most likely don’t need AR coating for water/B33 interface

9 LAPPD Team meeting 6/10/2010 Compatibility and Transmittance of Windows B33 Transmittance is typical for borosilicate glasses B270 Transmittance is only slightly worse than B33 Both materials have similar mechanical properties, strength, hardness, etc, BUT the thermal coeff’ts are not, 0.003”/100C for B33 and 0.008”/100C for B270 - not clear that this is an issue x /K 8.8 x /K Thermal

10 LAPPD Team meeting 6/10/2010 Conductive Layer Properties for Windows Braem, NIMA 2003 ITO is a possibility for the conductive underlayer, BUT - it might affect the cathode QE! So we can also try metal conductor stripes as we did for GALEX.

11 LAPPD Team meeting 6/10/2010 Small Tube and Cathode Process Tank System Small window cathode development, 33mm samples - Process samples to optimize QE and bandpass -Na 2 KSb, K 2 CsSb cathodes - Use several substrate materials, SiO 2, verify B33/B270 - Test precursor/ITO/conductor underlayer for cathodes Large size window cathode study, 8” windows. - Study source alkali design for large cathodes - Develop techniques to make larger area uniform QE - Optimize cathode QE levels - Test metal/ITO conductor underlayer for cathodes - Test metalization and sealing techniques

12 LAPPD Team meeting 6/10/ mm Cathode Test Samples We have cut up one B33 and one B270 window to make 30ea 1.3” test samples each, also have 18ea fused silica as control samples. Inconel annular electrodes were evaporated just as they would be for In seals

13 LAPPD Team meeting 6/10/ Tube Lab, 33mm sample test/process station. Small tank used to process alkali cathodes (33mm) and tubes of small area. Can take 4 samples/run. 1st run done, making mods for 2nd run. - Small sample test runs - Substrate material tests

14 LAPPD Team meeting 6/10/2010 Initial Bialkali Trials on 33mm Sample Substrates Trying to set up process parameters for comparative tests and optimizations. Used quartz, B33 and B270 sequential depositions in one pumpdown. Short process / thin cathode -ended up too blue / low QE. -Had problems with K channels that precluded optimal process, mostly on later depositions. Initial cathode trials, Process order Plan for next run -Fix alkali dispensers, retool window holders -shoot all substrates in one go at same time -Add extra cycles to push peak redder-higher QE

15 LAPPD Team meeting 6/10/2010 Cathode Process Test Tank System replacement for 33mm chamber Larger 16” flange tank, can take full size windows (8.7”) to test -Quantum efficiency -QE Uniformity -Seal tests

16 LAPPD Team meeting 6/10/2010 Evaporator design modifications to accommodate 8.7” windows Design done for NiCr/Cu evaporation tooling for 8.7” windows Currently OK to 5” Rotation stage for 8.7” windows

17 LAPPD Team meeting 6/10/2010 Window Seal Development and Cathode Test “Diodes” 3” window test article on metal frame with Indium seal Will metalize 8.7”window and produce an Indium seal on a frame to test leak tightness of the seal. 3” ceramic body with strip anode, and metal frame with Indium seal

18 LAPPD Team meeting 6/10/2010 8” Tube and Cathode Process Tank System UHV 18” process Chamber:- Initial use for cathode and seal development. Eventually use for complete tube process task. B33/B ” windows - large area cathodes - uniformity tests - QE optimization

19 LAPPD Team meeting 6/10/2010 8” Tube and Cathode Process Tank System Large window cathode development, 8.66” square - Implement alkali source design for large cathode areas - Develop wet cleaning and plasma cleaning processes - Establish metalization scheme - Test metal/ITO conductor underlayer for 8” cathodes - Implement AR coatings/treatment on both surfaces - Develop techniques to make 8” area uniform QE - Optimize cathode QE levels - Trial seals on 8.66” “frames” - Then - Make LAPD 8” tubes