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Soil Science Department of Soil Science and Soil Protection Martin Kočárek: office no. 225, kocarek@af.czu.cz Practicals / Seminars Introduction. Semestral.

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Presentation on theme: "Soil Science Department of Soil Science and Soil Protection Martin Kočárek: office no. 225, kocarek@af.czu.cz Practicals / Seminars Introduction. Semestral."— Presentation transcript:

1 Soil Science Department of Soil Science and Soil Protection Martin Kočárek: office no. 225, Practicals / Seminars Introduction. Semestral work setting. Morphological features of soil horizons. Soil profiles description. Soil texture analysis: presentation of principles and methodology. Soil texture analysis: sample preparation, measurement  Soil organic matter content determination.  Soil reaction. Explanation of principles. Determination of pHH2O, pHKCl, exchangeable acidity.  Soil sorption characteristics: explanation of principles; determination of C.E.C. by Bower method.  Soil sorption characteristics: determination of hydrolytic acidity; calculation of base saturation.  Soil salinity: principles of determination; measurement of electrical conductivity soil alcohol extracts.  Presentation of advanced methods of soil analysis  Soil maps, soil information systems   Presentation of students' semestral work  Discussion of major problems of soil degradation in Europe and in the World: case studies. Credit. 

2 Protocols Soil texture analysis
Soil organic matter content determination.  Soil reaction. Determination of pHH2O, pHKCl, exchangeable acidity Soil sorption characteristics: determination of C.E.C. by Bower method, determination of hydrolytic acidity; calculation of sum of base cation and base saturation.  Soil salinity Summarization of protocols (students' semestral work)

3 Requirements for credit
Protocols Presentation of students' semestral work Presence at the practicals 80 %

4 Semestral work setting.
You will work in pairs At the beginning of the semester you will be given a soil sample from soil units which are localized close to Suchdol Each practical lesson you will determine some soil property (mentioned above) of your sample. For each soil property you will complete a protocol At the end of the semester you will summarize the results about your samples and samples of your colleagues (to describe the whole soil profile of the soil unit) in a semestral work which you will present in the last lesson

5 Morphology of Soil Profile - Horizon
Colour Structure Texture Coarse Fragment Content Humidity Consistence Concretions Redoximorphic Features and other New formations Carbonates and soluble salt content Porosity and cracks Rooting and a biological activation Width and Topography of horizon boundary

6 Width of Soil Horizon Boundary
ABRUPT (0-2cm) CLEAR (2-5cm)

7 Width of Soil Horizon Boundary
GRADUAL (5-15 cm) DIFFUSE (>15 cm)

8 Topography of Soil Horizon Boundary
Smooth Oblique Wavy Irregular Broken pockets are wider than depths pockets are deeper than width horizon is not continuous

9 Soil Horizon Boundary Wavy Oblique

10 Soil Horizon Boundary Smooth Irregular

11 Soil Colour Subjective description e.g. „ light brown, dark gray“
Objective description – Munsell colour system e.g. „7,5YR 4/6“

12 5YR 4/6 Hue = Basic color R – red Y – yellow G – green B – blue
RP R – red Y – yellow G – green B – blue P - purple Y P GY 5YR 4/6 PB G B BG Chroma = intensity level hue 5 yellow red value 4 chroma 6 Value = tint (admixture of gray)

13 Chroma refers to the relative purity or strength of the spectral color
Chroma refers to the relative purity or strength of the spectral color. Chroma runs from 0 (neutral gray) to 8 (highest strength of color found in soils). Chroma increases to the right across the Munsell page. All chips in a column have equal chroma. Zero-chroma chips have no color, they are neutral gray. Often they are simply given a hue designation N (neutral).

14 Value refers to the amount of light reflected from the chip
Value refers to the amount of light reflected from the chip. On a neutral gray scale, a value of 10 indicates pure white, and value of 0 indicates pure black. Value runs north-south (Vertical) on the Munsell page. All chips in a row have equal value.

15 VALUE CHROMA

16 Soil Colour

17 Soil Structure natural organization of soil particles into discrete soil units (aggregates or peds) Structureless - Single grain Structureless – Massive coherent mass Structural (soil aggregates)

18 Structure types according to shape
STRUCTURAL ELEMENTS equally developed vertically elongated Horizontally elongated prism-like spheroidal angular platy upper part without rounding Rounded tops granual angular blocky subangular blocky columnar prismatic

19 Soil Structure

20 Soil Structure A-horizon E-horizon

21 Soil Structure B-horizon B-horizon

22 Soil Structure

23 Soil Structure B-horizon Bt-horizon

24 Structure types according to shape
1 - Granual 2 - Angular 3a - Prismatic 4 - Platy 3b - Columnar

25 Structure

26 Soil Texture 20 % Sand 30 % Silt 50 % Clay Sand + Silt + Clay = 100%
Texture = Clay 20 % Sand 30 % Silt 50 % Clay

27 Soil Texture Classes

28 Coarse surface fragments

29 Humidity - Dry Moist Wet

30 Consistence

31 Consistence Stickiness – moist soil

32 Consistence Plasticity – moist soil

33 Concretions – Cutanic Features
features of clay iluviation (e.g.: clay coatings on the structure elements – peds)

34 Concretions – Cutanic Features
vertic features – wedge-like peds

35 Concretions – Cutanic Features
vertic features –cracks

36 Concretions – Cutanic Features
vertic features –slickensides

37 Concretions – Cutanic Features
Ortstein features (in Podzols) kvádrový pískovec štěrkopísek

38 Concretions – Cutanic Features
Gleyic features – rusty coatings

39 Concretions – Cutanic Features
Gleyic features – rusty coatings

40 Concretions – Cutanic Features
mottling

41 Concretions – Cutanic Features

42 Concretions – Cutanic Features
Fe - Mn concretions – nodules

43 Concretions – Cutanic Features
CaCO3 accumulation pseudomycelias Hard hollow concretions

44 Concretions – Cutanic Features
biological activity – Crotovinas

45 Concretions – Cutanic Features
biological activity - earthworm coprolites

46 Roots Size (diameters) Abundance Depth

47 Carbonates reaction with10% HCl depth
content (intensity of effervescence) forms of secondary carbonates

48 Carbonates reaction with10% HCl depth content (intenzita šumění)
forms of secondary carbonates reaction with10% HCl depth content (intenzita šumění)

49 Hydrometric method Measuring cylinder and hydrometer calibration
KPG Katedra pedologie a geologie Hydrometric method Measuring cylinder and hydrometer calibration For correction of hydrometer weight base volume Scale markings 1,030 Weighted base

50 Hydrometric method Measuring cylinder and hydrometer calibration 1,000
KPG Katedra pedologie a geologie Hydrometric method Measuring cylinder and hydrometer calibration 1,000 hR = h1 + h0/2 ∆h = h – h0 ∆h = V/F V/F = h – h0 h0 = h – V/F h0/2 = h/2 – V/2F hR = h1 + h/2 – V/2F h1 = L – R.L/S S – the number of units on the scale (30) h1 = L/S (S – R) L R 1,019 h1 h1 1,030 ∆h hR h0 h F ∆h V

51 Hydrometric method S The number of units on the scale (30)
KPG Katedra pedologie a geologie Hydrometric method S The number of units on the scale (30) R Hydrometer reading (1,019; CORRECTION 19!!!!!) L Scale lenght (cm) h/2 Half height of weighted base (cm) V Volume of weighted base (cm3) F Area of measuring cylinder base (cm2)

52 Hydrometric method Sample preparation
KPG Katedra pedologie a geologie Hydrometric method Sample preparation To break soil aggregates to single (elementary) grains Can by done by mechanical way, chemical way or combination of both Methodology of sample preparation: Soil weight: 80 – 100 g Light soil 40 – 60 g Intermediate soil 20 – 40 g Heavy soil Place soil sample into the boiling cup and mix it with distillate water and dispersing agent (Na3(PO4)6) by ratio 1g : 1ml : 1ml Boil the soil suspension for 3 min. and move it quantitatively into measuring cylinder

53 Hydrometric method Methodology of soil texture analyses
KPG Katedra pedologie a geologie Hydrometric method Methodology of soil texture analyses Move the soil suspension into measuring cylinder and fill the measuring cylinder to the mark of 1000 ml Stir the soil suspension in measuring cylinder violently Put hydrometer into measuring cylinder and read the values in defined times (see below) Measure the soil suspension temperature after every hydrometer reading

54 Hydrometric method Methodology of soil texture analyses Time
KPG Katedra pedologie a geologie Hydrometric method Methodology of soil texture analyses Time Temperature R R0 hR d Σ% 30´´ T1 1,029 26 23 19 10´ T2 14 20´ T3 13 30´ T4 12 40´ T5 11 50´ T6 60´ T7 Leave the hydrometer in soil suspension Remove the hydrometr afther every reading and clean it

55 Hydrometric method Methodology of soil texture analyses Time Temp. R
KPG Katedra pedologie a geologie Hydrometric method Methodology of soil texture analyses Time Temp. R R0 hR d (mm) Σ% 30´´ T1 29 26 23 19 10´ T2 14 20´ T3 13 30´ T4 12 40´ T5 11 50´ T6 60´ T7

56 °C 20 21 22 23 24 25 Correction 0 + 0,5 + 0,36

57 Hydrometric method Methodology of soil texture analyses Time Temp. R
KPG Katedra pedologie a geologie Hydrometric method Methodology of soil texture analyses Time Temp. R R0 hR d (mm) Σ% 30´´ T1 29 26 23 19 10´ T2 14 20´ T3 13 30´ T4 12 40´ T5 11 50´ T6 60´ T7 R + correction

58 Hydrometric method Methodology of soil texture analyses Time Temp. R
KPG Katedra pedologie a geologie Hydrometric method Methodology of soil texture analyses Time Temp. R R0 hR d (mm) Σ% 30´´ T1 29 26 23 19 10´ T2 14 20´ T3 13 30´ T4 12 40´ T5 11 50´ T6 60´ T7

59 Hydrometric method Methodology of soil texture analyses Time Temp. R
KPG Katedra pedologie a geologie Hydrometric method Methodology of soil texture analyses Time Temp. R R0 hR d (mm) Σ% 30´´ T1 29 26 23 19 10´ T2 14 20´ T3 13 30´ T4 12 40´ T5 11 50´ T6 60´ T7

60 d v Time ρZ A T Nomogram for Particle Size Determination ρz hours
dynamic viscosity of liquids [g.cm-1.s-1] particle density [g.cm-3] specific gravity of liquid [g.cm-3] sedimentation rate [cm.s-1] particle diameters [mm] suspension temperature [OC] Depth [cm] time Nomogram for Particle Size Determination Temperaure correction ( t ) Key for particle size determination hours seconds minutes (Casagrande A., Modified) ρz d v Time ρZ A T

61 Hydrometric method Methodology of soil texture analyses Time Temp. R
KPG Katedra pedologie a geologie Hydrometric method Methodology of soil texture analyses Time Temp. R R0 hR d (mm) Σ% 30´´ T1 29 26 23 19 10´ T2 14 20´ T3 13 30´ T4 12 40´ T5 11 50´ T6 60´ T7 Σ% = 100/g * (ρZ.R0 / ρZ-1) g......Soil weight used for analyses

62 PARTICLE SIZE CURVE Grevel Sand Silt Clay Particle size diameters [mm]
Percentage of particle size Grevel Sand Silt Clay Clay % 11 Silt % 26 Sand % 63 PARTICLE SIZE CURVE 2 mm 0.063 mm 0.002 mm

63 Soil Texture by Feel Analyses

64 PARTICLE SIZE CURVE Grevel Sand Silt Clay 2 mm 0.063 mm 0.002 mm
Percentage of particle size Particle size diameters [mm]

65 Nomogram for Particle Size Determination
dynamic viscosity of liquids [g.cm-1.s-1] particle density [g.cm-3] specific gravity of liquid [g.cm-3] sedimentation rate [cm.s-1] particle diameters [mm] suspension temperature [OC] Depth [cm] time Nomogram for Particle Size Determination Temperaure correction ( t ) Key for particle size determination hours seconds minutes (Casagrande A., Modified) ρz


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