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Advanced LIGO Photodiodes ______
David Jackrel*, Zhilong Rao, James S. Harris *Dept. of Materials Science and Engineering Dept. of Electrical Engineering LSC Meeting – LHO August 19th, 2004 LIGO-G Z
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Optoelectronic Device Results
Outline Introduction AdLIGO Photodiode Specifications Device Materials & Structures Optoelectronic Device Results I-V Character Quantum Efficiency AdLIGO Devices
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Advanced LIGO Schematic
Auxiliary Length Sensing Power Stabilization
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Photodiode Specifications
LIGO I Advanced LIGO Detector Bank of 6PDs Power Stabilization Aux. Length (RF) Detection GW Channel Steady-State “Power” 0.6 W ~ 300 mA 10 – 100 mW 30 mW Operating Frequency ~29 MHz 100 kHz 200 MHz Quantum Efficiency 80% > 80% 90% (300mA)/(0.868A/W * 0.90 QE) = 385mW Resonating Tank Circuit Trades w/ Sensitivity
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GaInNAs vs. InGaAs GaInNAs 25% InGaAs 53% InGaAs 1064nm light 1.13eV
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Rear-Illuminated PD Advantages
High Power Linear Response High Speed Conventional PD Adv. LIGO Rear-Illuminated PD
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Quantum Efficiency – Thick Sub.
Ext. Efficiency Bias (Volts) Optical Power (mW)
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‘Thick’ and ‘Thinned’ Structures
0.) Thick Substrate – Mounted w/ Conducting Epoxy 1.) Epoxy (or BCB) Underfill – Mounted w/ Flip-Chip Bonder 2.) Photoresist Underfill – Mounted w/ Flip-Chip Bonder 3.) Photoresist Encapsulant – Mounted w/ Conducting Epoxy
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Dark Current: Various Encapsulants
Large Variation Between Devices Test Structures, Not the Best Starting Material… Epoxy Underfill Photoresist Underfill Photoresist Encapsulant BCB Underfill
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Thinned Device Quantum Efficiency
~ 85% ~ 60%
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AdLIGO Devices Detector Power Stabilization RF Detection GW Channel
Diameter 3 - 5 mm 1.5 mm 1 mm (or larger?) Steady-State Power 400 mW 100 mW 50 mW 3-dB 1/RC Bandwidth 1 - 3 MHz 30 MHz ( 180 MHz) 60 MHz Quantum Efficiency > 80 % > 90 % Damage Threshold ? Important?!
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AdLIGO Devices: Commercial Vendors
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MBE Crystal Growth Effusion cells for In, Ga, Al Cracking cell for As
N Plasma Source Effusion cells for In, Ga, Al Cracking cell for As Abrupt interfaces Chamber is under UHV conditions to avoid incorporating contaminants RHEED can be used to analyze crystal growth in situ due to UHV environment T= C Atomic source of nitrogen needed Plasma Source!
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InGaAs vs. GaInNAs PD Designs
2 m GaInNAs lattice-matched to GaAs!
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Full Structure Simulated by ATLAS
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Heterojunction Band Gap Diagram
InAlAs and GaAs transparent at 1.064m Absorption occurs in I-region (in E-field ) p- i- n- N-layer: In.25Al.75As or GaAs Eg2= eV I-layer: In.25Ga.75As, or Ga.88In.12N.01As.99 Eg1=1.1eV P-layer: In.25Al.75As or GaAs Eg2= eV
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Fabrication Procedure
1. P-Contact Lift-Off Process 2. Mesa Etch H2SO4:H2O2:H2O (1:1:20) Etch Rate ~ 0.75 micron/min 3. Au on Heat Sink Lift-Off Process 4. In Bumps Lift-Off Process ~3um In Au GaAs Substrate PIN Epi- Layers AlN Heat Sink In Bumps PR Encapsulant AR Coating Epoxy
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Standard Epoxy Procedure
Now you can’t pattern the top contact (or the ARC) w/ standard processing... But, shadow masks might work... 5. Flip-Chip Bond & Under-fill w/ Epoxy Low viscosity – Fills all of the voids Makes chip mechanically stable 6. Thin GaAs Substrate Piranha - H2SO4:H2O2:H2O (1:8:1) Doesn’t affect epoxy!
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Shadow Masking
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Photoresist Underfill Technique
5. Flip-Chip Bond 1 g / 100 sq. micron, 140˚C 6A. Apply Photoresist SPR 3612 Positive PR 6B. Blanket Exposure Long exposure, Hard Bake 240˚C
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Photoresist Underfill Technique (2)
7. Thin GaAs Substrate Piranha - H2SO4:H2O2:H2O (1:8:1) Etch Rate ~10 microns / min 8. N-Contact Lift-off Process 9. Evaporate AR Coating Etch Process (SiNx, HfO, …depends where done)
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Dimensions 6-18 mm 500um 1-4 mm 4-5um 1-2um 3000A ~25 mm
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Dark Current: Various Encapsulants
Epoxy Underfill Photoresist Underfill Photoresist Encapsulant BCB Underfill
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Free-Carrier Absorption
S-I
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Free-Carrier Absorption
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Free-Carrier Absorption
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Free-Carrier Absorption
A = 1 – exp(-tsub•fc) , fc = Nd * 3e-18
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Thinned Device Photocurrent
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Thinned Device QE
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Surface Passivation Results (2)
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(NH4)2S+ Surface States GaAs(111)A GaAs(111)B (Green and Spicer, 1993)
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Surface Passivation Results
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Large InGaAs Devices, –20V Bias
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InGaAs vs. GaInNAs Dark Current
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InGaAs vs. GaInNAs Dark Current
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GaInNAs Dark Current
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InGaAs Dark Current
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GaInNAs H2SO4 vs. (NH4)2S+
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GaInNAs H2SO4 vs. (NH4)2S+
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Theoretical Saturation Powers
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Theoretical Saturation Powers
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RC-Circuit Bode Plot 3-dB 30MHz
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RC- and LCR- Transmittance
RC-Circuit LCR-Circuit
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LCR- Circuit Impedance
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