Presentation is loading. Please wait.

Presentation is loading. Please wait.

Optimization of an analytical method for detecting paraphenylenediamine (PPD) by GC/MS-iontrap in biological liquids  A. Stambouli, M.A. Bellimam, N.

Published byAndrew Washington Modified over 6 years ago

Similar presentations

Presentation on theme: "Optimization of an analytical method for detecting paraphenylenediamine (PPD) by GC/MS-iontrap in biological liquids  A. Stambouli, M.A. Bellimam, N."— Presentation transcript:

1 Optimization of an analytical method for detecting paraphenylenediamine (PPD) by GC/MS-iontrap in biological liquids  A. Stambouli, M.A. Bellimam, N. El Karni, T. Bouayoun, A. El Bouri  Forensic Science International  Volume 146, Pages S87-S92 (December 2004) DOI: /j.forsciint Copyright © 2004 Elsevier Ireland Ltd Terms and Conditions

2 Fig. 1 PPD derivatizated with iodomethane.
Forensic Science International  , S87-S92DOI: ( /j.forsciint ) Copyright © 2004 Elsevier Ireland Ltd Terms and Conditions

3 Fig. 2 PPD derivatizated with TFA.
Forensic Science International  , S87-S92DOI: ( /j.forsciint ) Copyright © 2004 Elsevier Ireland Ltd Terms and Conditions

4 Fig. 3 Analysis of crude product.
Forensic Science International  , S87-S92DOI: ( /j.forsciint ) Copyright © 2004 Elsevier Ireland Ltd Terms and Conditions

5 Fig. 4 Calibration curve of PPD using benzidine as internal standard.
Forensic Science International  , S87-S92DOI: ( /j.forsciint ) Copyright © 2004 Elsevier Ireland Ltd Terms and Conditions

6 Fig. 5 GC/MS chromatogram obtained from a blank urine contamined by PPD with benzidine as internal standard. Forensic Science International  , S87-S92DOI: ( /j.forsciint ) Copyright © 2004 Elsevier Ireland Ltd Terms and Conditions

7 Fig. 6 Chromatogrm GC/MS after reconstituting ion 300 from gastric content. Forensic Science International  , S87-S92DOI: ( /j.forsciint ) Copyright © 2004 Elsevier Ireland Ltd Terms and Conditions

8 Fig. 7 Chromatogram GC/MS of urine extract after reconstituting ions 300 and 376. Forensic Science International  , S87-S92DOI: ( /j.forsciint ) Copyright © 2004 Elsevier Ireland Ltd Terms and Conditions

Download ppt "Optimization of an analytical method for detecting paraphenylenediamine (PPD) by GC/MS-iontrap in biological liquids  A. Stambouli, M.A. Bellimam, N."

Similar presentations

The most efficient STR loci in forensic genetics in population of central Poland R. Jacewicz, M. Jedrzejczyk, J. Berent Forensic Science International:

The most efficient STR loci in forensic genetics in population of central Poland R. Jacewicz, M. Jedrzejczyk, J. Berent Forensic Science International:
Analysis of deteriorated rubber-based pressure sensitive adhesive by pyrolysis-gas chromatography/mass spectrometry and attenuated total reflectance Fourier.

Analysis of deteriorated rubber-based pressure sensitive adhesive by pyrolysis-gas chromatography/mass spectrometry and attenuated total reflectance Fourier.
The importance of Guthrie cards and other medical samples for the direct matching of disaster victims using DNA profiling  D. Hartman, L. Benton, L. Morenos,

The importance of Guthrie cards and other medical samples for the direct matching of disaster victims using DNA profiling  D. Hartman, L. Benton, L. Morenos,
Right heart ischemia in cases of sepsis

Right heart ischemia in cases of sepsis
Headspace-GC/MS detection of TATP traces in post-explosion debris

Headspace-GC/MS detection of TATP traces in post-explosion debris
Cyanide quantification in post-mortem biological matrices by headspace GC–MS  Brigitte Desharnais, Geneviève Huppé, Martine Lamarche, Pascal Mireault,

Cyanide quantification in post-mortem biological matrices by headspace GC–MS  Brigitte Desharnais, Geneviève Huppé, Martine Lamarche, Pascal Mireault,
Buprenorphine and major metabolites in blood specimens collected for drug analysis in law enforcement purposes  Stephanie Oechsler, Gisela Skopp  Forensic.

Buprenorphine and major metabolites in blood specimens collected for drug analysis in law enforcement purposes  Stephanie Oechsler, Gisela Skopp  Forensic.
The ideal subject distance for passport pictures

The ideal subject distance for passport pictures
Volatile organic compounds in polyethylene bags⿿A forensic perspective

Volatile organic compounds in polyethylene bags⿿A forensic perspective
Real time quantitative colourimetric test for methamphetamine detection using digital and mobile phone technology  Aree Choodum, Kaewalee Parabun, Nantikan.

Real time quantitative colourimetric test for methamphetamine detection using digital and mobile phone technology  Aree Choodum, Kaewalee Parabun, Nantikan.
Fast LC–MS/MS method for the determination of amphetamine, methamphetamine, MDA, MDMA, MDEA, MBDB and PMA in urine  Marta Concheiro, Susana Maria dos.

Fast LC–MS/MS method for the determination of amphetamine, methamphetamine, MDA, MDMA, MDEA, MBDB and PMA in urine  Marta Concheiro, Susana Maria dos.
High-performance combination method of electric network frequency and phase for audio forgery detection in battery-powered devices  Maryam Savari, Ainuddin.

High-performance combination method of electric network frequency and phase for audio forgery detection in battery-powered devices  Maryam Savari, Ainuddin.
The effect of sodium fluoride on the stability of cyanide in postmortem blood samples from fire victims  J.L. McAllister, R.J. Roby, Barry Levine, David.

The effect of sodium fluoride on the stability of cyanide in postmortem blood samples from fire victims  J.L. McAllister, R.J. Roby, Barry Levine, David.
Ethanol production by Candida albicans in postmortem human blood samples: Effects of blood glucose level and dilution  Daisuke Yajima, Hisako Motani,

Ethanol production by Candida albicans in postmortem human blood samples: Effects of blood glucose level and dilution  Daisuke Yajima, Hisako Motani,
Piotr Adamowicz, Dariusz Zuba, Karolina Sekuła 

Piotr Adamowicz, Dariusz Zuba, Karolina Sekuła 
Előd Hidvégi, Péter Fábián, Zsuzsa Hideg, Gábor Somogyi 

Előd Hidvégi, Péter Fábián, Zsuzsa Hideg, Gábor Somogyi 
A snapshot on NPS in Italy: Distribution of drugs in seized materials analysed in an Italian forensic laboratory in the period 2013–2015  Sara Odoardi,

A snapshot on NPS in Italy: Distribution of drugs in seized materials analysed in an Italian forensic laboratory in the period 2013–2015  Sara Odoardi,
A snapshot on NPS in Italy: Distribution of drugs in seized materials analysed in an Italian forensic laboratory in the period 2013–2015  Sara Odoardi,

A snapshot on NPS in Italy: Distribution of drugs in seized materials analysed in an Italian forensic laboratory in the period 2013–2015  Sara Odoardi,
Determination of ketamine and norketamine in hair by micropulverized extraction and liquid chromatography–high resolution mass spectrometry  Donata Favretto,

Determination of ketamine and norketamine in hair by micropulverized extraction and liquid chromatography–high resolution mass spectrometry  Donata Favretto,
Simultaneous determination of mushroom toxins α-amanitin, β-amanitin and muscarine in human urine by solid-phase extraction and ultra-high-performance.

Simultaneous determination of mushroom toxins α-amanitin, β-amanitin and muscarine in human urine by solid-phase extraction and ultra-high-performance.

Similar presentations

Ads by Google