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X-Ray Facility Overview [BCH 4053]

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Presentation on theme: "X-Ray Facility Overview [BCH 4053]"— Presentation transcript:

1 X-Ray Facility Overview [BCH 4053]
IMB X-Ray Facility Kasha Laboratory This version was made for BCH 4053 under-graduate student lab tour conducted on Monday March 26 and Tuesday March 27, 2007 March 26 & 27, 2007 © Thayumanasamy Somasundaram

2 ©2002-2007 Thayumanasamy Somasundaram
IMB X-Ray Facility Inter-disciplinary Institute Structural Biology Program Core Facility [Estd: 1993] No charge for use Open Access What XRF can do for you? March 26 & 27, 2007 © Thayumanasamy Somasundaram

3 What XRF Can Do For You? Crystal Diffraction XRF can help you in Steps
Images courtesy of Michael Chapman Lab Crystal Diffraction XRF can help you in Steps What XRF can do for you? E Density Structure March 26 & 27, 2007 © Thayumanasamy Somasundaram

4 ©2002-2007 Thayumanasamy Somasundaram
X-Ray Generators Rigaku RU-H2R Cu Rotating Anode Single Wavelength Brilliant Beam General information about x-ray generators. March 26 & 27, 2007 © Thayumanasamy Somasundaram

5 ©2002-2007 Thayumanasamy Somasundaram
X-Ray Detector 1 Imaging Plate (IP) Rigaku R-Axis IIc Two 19cm2 IPs 8 minute Read-out Variable Distance Specific details of R-Axis IIc IP detector. March 26 & 27, 2007 © Thayumanasamy Somasundaram

6 ©2002-2007 Thayumanasamy Somasundaram
X-Ray Detector-2 Charge Coupled Device MarCCD165 Single CCD 3s Read-out Variable Distance Specific details about MarCCD165 detector. March 26 & 27, 2007 © Thayumanasamy Somasundaram

7 ©2002-2007 Thayumanasamy Somasundaram
X-Ray Detector-3 Multiwire Xentronics X-1000 Gas-filled Accurate X-Ray Scattering Specific details about MarCCD165 detector. March 26 & 27, 2007 © Thayumanasamy Somasundaram

8 X-Ray Monochromatization
Multi-layer Mirrors Osmic Confocal Wavelength Purity High Flux General and specific details about multilayer mirrors. March 26 & 27, 2007 © Thayumanasamy Somasundaram

9 ©2002-2007 Thayumanasamy Somasundaram
X-Ray Data Collection Cryo Coolers Oxford CryoSystem Now at 100°K Before at RT To Protect Crystals March 26 & 27, 2007 © Thayumanasamy Somasundaram

10 ©2002-2007 Thayumanasamy Somasundaram
X-Ray Data Control Linux/Windows MarCCD/CrystalClear GUI Automated Analog»Digital March 26 & 27, 2007 © Thayumanasamy Somasundaram

11 ©2002-2007 Thayumanasamy Somasundaram
Accessories Computers Software Cryo Hardware List of typical accessories at XRF. March 26 & 27, 2007 © Thayumanasamy Somasundaram

12 ©2002-2007 Thayumanasamy Somasundaram
Amenities Crystal Room Cold Room Variable T Incubator Digital Imaging Synchrotron Time Software Licenses Details of general amenities of XRF. Coldroom March 26 & 27, 2007 © Thayumanasamy Somasundaram

13 ©2002-2007 Thayumanasamy Somasundaram
Crystal Services Crystal Screening Crystallization Data Collection Collection Strategy Crystal Storage Crystal Transport Synchrotron Help Details of XRF services. March 26 & 27, 2007 © Thayumanasamy Somasundaram

14 ©2002-2007 Thayumanasamy Somasundaram
Data Services Data Processing Data Visualization Data Interpretation Data Archives Data Storage Data Extraction Description of XRF services. March 26 & 27, 2007 © Thayumanasamy Somasundaram

15 XRF-Contact Thayumanasamy “Soma”sundaram
414 Institute of Molecular Biophysics Florida State University Tallahassee, FL Phone: | Fax: Web: Contact information for Facility Director March 26 & 27, 2007 © Thayumanasamy Somasundaram

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