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CTBT-laboratory activities in STUK
Jani Turunen Inspector, PhD FIL07 Official Environmental Radiation Surveillance and Emergency Preparedness Radiation and Nuclear Safety Authority (STUK)
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CTBTO The Comprehensive Nuclear-Test-Ban Treaty (CTBT) bans all nuclear explosions The CTBT was negotiated in 1996 44 specific nuclear technology holder countries must sign and ratify the treaty before the CTBT can enter into force. The Preparatory Commission for the CTBTO was founded in 1996 and it is based in Vienna. Signs of nuclear explosions are monitored with the International Monitoring System (IMS). It will consist of 337 facilities worldwide, when completed. Data from the IMS monitoring stations is sent to The International Data Centre (IDC) at the CTBTO's headquarters in Vienna.
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Comprehensive Nuclear-Test-Ban Treaty
States, whose signature and ratification are required for the Treaty to enter into force are listed in the CTBT, Annex 2. States that have signed and ratified the Treaty States that have signed the Treaty and are current members of the Preparatory Commission for the CTBTO States that have neither signed nor ratified the Treaty
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International Monitoring System (IMS)
Total 337 Certified 283 Installed 19 Under construction 17 Planned 18 Primary Seismic Auxiliary Seismic 120 Infrasound Hydroacoustic Radionuclide Radionuclide Laboratories 16
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IMS Radionuclide Stations
Total 80 Certified 63 Installed 4 Under construction 9 Planned 4 40 Radionuclide Stations will have the capability to detect noble gases
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IMS Radionuclide Laboratories
FIL07 GBL15 RUL13 ATL03 USL16 CAL05 FRL08 JPL11 ITL10 ILL09 CNL06 BRL04 ARL01 ZAL14 Total 16 Certified 12 Installed 4 Under construction 0 Planned 0 AUL02 NZL12 Radionuclide Laboratories supporting the monitoring network: Buenos Aires (AR), Melbourne (AU), Seibersdorf (AT), Rio de Janeiro (BR), Ottawa (CA), Beijing (CN), Helsinki (FI), Bruyères-le-Châtel (FR), Yavne (IL), Rome (IT), Tokai (JP), Christchurch (NZ), Moscow (RU), Pelindaba (ZA), Aldermaston (GB), Richland (US)
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Roles of the 16 Radionuclide Laboratories
Station samples for radionuclide network quality assurance Station back-up samples when a station is down Samples from station visits Proficiency test exercise samples, one each year Special measurements agreed between the laboratory and the Commission Additional sample analysis of a suspect or irregular sample to verify the presence or absence of fission and/or activation products
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Radionuclide laboratory FIL07
STUK hosts one of the CTBTO IMS radionuclide laboratories, FIL07 FIL07 was certified in Hosted by the Environmental Radiation Surveillance and Emergency Preparedness Department (VALO) of STUK Most part of management, analysts and laboratory personnel from the Environmental surveillance and measurement laboratory (VAM) Analysts and lab personnel also from other units/departments of STUK.
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FIL07 Organizational details
The quality manager of the VALO department is also the head of FIL07. The Head of FIL07 formally approves the quality manuals and is responsible for providing needed resources to FIL07. The FIL07 Official is responsible for maintaining the FIL07 quality system and FIL07 specific infrastructure, IMS sample analysis, daily operations and preparedness, periodic reporting and FIL07 specific aspects of QA/QC program, maintaining relations to PTS and taking part into national CTBTO related work (WGB meetings, workshops, national meetings, etc..). VAM laboratory is responsible for QA/QC program components common with the ISO/IEC requirements, counting rooms and spectrometer upkeep and providing analysts for FIL07
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STUK gamma laboratory facilities
Two low background counting rooms: Construction from selected concrete and mortar with low abundance of natural radionuclides Special air ventilation and continuous radon monitoring (radon levels ~3Bq/m3) ≈ 15 HPGes in vertical cryostats (LN/electric) Pb BG-shielding ISO/IEC accreditation. Currently one certified spectrometer for IMS sample analysis Certification of a second spectrometer under way
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FIL07 hardware and software
LN cooled Canberra BEGe-5030 spectrometer (48% rel. eff.) 13 cm lead shield Ortec Dspec Pro Unisampo acquisition software Unisampo-Shaman analysis software Linssi database Physically separate LAN, firewalled access Satellite connection based GCI link Electronic Document Management System – SAHA
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FIL07 software and database
Unisampo acquisition software (interfaces with the Ortec Dspec Pro MCA) Unisampo-Shaman analysis software Peak analysis in Unisampo, Shaman runs the nuclide identification engine Linssi 1.1 database, lab specific web interface and message management Messages, calibration, sample, measurement and analysis data in the database Generation and management of messages between FIL07 and IDC Automatic incoming and outgoing message processing and database input Automatic sample generation into database from PRESDN and LABSDN messages Sample information updated for lab-pressed samples Measurement and analysis data input (from Unisampo and Shaman ) Analysis reports output (PHD, RLR) Runs on a linux server Dedicated authentication server (digital signature to outgoing messages) Sample chain-of-custody records are updated in the Linssi database as the sample is processsed trough the various stages in the analysis chain
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Web interface Web interface for generating messages and sample tracking
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FIL07 sample preparation and storage
Dedicated sample preparation and storage room for IMS samples Limited access Locked cabinet for IMS samples Separate facilities for high activity samples
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IMS sample types IMS samples include three different types of filter samples RASA, Manual50 and Cincerella. Manual50 samples are compressed to optimal geometry in the stations. No sample preparation needed in the lab. Cinderella filters are measured in stacks. RASA filters are delivered to the lab as whole filters and they are compressed in the lab. Manual50 RASA Cinderella
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Measurement and analysis chain
Sample related Linssi tables updated automatically from PRESDN and LABSDN messages (a new sample or existing sample data updated or amended) Sample preparation for HPGe measurement updating the sample data in the Linssi database via web interface measurementSetup information Generation of null phd with calibration and sample data Sample measured using Unisampo software (1-7 d) sample data from the null phd to Unisampo when starting the measurement Spectrum is saved at regular intervals (as a phd file) Manual analysis using Unisampo-Shaman Phd file is manually read in Analysis results saved to Linssi (manual save) Automated pipeline is not in use Report (PHD, RLR) generation from the Linssi web interface Lab message pipeline autheticates and pushes the results into GCI Results have to be reported in 15 days from sample arrival
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Other FIL07 tasks Analysed samples are returned to Vienna at least four times a year. Quarterly Laboratory Operations Report and billing Proficiency Test Excercise (PTE) every year Surveillance Assessment Visit (SAV) once in three years Working Group B meetings in Vienna twice a year Laboratory workshops once in two years
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