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Gold nanoparticles grafted modified silica gel as a new stationary phase for separation and determination of steroid hormones by thin layer chromatography 

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Presentation on theme: "Gold nanoparticles grafted modified silica gel as a new stationary phase for separation and determination of steroid hormones by thin layer chromatography "— Presentation transcript:

1 Gold nanoparticles grafted modified silica gel as a new stationary phase for separation and determination of steroid hormones by thin layer chromatography  Mitra Amoli-Diva, Kamyar Pourghazi  Journal of Food and Drug Analysis  Volume 23, Issue 2, Pages (June 2015) DOI: /j.jfda Copyright © Terms and Conditions

2 Fig. 1 Structure of (A) progesterone and (B) testosterone.
Journal of Food and Drug Analysis  , DOI: ( /j.jfda ) Copyright © Terms and Conditions

3 Fig. 2 (A) UV–Vis spectrum and (B) TEM image of the prepared Au NPs. Au NP = gold nanoparticle; TEM = transmission electron microscopy; UV–Vis = ultraviolet–visible. Journal of Food and Drug Analysis  , DOI: ( /j.jfda ) Copyright © Terms and Conditions

4 Fig. 3 Schematic illustration of preparation of Au NPs-APTS modified silica gel stationary phase. Au NPs-APTS = gold nanoparticles grafted 3-triethoxysilyl propylamine. Journal of Food and Drug Analysis  , DOI: ( /j.jfda ) Copyright © Terms and Conditions

5 Fig. 4 Densitograms of standard solution of progesterone and testosterone (50 ng per spot) on the Au NPs-APTS modified silica gel plate. Au NPs-APTS = gold nanoparticles grafted 3-triethoxysilyl propylamine; PRO = progesterone; TES = testosterone. Journal of Food and Drug Analysis  , DOI: ( /j.jfda ) Copyright © Terms and Conditions

6 Fig. 5 Densitograms of sample solution (urine) containing progesterone and testosterone (50 ng per spot) on the plain silica gel plate. PRO = progesterone; TES = testosterone. Journal of Food and Drug Analysis  , DOI: ( /j.jfda ) Copyright © Terms and Conditions

7 Fig. 6 Densitograms of sample solution (urine) containing progesterone and testosterone (50 ng per spot) on the Au NPs-APTS modified silica gel plate. Au NPs-APTS = gold nanoparticles grafted 3-triethoxysilyl propylamine; PRO = progesterone; TES = testosterone. Journal of Food and Drug Analysis  , DOI: ( /j.jfda ) Copyright © Terms and Conditions


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