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Department of Science, systems and Models
Relaxation Spin lattice Spin-spin 2D NMR Department of Science, systems and Models
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Department of Science, systems and Models
Relaxation times 2D NMR Department of Science, systems and Models
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Relaxation mechanisms
Dipole-dipole Spin-rotation Anisotropy Scalar coupling constants Paramagnetic molecules Quadrupolar nuclei 2D NMR Department of Science, systems and Models
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Inversion recovery experiment
2D NMR Department of Science, systems and Models
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Inversion recovery experiment
2D NMR Department of Science, systems and Models
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Department of Science, systems and Models
Relaxaton times of H1 2D NMR Department of Science, systems and Models
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T1 relaxation times of toluene
2D NMR Department of Science, systems and Models
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Department of Science, systems and Models
Decoupling Decoupling=multiple resonance 2D NMR Department of Science, systems and Models
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Department of Science, systems and Models
Decoupling of 14N 2D NMR Department of Science, systems and Models
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Department of Science, systems and Models
Decoupling 2D NMR Department of Science, systems and Models
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Department of Science, systems and Models
2D NMR Department of Science, systems and Models
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Department of Science, systems and Models
2D NMR Department of Science, systems and Models
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Department of Science, systems and Models
Ammonium ion 2D NMR Department of Science, systems and Models
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14N NMR spectrum of partially deuteriated ammonium ions
2D NMR Department of Science, systems and Models
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Off-resonance decoupling
2D NMR Department of Science, systems and Models
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Department of Science, systems and Models
Diff NOE 2D NMR Department of Science, systems and Models
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Spin-echo experiment with heteronuclear coupling
2D NMR Department of Science, systems and Models
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Department of Science, systems and Models
NOE effect 2D NMR Department of Science, systems and Models
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Department of Science, systems and Models
Overhauser effect h = girr/gobs(W2-W0/W0+2W1+W2) 2D NMR Department of Science, systems and Models
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Department of Science, systems and Models
2D NMR Department of Science, systems and Models
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Department of Science, systems and Models
No NOE !!!! Negative gamma Intermediate molecular size 2D NMR Department of Science, systems and Models
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Department of Science, systems and Models
Decoupling schemes 2D NMR Department of Science, systems and Models
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Department of Science, systems and Models
NOE effects 2D NMR Department of Science, systems and Models
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Department of Science, systems and Models
Three-spin effect 2D NMR Department of Science, systems and Models
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Spin echo experiment (remove inhomogeneity)
2D NMR Department of Science, systems and Models
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Department of Science, systems and Models
Red blood cells (erythrocytes) 2D NMR Department of Science, systems and Models
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Department of Science, systems and Models
2D NMR Department of Science, systems and Models
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Department of Science, systems and Models
Hydrolysis of aspirin 2D NMR Department of Science, systems and Models
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NMR spectrum of asprin in blood
2D NMR Department of Science, systems and Models
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Department of Science, systems and Models
Cultured astrocytes 2D NMR Department of Science, systems and Models
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Conversion of acetaldehyde in astrocytes
Acetic acid 2D NMR Department of Science, systems and Models
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Department of Science, systems and Models
Spectral editing 2D NMR Department of Science, systems and Models
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Department of Science, systems and Models
CH and CH2 2D NMR Department of Science, systems and Models
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Attached proton test (APT) for cholesteryl acetate
2D NMR Department of Science, systems and Models
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Department of Science, systems and Models
Inadequate 2D NMR Department of Science, systems and Models
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Phase cycling inversion recovery
2D NMR Department of Science, systems and Models
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Spin-echo experiment with heteronuclear coupling
2D NMR Department of Science, systems and Models
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Department of Science, systems and Models
Composite pulse 2D NMR Department of Science, systems and Models
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Department of Science, systems and Models
Shaped pulses 2D NMR Department of Science, systems and Models
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Text for tomorrow Chapter 6
Problems for tomorrow Handouts problems 8.3 and 8.4 2D NMR Department of Science, systems and Models
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Department of Science, systems and Models
2D NMR Department of Science, systems and Models
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Department of Science, systems and Models
2D NMR Department of Science, systems and Models
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Department of Science, systems and Models
2D NMR Department of Science, systems and Models
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Department of Science, systems and Models
2D NMR Department of Science, systems and Models
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Department of Science, systems and Models
2D NMR The gateway to assignment and structure determination of biological molecules 2D NMR Department of Science, systems and Models
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Department of Science, systems and Models
Nomenclature 2D NMR Department of Science, systems and Models
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Department of Science, systems and Models
COSY pulse sequence 2D NMR Department of Science, systems and Models
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Department of Science, systems and Models
COSY experiment 2D NMR Department of Science, systems and Models
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Department of Science, systems and Models
2D NMR Department of Science, systems and Models
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Department of Science, systems and Models
2D NMR Department of Science, systems and Models
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Department of Science, systems and Models
Progressive Regressive parallel 2D NMR Department of Science, systems and Models
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Department of Science, systems and Models
2D NMR Department of Science, systems and Models
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Department of Science, systems and Models
COSY of 2D NMR Department of Science, systems and Models
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COSY of m-dinitobezene
2D NMR Department of Science, systems and Models
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Department of Science, systems and Models
2D NMR Department of Science, systems and Models
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Department of Science, systems and Models
COSY 2D NMR Department of Science, systems and Models
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Department of Science, systems and Models
2D NMR Department of Science, systems and Models
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Department of Science, systems and Models
2D NMR Department of Science, systems and Models
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Department of Science, systems and Models
Tripeptide 2D NMR Department of Science, systems and Models
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Department of Science, systems and Models
2D NMR Department of Science, systems and Models
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Department of Science, systems and Models
2D NMR Department of Science, systems and Models
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Department of Science, systems and Models
Assignment 2D NMR Department of Science, systems and Models
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Department of Science, systems and Models
Artefacts Differences in digital resolution Transverse relaxation Longitudinal relaxation = T1 noise Incorrect pulse lengths 2D NMR Department of Science, systems and Models
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Department of Science, systems and Models
Remedies Checking pulse lengths Phase cycling Symmetrization Cyclops 2D NMR Department of Science, systems and Models
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Department of Science, systems and Models
2D NMR Department of Science, systems and Models
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Department of Science, systems and Models
2D NMR Department of Science, systems and Models
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Department of Science, systems and Models
2D NMR Department of Science, systems and Models
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Department of Science, systems and Models
Tilt AMX system 2D NMR Department of Science, systems and Models
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Department of Science, systems and Models
Phase sensitive Parallel transitions no phase shift Progressive -90 Regressive 90 Magnitude spectra 2D NMR Department of Science, systems and Models
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Department of Science, systems and Models
DQF COSY 2D NMR Department of Science, systems and Models
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Department of Science, systems and Models
DFQ COSY 2D NMR Department of Science, systems and Models
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Department of Science, systems and Models
Phase sensitive COSY 2D NMR Department of Science, systems and Models
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Department of Science, systems and Models
COSY and Relayed COSY 2D NMR Department of Science, systems and Models
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Department of Science, systems and Models
2D NMR Department of Science, systems and Models
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Department of Science, systems and Models
2D NMR Department of Science, systems and Models
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Department of Science, systems and Models
COSY and TOCSY 2D NMR Department of Science, systems and Models
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Department of Science, systems and Models
TOCSY 2D NMR Department of Science, systems and Models
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Department of Science, systems and Models
TOCSY 2D NMR Department of Science, systems and Models
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Department of Science, systems and Models
2D NMR Department of Science, systems and Models
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Gradient version of COSY exp.
2D NMR Department of Science, systems and Models
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Department of Science, systems and Models
COSY and COSY-45 2D NMR Department of Science, systems and Models
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Department of Science, systems and Models
High resolution 2D NMR Department of Science, systems and Models
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Department of Science, systems and Models
Expansion 2D NMR Department of Science, systems and Models
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J-resolved spectroscopy
2D NMR Department of Science, systems and Models
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Department of Science, systems and Models
Opgaver 2D NMR Department of Science, systems and Models
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Department of Science, systems and Models
HETCOR pulse sequence 2D NMR Department of Science, systems and Models
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Department of Science, systems and Models
HETCOR pulse sequence 2D NMR Department of Science, systems and Models
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Department of Science, systems and Models
HETCOR 2D NMR Department of Science, systems and Models
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Department of Science, systems and Models
2D NMR Department of Science, systems and Models
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Department of Science, systems and Models
2D NMR Department of Science, systems and Models
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Department of Science, systems and Models
HETCOR spectrum 2D NMR Department of Science, systems and Models
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Department of Science, systems and Models
HMQC pulse sequence 2D NMR Department of Science, systems and Models
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Department of Science, systems and Models
HMQC spectrum 2D NMR Department of Science, systems and Models
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Department of Science, systems and Models
BIRD sequence 2D NMR Department of Science, systems and Models
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Department of Science, systems and Models
COLOC spectrum 2D NMR Department of Science, systems and Models
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Department of Science, systems and Models
HSQC 2D NMR Department of Science, systems and Models
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Department of Science, systems and Models
HMBC sequence 2D NMR Department of Science, systems and Models
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Department of Science, systems and Models
HMBC spectrum 2D NMR Department of Science, systems and Models
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Department of Science, systems and Models
HMBC 2D NMR Department of Science, systems and Models
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Department of Science, systems and Models
HSC and H-H-C relayed 2D NMR Department of Science, systems and Models
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Department of Science, systems and Models
2D NMR Department of Science, systems and Models
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Department of Science, systems and Models
2D NMR Department of Science, systems and Models
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Department of Science, systems and Models
2D NMR Department of Science, systems and Models
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Department of Science, systems and Models
NOESY spectrum 2D NMR Department of Science, systems and Models
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Department of Science, systems and Models
Peak intensities 2D NMR Department of Science, systems and Models
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Department of Science, systems and Models
NOE factors 2D NMR Department of Science, systems and Models
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Department of Science, systems and Models
EXSY 2D NMR Department of Science, systems and Models
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Department of Science, systems and Models
2D INADEQUATE 2D NMR Department of Science, systems and Models
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Department of Science, systems and Models
NOESY spectrum 2D NMR Department of Science, systems and Models
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Department of Science, systems and Models
2D NMR Department of Science, systems and Models
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Department of Science, systems and Models
Gradients 2D NMR Department of Science, systems and Models
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Department of Science, systems and Models
2D NMR Department of Science, systems and Models
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Department of Science, systems and Models
2D NMR Department of Science, systems and Models
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Department of Science, systems and Models
2D NMR Department of Science, systems and Models
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Department of Science, systems and Models
2D NMR Department of Science, systems and Models
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Department of Science, systems and Models
2D NMR Department of Science, systems and Models
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Department of Science, systems and Models
2D NMR Department of Science, systems and Models
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Department of Science, systems and Models
6´ 6´ 3´ 2´ 5´ 5´ 4´ 2D NMR Department of Science, systems and Models
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Department of Science, systems and Models
1 1 3 2D NMR Department of Science, systems and Models
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Department of Science, systems and Models
5 4 3 6 6 2D NMR Department of Science, systems and Models
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Department of Science, systems and Models
2D NMR Department of Science, systems and Models
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Department of Science, systems and Models
2D NMR Department of Science, systems and Models
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Department of Science, systems and Models
2D NMR Department of Science, systems and Models
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Department of Science, systems and Models
2D NMR Department of Science, systems and Models
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Department of Science, systems and Models
2D NMR Department of Science, systems and Models
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Department of Science, systems and Models
2D NMR Department of Science, systems and Models
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Department of Science, systems and Models
2D NMR Department of Science, systems and Models
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Department of Science, systems and Models
2D NMR Department of Science, systems and Models
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Department of Science, systems and Models
2D NMR Department of Science, systems and Models
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Department of Science, systems and Models
2D NMR Department of Science, systems and Models
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Department of Science, systems and Models
2D NMR Department of Science, systems and Models
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Department of Science, systems and Models
2D NMR Department of Science, systems and Models
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Department of Science, systems and Models
2D NMR Department of Science, systems and Models
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Department of Science, systems and Models
2D NMR Department of Science, systems and Models
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Department of Science, systems and Models
2D NMR Department of Science, systems and Models
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Department of Science, systems and Models
2D NMR Department of Science, systems and Models
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Department of Science, systems and Models
2D NMR Department of Science, systems and Models
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Department of Science, systems and Models
2D NMR Department of Science, systems and Models
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Department of Science, systems and Models
2D NMR Department of Science, systems and Models
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Department of Science, systems and Models
2D NMR Department of Science, systems and Models
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Department of Science, systems and Models
2D NMR Department of Science, systems and Models
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Department of Science, systems and Models
2D NMR Department of Science, systems and Models
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Department of Science, systems and Models
2D NMR Department of Science, systems and Models
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Department of Science, systems and Models
2D NMR Department of Science, systems and Models
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Department of Science, systems and Models
2D NMR Department of Science, systems and Models
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Department of Science, systems and Models
2D NMR Department of Science, systems and Models
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Department of Science, systems and Models
2D NMR Department of Science, systems and Models
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Department of Science, systems and Models
2D NMR Department of Science, systems and Models
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Department of Science, systems and Models
2D NMR Department of Science, systems and Models
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Department of Science, systems and Models
2D NMR Department of Science, systems and Models
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Department of Science, systems and Models
2D NMR Department of Science, systems and Models
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