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Dr. Muhammad Qasim Hayat
Course: Medicinal Plants Technique: Soxhlet Extraction and Rotary Evaporator Dr. Muhammad Qasim Hayat
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Soxhlet Extractor A piece of laboratory apparatus invented in 1879 by Franz von Soxhlet. Originally designed for the extraction of a lipid from a solid material. However, a Soxhlet extractor is not limited to the extraction of lipids. Typically, a Soxhlet extraction is only required where the desired compound has a limited solubility in a solvent, and the impurity is insoluble in that solvent.
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Parts of Soxhlet extractor
Stirrer bar Still pot Distillation path Thimble Solid Siphon top Siphon exit Expansion adapter Condenser Cooling water in Cooling water out
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THE SOXHLET EXTRACTOR Continuous extraction of a component from a solid mixture. Boiling solvent vapors rise up through the larger side-arm
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Condensed drops of solvent fall into the porous cup, dissolving out the desired component from a solid mixture
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When the smaller side-arm fills to overflowing, it initiates a siphoning action.
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Residual solvent then drains out of the porous cup, as fresh solvent drops continue to fall into the porous cup.
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. . . and the cycle repeats . . .
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It should look something like THIS:
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The solvent, containing the dissolved component, is siphoned into the boiler below
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ROTARY EVAPORATOR
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