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Application Notes PCSM XYL 64% in LPS Formulation, Secondary Capping and Curing
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Nanocomposite with 64 wt% ZrO2 loading in LPS-1505
Batch:070615#C01
Tested on 07/10/2015
PCSM XYL
9.0 g
LPS-1505 Part B 50 wt. % in XYL
2.53 g
LPS-1505 Part A 50 wt. % in XYL
A clear drop-cast film of the nanocomposite
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64 wt% ZrO2 in LPS-1505
1. Pre-reaction with LPS-1505
In a 40 ml vial (Thermo Scientific, #B7999-6) add the PCSM XYL .
Add LPS 1505 Part B solution to the mixture and mix for 2 min at room temperature with a cap on.
Add LPS 1505 Part A solution to the mixture and mix for 2 min at room temperature with a cap on.
Stir at 110 C for 40 to 50 min* with a cap on. Viscosity of mixture may increase .
2. Drop cast
Pipette the mixture and drop cast onto a glass slide. Keep the film for 10 min at room temperature.
Bake the slide at 70 C for 20 min or longer to remove solvent and cure the film.
* Drop cast films begin to get clear at 40 to 50 min. Time to gel is min.
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