1. Brief Introduction of Liquor Testing in SHCIQ, China
上海出入境检验检疫局酒类检测情况简介
Yang Zhenyu 杨振宇 Technical center for animal, plant and food inspection & quarantine Shanghai Entry-Exit Inspection and Quarantine Bureau （SHCIQ） 上海出入境检验检疫局动植物与食品检验检疫技术中心
Gallo produces amazing wines in every category, to suit every taste.  Gallo also imports wines from nine wine growing countries in the world.  Gallo’s wine portfolio totals over 60 unique brands:
Barefoot is the number 1 wine in the US and has introduced many new wine drinkers to the wine category.
In 2011 alone we updated the Bella Sera Label and updated the Redwood Creek Label. Last year we also introduced The Naked Grape from California and Bodega Elena from Argentina.

2. Outline 目录 酒类检测实验室的质量保证
General situation of the wine import through Shanghai port 上海口岸葡萄酒进口及检验概况
General situation of liquor testing lab 酒类检测实验室概况
The quality assurance(QA) of liquor testing lab
酒类检测实验室的质量保证
Gallo produces amazing wines in every category, to suit every taste.  Gallo also imports wines from nine wine growing countries in the world.  Gallo’s wine portfolio totals over 60 unique brands:
Barefoot is the number 1 wine in the US and has introduced many new wine drinkers to the wine category.
In 2011 alone we updated the Bella Sera Label and updated the Redwood Creek Label. Last year we also introduced The Naked Grape from California and Bodega Elena from Argentina.

3. General situation of the wine import through Shanghai port
Supervision and inspection of import food (including wine), cosmetics through Shanghai port is one of the responsibilities of Shanghai Entry-Exit Inspection and Quarantine Bureau （SHCIQ）.
上海口岸进口食品和化妆品（包括葡萄酒）的监管和检验由上海出入境检验检疫局负责。
Gallo produces amazing wines in every category, to suit every taste.  Gallo also imports wines from nine wine growing countries in the world.  Gallo’s wine portfolio totals over 60 unique brands:
Barefoot is the number 1 wine in the US and has introduced many new wine drinkers to the wine category.
In 2011 alone we updated the Bella Sera Label and updated the Redwood Creek Label. Last year we also introduced The Naked Grape from California and Bodega Elena from Argentina.

4. General situation of the wine import through Shanghai port
As a technical subsidiary of SHCIQ, Technical center for animal, plant and food inspection & quarantine(AFTC) undertakes the all lab testing work of import food , cosmetics in Shanghai port.
作为上海出入境检验检疫局的下属技术机构，食品中心执行上海口岸进口食品和化妆品的实验室测试工作。
The inspection of wine is carried out by Technical Center for Liquor and Cosmetics Inspection, which is a sub center of AFTC.
葡萄酒分析工作由食品中心的子中心酒类化妆品检测中心的实验室完成。
Gallo produces amazing wines in every category, to suit every taste.  Gallo also imports wines from nine wine growing countries in the world.  Gallo’s wine portfolio totals over 60 unique brands:
Barefoot is the number 1 wine in the US and has introduced many new wine drinkers to the wine category.
In 2011 alone we updated the Bella Sera Label and updated the Redwood Creek Label. Last year we also introduced The Naked Grape from California and Bodega Elena from Argentina.

5. 2014-2015 The wine import through Shanghai port
General situation of the wine import through Shanghai port
The wine import through Shanghai port
2014年-2015年上海葡萄酒进口量
Batch
Weight(Ton)
US Dollar(10K)
2014
2015
France
9100
9944
51303
62463
32145
28100
Italy
2604
2575
9611
9752
4286
3990
Chile
1312
1626
12712
16548
4823
6049
Australia
2940
3220
13472
17802
8053
9802
Spain
1986
2369
14740
21555
3576
4033
USA
1114
882
5793
4932
2726
2534
Gallo produces amazing wines in every category, to suit every taste.  Gallo also imports wines from nine wine growing countries in the world.  Gallo’s wine portfolio totals over 60 unique brands:
Barefoot is the number 1 wine in the US and has introduced many new wine drinkers to the wine category.
In 2011 alone we updated the Bella Sera Label and updated the Redwood Creek Label. Last year we also introduced The Naked Grape from California and Bodega Elena from Argentina.

6. 2014-2015 The wine import through Shanghai port
General situation of the wine import through Shanghai port
The wine import through Shanghai port
2014年-2015年上海葡萄酒进口量
Gallo produces amazing wines in every category, to suit every taste.  Gallo also imports wines from nine wine growing countries in the world.  Gallo’s wine portfolio totals over 60 unique brands:
Barefoot is the number 1 wine in the US and has introduced many new wine drinkers to the wine category.
In 2011 alone we updated the Bella Sera Label and updated the Redwood Creek Label. Last year we also introduced The Naked Grape from California and Bodega Elena from Argentina.

7. General situation of the wine import through Shanghai port
2015 year the wine import through Shanghai port
2015年进口葡萄酒概况
Gallo produces amazing wines in every category, to suit every taste.  Gallo also imports wines from nine wine growing countries in the world.  Gallo’s wine portfolio totals over 60 unique brands:
Barefoot is the number 1 wine in the US and has introduced many new wine drinkers to the wine category.
In 2011 alone we updated the Bella Sera Label and updated the Redwood Creek Label. Last year we also introduced The Naked Grape from California and Bodega Elena from Argentina.

8. Outline 目录 酒类检测实验室的质量保证
General situation of the wine import through Shanghai port 上海口岸葡萄酒进口及检验概况
General situation of liquor testing lab 酒类检测实验室概况
The quality assurance(QA) of liquor testing lab
酒类检测实验室的质量保证
Gallo produces amazing wines in every category, to suit every taste.  Gallo also imports wines from nine wine growing countries in the world.  Gallo’s wine portfolio totals over 60 unique brands:
Barefoot is the number 1 wine in the US and has introduced many new wine drinkers to the wine category.
In 2011 alone we updated the Bella Sera Label and updated the Redwood Creek Label. Last year we also introduced The Naked Grape from California and Bodega Elena from Argentina.

9. Personnel General situation of liquor testing人员
33 dedicated and highly trained professionals work for this center, among whom there are
33名专业技术人员，其中：
2 senior research scientists, 4 senior professionals and 6 intermediate professionals,
2位研究员，4位高级技术人员和6位中级技术人员
including 4 doctors, 3 masters and 17 bachelors.
学历为：3位博士，3位硕士和17名学士
Gallo produces amazing wines in every category, to suit every taste.  Gallo also imports wines from nine wine growing countries in the world.  Gallo’s wine portfolio totals over 60 unique brands:
Barefoot is the number 1 wine in the US and has introduced many new wine drinkers to the wine category.
In 2011 alone we updated the Bella Sera Label and updated the Redwood Creek Label. Last year we also introduced The Naked Grape from California and Bodega Elena from Argentina.

10. Instrument and Equipment
General situation of liquor testing lab
Instrument and Equipment
仪器设备
The total amount of instrument and equipment for liquor testing has exceeded 3 million USD in lab.
实验室配置了超过3百万美元的仪器设备
Include:
HPLC 5 sets; GC 3 sets; IC 1 sets; AAS 2 sets;
HPLC-MS/MS 2 set; HPLC-IT-TOF 1 set;
ICP-OES 2 set;
GC-MS 3 sets;
Alcolyzer Plus Beer Me 2 set;
Thermo Arena 1 set;
IRMS and NMR is in the process of purchasing.
Gallo produces amazing wines in every category, to suit every taste.  Gallo also imports wines from nine wine growing countries in the world.  Gallo’s wine portfolio totals over 60 unique brands:
Barefoot is the number 1 wine in the US and has introduced many new wine drinkers to the wine category.
In 2011 alone we updated the Bella Sera Label and updated the Redwood Creek Label. Last year we also introduced The Naked Grape from California and Bodega Elena from Argentina.

11. Instrument and Equipment for liquor testing
General situation of liquor testing lab
Instrument and Equipment for liquor testing
Gallo produces amazing wines in every category, to suit every taste.  Gallo also imports wines from nine wine growing countries in the world.  Gallo’s wine portfolio totals over 60 unique brands:
Barefoot is the number 1 wine in the US and has introduced many new wine drinkers to the wine category.
In 2011 alone we updated the Bella Sera Label and updated the Redwood Creek Label. Last year we also introduced The Naked Grape from California and Bodega Elena from Argentina.

12. Instrument and Equipment for liquor testing
General situation of liquor testing lab
Instrument and Equipment for liquor testing
Gallo produces amazing wines in every category, to suit every taste.  Gallo also imports wines from nine wine growing countries in the world.  Gallo’s wine portfolio totals over 60 unique brands:
Barefoot is the number 1 wine in the US and has introduced many new wine drinkers to the wine category.
In 2011 alone we updated the Bella Sera Label and updated the Redwood Creek Label. Last year we also introduced The Naked Grape from California and Bodega Elena from Argentina.

13. Color（Carmine red, Sunset yellow,etc.）
General situation of liquor testing lab
Detection Capability 检测能力
No.
Item/Parameter
项目/参数 1
liquoricity
酒精度 9
Lead 铅 17
 Phthalate esters
邻苯二甲酸酯类 2
Total sugar 总糖 10
Total acidity 总酸 18
Caffeine
咖啡因 3
Dry extract
干浸出物 11
Saccharin sodium
糖精钠 19
Ethyl carbonate
氨基甲酸乙酯 4
Sulfur dioxide
二氧化硫 12
Sodium cyclamate
甜蜜素 20
Methanol 甲醇 5
Volatile acids
挥发酸 13
Acesulfame K
安赛蜜 21
Formaldehyde 甲醛 6
Iron 铁 14
Sorbic acid
山梨酸 22
Ochratoxin A
赭曲霉毒素 7
Copper 铜 15
Benzoic acid
苯甲酸 23
Citric Acid
柠檬酸 8
Reduced sugar
还原糖
 16
Color（Carmine red, Sunset yellow,etc.） 色素 24 ……
Gallo produces amazing wines in every category, to suit every taste.  Gallo also imports wines from nine wine growing countries in the world.  Gallo’s wine portfolio totals over 60 unique brands:
Barefoot is the number 1 wine in the US and has introduced many new wine drinkers to the wine category.
In 2011 alone we updated the Bella Sera Label and updated the Redwood Creek Label. Last year we also introduced The Naked Grape from California and Bodega Elena from Argentina.

14. Workload General situation of liquor testing lab 工作量 Year Batch Sample
Result
2014
6000
7500
30000
2015
5000
5500
22000
Gallo produces amazing wines in every category, to suit every taste.  Gallo also imports wines from nine wine growing countries in the world.  Gallo’s wine portfolio totals over 60 unique brands:
Barefoot is the number 1 wine in the US and has introduced many new wine drinkers to the wine category.
In 2011 alone we updated the Bella Sera Label and updated the Redwood Creek Label. Last year we also introduced The Naked Grape from California and Bodega Elena from Argentina.

15. Key laboratory 重点实验室 General situation of liquor testing lab
The lab was approved to be State Key Inspection and Testing Laboratory of liquor in 2011, by General Administration of Quality Supervision, Inspection and Quarantine of the People’s Republic of China (AQSIQ).
2011年该实验室被国家质检总局批准为国家酒类检测重点实验室。
Gallo produces amazing wines in every category, to suit every taste.  Gallo also imports wines from nine wine growing countries in the world.  Gallo’s wine portfolio totals over 60 unique brands:
Barefoot is the number 1 wine in the US and has introduced many new wine drinkers to the wine category.
In 2011 alone we updated the Bella Sera Label and updated the Redwood Creek Label. Last year we also introduced The Naked Grape from California and Bodega Elena from Argentina.

16. Proficiency Testing Provider 组织能力验证活动
General situation of liquor testing lab
Proficiency Testing Provider 组织能力验证活动
Organized the PT project of “total sugar, sorbic acid, manganese contents in wine”(CNCA-13-B14) in 2013.
A total of 114 laboratories took part in this test.
2013年组织葡萄酒中总糖、山梨酸和锰含量的能力验证活动（CNCA-13-B14），共有114家实验室参加。
Our lab is now organizing a CNCA PT of “ Lead, methanol content in distilled liquor” in 2016.
2016年我们实验室正在组织CNCA的“蒸馏酒中的铅和甲醇含量”能力验证项目。
Gallo produces amazing wines in every category, to suit every taste.  Gallo also imports wines from nine wine growing countries in the world.  Gallo’s wine portfolio totals over 60 unique brands:
Barefoot is the number 1 wine in the US and has introduced many new wine drinkers to the wine category.
In 2011 alone we updated the Bella Sera Label and updated the Redwood Creek Label. Last year we also introduced The Naked Grape from California and Bodega Elena from Argentina.

17. Outline 目录 酒类检测实验室的质量保证
General situation of the wine import through Shanghai port 上海口岸葡萄酒进口及检验概况
General situation of liquor testing lab 酒类检测实验室概况
The quality assurance(QA) of liquor testing lab
酒类检测实验室的质量保证
Gallo produces amazing wines in every category, to suit every taste.  Gallo also imports wines from nine wine growing countries in the world.  Gallo’s wine portfolio totals over 60 unique brands:
Barefoot is the number 1 wine in the US and has introduced many new wine drinkers to the wine category.
In 2011 alone we updated the Bella Sera Label and updated the Redwood Creek Label. Last year we also introduced The Naked Grape from California and Bodega Elena from Argentina.

18. The quality assurance(QA) of liquor testing lab
Quality management system 质量管理体系
Our lab is accredited by CNAS-CL01
(be equal to ISO/IEC 17025:2005)
Registration No./CNAS L1009
认可实验室编号
Gallo produces amazing wines in every category, to suit every taste.  Gallo also imports wines from nine wine growing countries in the world.  Gallo’s wine portfolio totals over 60 unique brands:
Barefoot is the number 1 wine in the US and has introduced many new wine drinkers to the wine category.
In 2011 alone we updated the Bella Sera Label and updated the Redwood Creek Label. Last year we also introduced The Naked Grape from California and Bodega Elena from Argentina.

19. The quality assurance(QA) of liquor testing lab
Quality control(QC) technique 质量控制技术
Process Control 过程控制
Separate control
独立控制
Gallo produces amazing wines in every category, to suit every taste.  Gallo also imports wines from nine wine growing countries in the world.  Gallo’s wine portfolio totals over 60 unique brands:
Barefoot is the number 1 wine in the US and has introduced many new wine drinkers to the wine category.
In 2011 alone we updated the Bella Sera Label and updated the Redwood Creek Label. Last year we also introduced The Naked Grape from California and Bodega Elena from Argentina.

20. The quality assurance(QA) of liquor testing lab
Process Control 过程控制
Every test batch must follow the process control.
每个测试批都必须有过程控制样品。
For trace analysis, the control items are recovery, blank,
slope, linearity, double test tolerance…
对痕量测试，控制项目一般有回收率、空白、斜率、线性、双试验允差等。
For macro analysis, the control items are blank, double test tolerance, control sample…
对常量测试，控制项目一般有空白、双试验允差、控制样等。
Gallo produces amazing wines in every category, to suit every taste.  Gallo also imports wines from nine wine growing countries in the world.  Gallo’s wine portfolio totals over 60 unique brands:
Barefoot is the number 1 wine in the US and has introduced many new wine drinkers to the wine category.
In 2011 alone we updated the Bella Sera Label and updated the Redwood Creek Label. Last year we also introduced The Naked Grape from California and Bodega Elena from Argentina.

21. The quality assurance(QA) of liquor testing lab
Control chart 控制图
Gallo produces amazing wines in every category, to suit every taste.  Gallo also imports wines from nine wine growing countries in the world.  Gallo’s wine portfolio totals over 60 unique brands:
Barefoot is the number 1 wine in the US and has introduced many new wine drinkers to the wine category.
In 2011 alone we updated the Bella Sera Label and updated the Redwood Creek Label. Last year we also introduced The Naked Grape from California and Bodega Elena from Argentina.

22. The quality assurance(QA) of liquor testing lab
Control chart 控制图
Xbar-R Chart of total sugar in wine
Gallo produces amazing wines in every category, to suit every taste.  Gallo also imports wines from nine wine growing countries in the world.  Gallo’s wine portfolio totals over 60 unique brands:
Barefoot is the number 1 wine in the US and has introduced many new wine drinkers to the wine category.
In 2011 alone we updated the Bella Sera Label and updated the Redwood Creek Label. Last year we also introduced The Naked Grape from California and Bodega Elena from Argentina.

23. The quality assurance(QA) of liquor testing lab
Separate control
独立控制
Every year lab makes a plan for separate quality control.
每个测试批都必须有过程控制样品。
Such as:
Join the proficiency testing;
Organize the inter-laboratory comparison;
Organize the inter-personal comparison;
Organize the inter-instrument comparison;
Perform the CRM testing; ……
Gallo produces amazing wines in every category, to suit every taste.  Gallo also imports wines from nine wine growing countries in the world.  Gallo’s wine portfolio totals over 60 unique brands:
Barefoot is the number 1 wine in the US and has introduced many new wine drinkers to the wine category.
In 2011 alone we updated the Bella Sera Label and updated the Redwood Creek Label. Last year we also introduced The Naked Grape from California and Bodega Elena from Argentina.

24. The quality assurance(QA) of liquor testing lab
Quality control(QC) technique 质量控制技术
Guide:
GB/T Criterion on quality control of laboratories--Chemical testing of food
GB/T 实验室质量控制规范 食品理化检测
IUPAC Technical Report: Harmonized guidelines for internal quality control in analytical chemistry laboratories
CNAS GL39 Guidance on internal quality control in chemical analysis laboratory—The application of control chart
CNAS GL39 化学分析实验室内部质量控制指南—控制图的应用
LGC/VAM/1998/040 Guidelines for the in-house production of reference materials ……
Gallo produces amazing wines in every category, to suit every taste.  Gallo also imports wines from nine wine growing countries in the world.  Gallo’s wine portfolio totals over 60 unique brands:
Barefoot is the number 1 wine in the US and has introduced many new wine drinkers to the wine category.
In 2011 alone we updated the Bella Sera Label and updated the Redwood Creek Label. Last year we also introduced The Naked Grape from California and Bodega Elena from Argentina.

25. The quality assurance(QA) of liquor testing lab
Detection Limit 检出限
We evaluated the detection limit for all trace analytical methods and some macro analytical methods
所有痕量测试方法和一部分常量测试方法都评估并给出了检出限。
Detection limits reported to clients are usually limits of quantification(LOQ).
通常实验室报告的检出限为定量检出限（LOQ）。
For example:
Pb<0.010 mg/L
(0.010 mg/L is the LOQ of Pb in wine by AAS method)
Gallo produces amazing wines in every category, to suit every taste.  Gallo also imports wines from nine wine growing countries in the world.  Gallo’s wine portfolio totals over 60 unique brands:
Barefoot is the number 1 wine in the US and has introduced many new wine drinkers to the wine category.
In 2011 alone we updated the Bella Sera Label and updated the Redwood Creek Label. Last year we also introduced The Naked Grape from California and Bodega Elena from Argentina.

26. The quality assurance(QA) of liquor testing lab
Uncertainty 不确定度
The rough uncertainty evaluation program is built for every quantitative test procedure.
实验室对每一个定量测试过程建立不确定度的粗略评估程序。
If necessary, we can do a detailed uncertainty evaluation for a specific result and report it to the client.
如果需要，可以对某一个具体测试结果进行详细的不确定度评估，并报告给相关客户。
Gallo produces amazing wines in every category, to suit every taste.  Gallo also imports wines from nine wine growing countries in the world.  Gallo’s wine portfolio totals over 60 unique brands:
Barefoot is the number 1 wine in the US and has introduced many new wine drinkers to the wine category.
In 2011 alone we updated the Bella Sera Label and updated the Redwood Creek Label. Last year we also introduced The Naked Grape from California and Bodega Elena from Argentina.

27. The quality assurance(QA) of liquor testing lab
Uncertainty 不确定度
Guide:
JJF Evaluation and Expression of Uncertainty in Measurement
JJF 测量不确定度评定与表示
JJF Evaluation of Uncertainty in Chemical Analysis Measurement
JJF 化学分析测量不确定度评定
EURACHEM/CITAC Guide Quantifying Uncertainty in Analytical Measurement
Gallo produces amazing wines in every category, to suit every taste.  Gallo also imports wines from nine wine growing countries in the world.  Gallo’s wine portfolio totals over 60 unique brands:
Barefoot is the number 1 wine in the US and has introduced many new wine drinkers to the wine category.
In 2011 alone we updated the Bella Sera Label and updated the Redwood Creek Label. Last year we also introduced The Naked Grape from California and Bodega Elena from Argentina.

28. Thank for your attention!
Gallo produces amazing wines in every category, to suit every taste.  Gallo also imports wines from nine wine growing countries in the world.  Gallo’s wine portfolio totals over 60 unique brands:
Barefoot is the number 1 wine in the US and has introduced many new wine drinkers to the wine category.
In 2011 alone we updated the Bella Sera Label and updated the Redwood Creek Label. Last year we also introduced The Naked Grape from California and Bodega Elena from Argentina.
SHCIQ, CHINA