1. Rapid Setting Cement Based Mortars Using Nano Materials
Instructor: Mohammad Saadeh
Advisor: Mohamed Zeidan
Blake Mchugh Jordan Perez & Benjamin Boyett
September 28, 2018

2. Composition of Mortar
Sand
Mortar +
Water
Cement + =

3. Rapid Setting Mortar Significance
Move at quicker rate
Less time on the job
Reduced job cost

4. Colloidal Silica
* Nano-silica particles that have been pre-suspended in liquid * Hypothesis: Nano- silica will decrease flowability, decrease set-time, and increase compressive strength.

5. BASF Superplasticizer
* Superplasticizer also known as high range water reducers, are chemical admixtures used where well-dispersed particle suspension is required. * MasterGlenium 7511: reduces water requirements 5%-40%. Increases flowability while maintaining early and ultimate strengths

6. Objective- Test effects of Colloidal Silica
Design mortar mix.
Create different samples.
Test each mix.
Compare results.

7. Mixed Designs Trial Mixtures Control Mix- Basic Mortar Mix.
Other mixes with different percentages of added Silica.
Trial Mixtures
Mixes
Cement (g)
Sand (g)
Water (g)
Cembinder 8 (g)
Total Weight
W/C
S/C
Control
758
2,273
426.3
3,458
.56
3.0 1%
750
418.7
15.16 2%
743
411.1
30.31 5%
720
388.4
75.8
Control II
826
2273
401
3500
.49
2.75
1%-02
818
393
16.53
3483
2%-02
810
384
33.06
3467
5%-02
787
362
78.5
3,422
8%-02
765
340
122.56
3,377
11%-02
744
319
163.90
3,336

8. Flow Table Test
Fill mold ½ way; tamp 25 times.
Fill mold the rest of the way; tamp 25 times.
Remove mold; turn handle (drop table) 25 times in 15 seconds.
Take average of 4 diameters.
Flow = (100) x (Avg. Diameter of Mortar – (Inner Base Diameter of Mold)
(Inner Base Diameter of Mold)

9. Compression Test
Surface Area = Average of 3 width measurements multiplied by the average of 3 height measurements.
Compressive Strength = Max Load / Surface Area or P/A.

10. Normal Consistency Test
Cement, Water, and Additives
Control, 1%, 2%, and 5%
Combine cement, water, and additives (if any).
Place ball into conical ring.
Normal Consistency = 10 mm of penetration after 30 seconds.

11. Vicat Needle Test Initial Setting Time/Final Setting Time
Control, 1%, 2%, 5%, 8%, 11%
Use Normal Consistency Mix to determine initial and final setting time.
Begin a timer when water touches cement.
Initial Setting Time = The elapsed time from when water is added to cement to when the needle penetrates 25 mm or less.
Final Setting Time = The elapsed time from when water touches cement to when the needle no longer penetrates the Cementous mix.

12. New Testing Method (Penetration Test)
The higher the penetration of the rod, the slower that designed mix is setting.
We believe that the more Cembinder 8 that we add to the mix, the less penetration there will be, resulting in a reduced set time.
Complete test for Control, 1%, 2%, 3%, and 5% (included in mix), and then repeat but this time, add the Cembinder to the surface.
Plunger Rod on Vicat Apparatus
Designed Mortar after it is released from the Caulk Gun. =
Penetration Distance

13. Flow Table Results Mix Average Diameter (in) Flowability (%)
Control (W/C = 0.56)
9.06
126.5
1% C8 (W/C = 0.56)
8.56
114
2% C8 (W/C = 0.56)
5% C8 (W/C = 0.56)
8.09
102.3
Control (W/C = 0.49)
9.19
129.7
5% C8 (W/C = 0.49)
7.66
91.5
1% C8 (W/C = 0.49)
114.1%
2% C8 (W/C = 0.49)
8.69
117.2%
8% C8 (W/C = 0.49)
6.72
68%
11% C8 (W/C = 0.49)
4.75
18.8%

17. Vicat Needle Results

18. Timeline August October November Time Activity Assigned Person
*Research, gather materials, and prepare lab equipment for 1, 7, and 28 day testing of new mix design (W/C = 0.49). This will be for 1%, 2%, 8%, and 11% (Cembinder 8)
Blake/Jordan/Ben
 September
*Mix new mixes and put in 2”x2” molds, which will later be used for testing.
*Remove solidified mixes from molds, and complete 1 day compression testing.
Jordan
*Complete 7 & 28 day compression tests on 1% & 2% mixes.
Blake/Jordan
*Gather results and complete the graph that shows the time to strength ratio.
Blake
*Gather materials and develop new testing method for laying mortar mixes with Caulk Gun Apparatus.
 Jordan
October
*Use Mortar Gun Apparatus to lay designed mortar mixes (Control, 1, 2, and 5%).
*Use new testing method to compare the overall strength of each mix.
November
*Use Caulk Gun Apparatus to construct models (walls) using our rapid setting cement based mortar mix
*Prepare for final presentation.

19. Timeline August November Time Activity Assigned Person
*Research, gather materials, and prepare lab equipment for 1, 7, and 28 day testing of new mix design (W/C = 0.49). This will be for 1%, 2%, 8%, and 11% (Cembinder 8)
Blake/Jordan/Ben
 September
*Mix new mixes and put in 2”x2” molds, which will later be used for testing.
*Remove solidified mixes from molds, and complete 1 day compression testing.
Jordan
*Complete 7 & 28 day compression tests on 1% and 2%, mixes.
*Complete 1 &7 day compression tests on 8% and 11% mixes
Ben
 October
* Normal consistency and Vicat Needle test for 8% and 11%
* Mix and Test Cembinder 30 1%, 2% 5% 8% and 11% to Cembinder 8 results
* Use a BASF superplasticizer in mix to add flowability
November
* Gather results and complete the graph that shows the time to strength ratio.
Blake
*Prepare for final presentation.