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Fig. 4 2D COSY NMR of DFB. 2D COSY NMR of DFB. (A) Homonuclear COSY pulse sequence, (B) simulated spectrum, and (C) experimental NV NMR spectrum of DFB.

Published byGrégoire Ruel Modified over 5 years ago

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Presentation on theme: "Fig. 4 2D COSY NMR of DFB. 2D COSY NMR of DFB. (A) Homonuclear COSY pulse sequence, (B) simulated spectrum, and (C) experimental NV NMR spectrum of DFB."— Presentation transcript:

1 Fig. 4 2D COSY NMR of DFB. 2D COSY NMR of DFB. (A) Homonuclear COSY pulse sequence, (B) simulated spectrum, and (C) experimental NV NMR spectrum of DFB. (D) A modified heteronuclear COSY sequence reveals off-diagonal peaks in both (E) simulation and (F) experiment. Color scales correspond to the normalized absolute value of the 2D Fourier transform. Vertical axes (f1 − fref) correspond to the frequencies of the t1 dimension, and horizontal axes (f2 − fref) correspond to the frequencies of the t2 dimension. In (C), 14 values of t1 in s increments up to s were used. Total acquisition time was 22 hours. In (F), 16 values of t1 in s increments up to s were used. Total acquisition time was 25 hours. In both cases, the t2 acquisition spanned from 0 to 1.25 s. All simulations were performed using the SPINACH package (41). Simulation and experimental data use the same windowing functions (see section SXV). Janis Smits et al. Sci Adv 2019;5:eaaw7895 Copyright © 2019 The Authors, some rights reserved; exclusive licensee American Association for the Advancement of Science. No claim to original U.S. Government Works. Distributed under a Creative Commons Attribution License 4.0 (CC BY).

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