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Published byDeja Colter Modified over 10 years ago
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InfraLum FT - 02 FT (Mid)IR Spectrometer CERTIFICATION FOURIER TRANSFORM SPECTROPHOTOMETER
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DEVICE LAYOUT Light Source Interferometer Focusing Optics Sample Compartment Detector
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PRINCIPLE OF OPERATION Permanently aligned “Double Cats Eye” interferometer ensures stability and durability. 1 – Light source 2 – Heat shield 3-4 – Focusing spherical mirrors 5 – Diaphragm 6 – “Double Cats Eye” interferometer 7 – Flat mirror 8, 9,11 – Toric mirrors 10 – Sample Compartment 12 – Detector
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ADVANTAGES high throughput high photometric accuracy high selectivity simultaneous analysis of several components variability of accessories
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ROUTINE MEASUREMENT Take a Sample Fill a Cell Place the Cell Measure Complete a Report Condition the Sample
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ROUTINE MEASUREMENT Take a Sample Fill a Cell Place the Cell Measure Complete a Report Condition the Sample
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ROUTINE MEASUREMENT Take a Sample Fill a Cell Place the Cell Measure Complete a Report Condition the Sample
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ROUTINE MEASUREMENT Take a Sample Fill a Cell Place the Cell Measure Complete a Report Condition the Sample Calcium gluconate transmission spectrum
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ROUTINE MEASUREMENT Take a Sample Fill a Cell Place the Cell Measure Complete a Report Condition the Sample Comparison with the standard spectrum
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MAIN APPLICATIONS Functional group analysis Unknown substance identification Pharmaceuticals identification (RF Pharmacopoeia) Oil content in water and in soil (DIN) Oil-in-water pollutant source identification
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MAIN APPLICATIONS Environmental Monitoring Air and emission measurement Determination of water oil polluters Detection of the presence of ozone- destructing substance Concentration of oil in water measurement Petrochemistry Fractional composition of oils Oil-type analysis Benzene content in gasoline Octane number, cetane number Determination of gas composition Testing the composition of polymer films and coatings Industry Pharmacology Determination of the authenticity of medicine preparations using IR reference standards Quality control of medicine preparations using IR reference standards Quality assurance of organic raw materials Forensic investigations At expert laboratories for qualitative analysis: drugs, medicine, pigments, gas and etc. sample identification
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AIR POLLUTANTS CONTROL PollutantDetection limit, mg/m 3 Carbon monoxide0,11 Carbon dioxide0,034 Water0,18 Hydrogen chloride0,11 Ammonia0,033 Sulfur dioxide0,25 Multi-component analysis of typical industrial air pollutants. Multi-pass gas cell, L = 2,1 m.
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OIL CONTENT IN WATER AND IN SOIL DIN 38409 H18 and Certificate of validation M 01-39-2000 Measured content range: from 0.025 to 50 mg/l Automatic calculation based on absorption peaks 2925. 2960, 3055 cm -1 Quartz cell, L = 4 cm
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OIL POLLUTANT IDENTIFICATION Identification of oil-in-water pollution source by Department of Ecology rule No 241 Automatic calculation based on 12 absorption peaks (1600, 1375, 1310, 1170, 1030, 970, 870, 810, 770, 750, 720, 695 cm -1 ). Sealed Cell, NaCl, L=0.04-0.10 mm
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HHC IDENTIFICATION Comparison of the measured spectrum with the prohibited halogenated hydrocarbons database using Euclidian distance. Sample: C 2 F 4 Br 2 Gas cell, KBr, L=10 cm
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PHARMACEUTICALS IDENTIFICATION Comparison of the measured spectrum with the RF Pharmacopoeia database using Euclidian distance. Sample: Calcium Gluconate Demountable cell, Nujol Suspension.
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PERFUME RAW MATERIALS QC Determination of contaminant in perfume raw materials. Sample: CH 3 -(CH 2 ) 10 - (CH 2 -CH 2 O) 2 -OSO 3 Na Demountable cell, CaF 2, L=0.05 cm. Black - a standard sample Red - a contaminated sample.
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HARDWEAR ParameterSpecification Optical SystemSingle Beam Optics Interferometer Proprietary “Double Cats Eye” interferometer, Sealed and Desiccated Beam SplitterMulti-layer Coated KBr plate Light SourceHigh Temperature Ceramic DetectorPyroelectric (LiTaO 3 or DTGS) Scanning speed1.6; 2; 3.2; 5 mm/sec
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HARDWEAR ParameterSpecification Size580х515х295 mm Weight37 kg Power Requirements~ 110/220 V, 50/60 Hz Operating Conditions Temperature: 10 o C to 35 o C, Humidity: Below 80% Typical analysis time60 sec Data acquisition and processing PC data station, Laptop
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SPECIFICATIONS ParameterSpecification Spectral resolution 0.5, 1, 2, 4, 8, 16 cm -1 Spectral range 6 500 350 cm -1 Wavenumber accuracy± 0.02 cm -1 Noise level of 100% transmission line (spectral range: 2000 50 cm -1 ; resolution: 4 cm -1 ) < 0.08 %
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