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Published byColten Edmands Modified over 9 years ago
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Cleaning of Hydrocarbon Buildup on Metallic-oxide Thin-Films Richard Sandberg Shannon Lunt, Elke Jackson, Kristi Adamson, Ross Robinson, Guillermo Acosta, Nick Webb, Mike Dheil, Luke Bissell
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Purpose: Will the Opticlean polymer remove hydrocarbon? Does this cleaning process damage our thin films? Outline 1. Sample Creation &Contamination rate 2. Effects of hydrocarbon “goo” buildup 3. Opticlean Process 4. Opticlean Residue 5. Damage to thin films 6. Removing Opticlean Residue 7. Conclusions
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Sample Creation & Contamination Rate Creation in vaccum chamber RF Sputtering Evaporation Rates Goo Thickness (Ǻ) Action Performed Elapsed Time (Hrs) 21Open Air425 143Touch fingersInstantaneous 10Dipped in WaterInstantaneous
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Reflectivity Effects With Goo Thickness
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Opticlean Process Opticlean Residue Opticlean significantly removes goo, but leaves a residue Ellipsometric Results Goo thickness on two runs: 1.17 Anstroms 2. 22 Anstroms
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Thin Film Damage Scanning Electron Microscope with EDAX showed no thin film damage X-Ray Photoelectric Spectroscopy found no metal traces
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Scanning Electron Microscope with EDAX
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X-Ray Photoelectric Spectroscopy
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Conclusions Subsequent removal of Opticlean residue with plasma etch Conclusion: Opiclean a very effective way to remove hydrocarbon buildup 1.Sufficiently removes goo 2.Does not damage the surface of thin film samples
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