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Comparison of Hg EDS and WDS Analysis on Commercial Plastic Material By John J. Donovan University of Oregon, Department of Chemistry
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EDS Analysis 100 sec counting time (no visible peak)
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EDS Analysis (cont’d) 500 sec counting time (no visible peak)
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EDS Analysis (cont’d) 1000 sec counting time, with Be window inserted (barely visible peak)
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WDS Analysis TakeOff = 40.0 KiloVolt = 20.0 Beam Current = 52.0 Beam Size = 0 Un 6 std-flex Results in Elemental Weight Percents ELEM: Hg Pb Cr TIME: 240.00 240.00 240.00 AVER:.09916 -.03815 -.00240 SDEV:.07870.06759.00271 Detection limit at 99 % Confidence ELEM: Hg Pb Cr AVER:.00485.00551.00280 990 PPM of Hg easily detected, with 40 PPM sensitivity 240 sec counting time
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