1. EXAMPLES

2. UBAID UR REHMAN 2008-CHEM-19 ANAM ASIF 2008-CHEM-107 PRESENTED BY 2 CHEMICAL ENGINEERING DEPARTMENT, UET

3. Introduction to Example The Aspen Plus Simulation Setting Up the Dynamic Simulation Running the Batch Column Example Initializing the Batch Column Example in Aspen Dynamics PRESENTATION LAYOUT 3 CHEMICAL ENGINEERING DEPARTMENT, UET

4. This is an example of a batch column simulation and illustrates these features of Aspen Dynamics: Use of scripts to automate initialization of an Aspen Dynamic flow sheet Use of tasks to start up and operate the batch reactor INTRODUCTION 4 CHEMICAL ENGINEERING DEPARTMENT, UET

5. 5

6. A mixture of methanol, ethanol and water is to be separated using a batch distillation column. The composition of the charge is 30% ethanol, 30% methanol and 40% water by weight. The required product purity is 68% ethanol w/w. STATEMENT 6 CHEMICAL ENGINEERING DEPARTMENT, UET

7. Aspen Plus has been used to set up the flow sheet for the batch column, which will be exported to Aspen Dynamics and initialized to be full of nitrogen at 20 C and 1 atmosphere The column has been modeled using a RadFrac block. Feed streams for the charge and nitrogen have been specified together with vapor and liquid distillate streams and a bottoms stream. The column has been specified with 10 stages, a partial vaporliquid condenser and a kettle reboiler. THE ASPEN PLUS SIMULATION 7 CHEMICAL ENGINEERING DEPARTMENT, UET

8. The column dimensions have been specified on the RadFrac Dynamic form together with the sump and reflux drum size and geometry. The LMTD heat transfer option has been selected for the condenser and the cooling medium temperature specified as 20 0 C The Constant temperature heat transfer option has been selected for the reboiler and the medium temperature has been specified as 120 C. THE ASPEN PLUS SIMULATION 8 CHEMICAL ENGINEERING DEPARTMENT, UET

9. USE OF SCRIPT To set up the dynamic simulation 9 CHEMICAL ENGINEERING DEPARTMENT, UET

10. A flowsheet level script called Setup and a RadFrac model script called Empty. The Flowsheet level script does the following: 1. Adds a reflux ratio controller 2. Sets the feed flow rates to zero 3. Calls the RadFrac Empty script to initialize the column to be full of nitrogen at 20 C and 1 atmosphere. 4. Performs an initialization run. 5. Saves a snapshot SETTING UP THE DYNAMIC SIMULATION 10 CHEMICAL ENGINEERING DEPARTMENT, UET

11. To run the BatchColumn example: 1. In Aspen Plus, open BatchColumn.bkp. If you installed Aspen Dynamics in the default location, BatchColumn.bkp is in: C:\Program Files\AspenTech\Aspen Dynamics 12.1\Examples\BatchColumn. 2. Perform a run. 3. Export it as a flow-driven dynamic simulation file. 4. Exit Aspen Plus. RUNNING THE BATCH COLUMN EXAMPLE 11 CHEMICAL ENGINEERING DEPARTMENT, UET

12. 12 CHEMICAL ENGINEERING DEPARTMENT, UET

13. 13 CHEMICAL ENGINEERING DEPARTMENT, UET

14. 14 CHEMICAL ENGINEERING DEPARTMENT, UET

15. 15 CHEMICAL ENGINEERING DEPARTMENT, UET

16. 16 CHEMICAL ENGINEERING DEPARTMENT, UET

17. 1. In Aspen Dynamics, open BatchColumn.dynf 2. In the All Items pane of the Simulation Explorer, ensure Flow sheet is selected. In the Contents pane, double-click Add Script. 3. Enter a name for the script, for example, Setup. INITIALIZING THE BATCH COLUMN EXAMPLE IN ASPEN DYNAMICS 17 CHEMICAL ENGINEERING DEPARTMENT, UET

18. 18 CHEMICAL ENGINEERING DEPARTMENT, UET

19. 19 CHEMICAL ENGINEERING DEPARTMENT, UET

20. 4. In the text editor window, click the right mouse button and point to Insert, then click File. Insert BatchColumnScript.txt. 5. Again click the right mouse button and click Invoke Script. Close the text editor window. INITIALIZING THE BATCH COLUMN EXAMPLE IN ASPEN DYNAMICS 20 CHEMICAL ENGINEERING DEPARTMENT, UET

21. 21 CHEMICAL ENGINEERING DEPARTMENT, UET

22. 22 CHEMICAL ENGINEERING DEPARTMENT, UET

23. 23 CHEMICAL ENGINEERING DEPARTMENT, UET

24. 24 CHEMICAL ENGINEERING DEPARTMENT, UET

25. 6. Now create a task called BatchOperation. To do this: 7. In the Contents pane of the Simulation Explorer, double-click Add Task. Enter the name BatchOperation. 8. In the text editor window, select all of the existing text with the mouse (or use Ctrl-A). Click the right mouse button and point to Insert, then click File. Insert BatchOperationTask.txt. 9. Again click with the right mouse button and click Compile or press F8. Close the text editor window. 10. In the Contents pane of the Simulation Explorer, double-click the task to activate it. 11. Change the run mode to Dynamic and perform a dynamic run. INITIALIZING THE BATCH COLUMN EXAMPLE IN ASPEN DYNAMICS 25 CHEMICAL ENGINEERING DEPARTMENT, UET

26. 26 CHEMICAL ENGINEERING DEPARTMENT, UET

27. 27 CHEMICAL ENGINEERING DEPARTMENT, UET

28. 28 CHEMICAL ENGINEERING DEPARTMENT, UET

29. 29 CHEMICAL ENGINEERING DEPARTMENT, UET

30. 30 CHEMICAL ENGINEERING DEPARTMENT, UET

31. USE 0F TASK To start up and operate the batch reactor 31 CHEMICAL ENGINEERING DEPARTMENT, UET

32. The operating sequence defined by the tasks is: At time = 0.5 hours: 1. Ramp the mass flow rate of the Feed stream to 1000 kg/hr over 0.1 hours. 2. Wait until the cumulative mass flow of stream Feed is >= 1000 kg. OPERATING SEQUENCE 32 CHEMICAL ENGINEERING DEPARTMENT, UET

33. 33 CHEMICAL ENGINEERING DEPARTMENT, UET

34. 34 CHEMICAL ENGINEERING DEPARTMENT, UET

35. 35 CHEMICAL ENGINEERING DEPARTMENT, UET

36. 3. Step the mass flow rate of the Feed stream to 0 kg/hr. 4. Wait for 3 minutes. OPERATING SEQUENCE 36 CHEMICAL ENGINEERING DEPARTMENT, UET

37. 37 CHEMICAL ENGINEERING DEPARTMENT, UET

38. 5. Increase the flow of the Nitrogen feed stream to 0.1 kmol/hr. This is needed to maintain the pressure in the column. OPERATING SEQUENCE 38 CHEMICAL ENGINEERING DEPARTMENT, UET

39. 39 CHEMICAL ENGINEERING DEPARTMENT, UET

40. 6.Ramp the reboiler medium temperature to 80 C over 30 minutes. 7. Wait until the reflux drum level >= 0.3 m. OPERATING SEQUENCE 40 CHEMICAL ENGINEERING DEPARTMENT, UET

41. 41 CHEMICAL ENGINEERING DEPARTMENT, UET

42. 8. Start the reflux flow. 9. Wait for 3 minutes. 10. Start the product draw. 11. Ramp the reboiler medium temperature to 90 over 30 minutes. 12. Wait until the mass fraction of methanol in the distillate receiver reaches 0.68. 13. Pause the simulation. OPERATING SEQUENCE 42 CHEMICAL ENGINEERING DEPARTMENT, UET

43. 43 CHEMICAL ENGINEERING DEPARTMENT, UET

44. 14. Use plots and tables to view the results of the simulation during the dynamic run. 15. If you wish to repeat the simulation, rewind to saved snapshot Empty_Initial and then run again. OPERATING SEQUENCE 44 CHEMICAL ENGINEERING DEPARTMENT, UET

45. 45 CHEMICAL ENGINEERING DEPARTMENT, UET

46. 46 CHEMICAL ENGINEERING DEPARTMENT, UET