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Relaxation Studies at UIUC Jacob Yoder February 7 th, 2008
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Illinois setup Polarize 3 He at room temperature with MEOP 3 He refrigerator reaches 0.35 K Measure polarization in lower cell by free induction decay
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December Cool Down Cooled down and attempted to run film burner during visit by George Seidel Cooled cell to ~1.2 K with superfluid in cell Two main problems: Heat load due to superfluid flow too high (300 W) Thermal link between 3 He pot and cell inadequate
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Addressing the Problems Film burner not really necessary, replaced with copper “hat” to facilitate heat transfer 1 mm bore capillary extended up to 1 K anchor to slow film flow Thermal link improved two ways: copper-copper connections made either by welding or strong mechanical contact. Wire braid replaced with two.3” X.032” copper strips Copper strips have good A/L, but are fairly stiff
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Copper Hat
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January Cool Down Glass to copper link broke during LHe fill Contraction of steel pipe during fill pulled on the joint and snapped the capillary
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Copper Strips Replaced 1000 36 AWG wires (Alloy 110) used to make thermal link 8” long braids bent into C shape to give maximum flexibility
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February (Ongoing) Cool Down Nothing broke Cell reached 0.68 K with ~ 0.1 mol 4He in cell Small FID signal in cold cell, but pumping cell hasn’t been properly cleaned yet T 1 measurement not possible without full polarization in pumping cell T 2 significantly longer than 50 ms measurement interval
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To Do Continue T 1 and T 2 measurements after cleaning pumping cell in situ Reduce length, increase cross section of braid to get ~ 10X improvement in A/L Construct d-TPB cell All deuterated materials on hand
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