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Published byDaniel Moran Modified over 11 years ago
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Somervale School, Midsomer Norton, Bath 7 th January 2009
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The experiment we completed was
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1. Safety precautions were taken, glasses and coat!
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2. We boiled 5 tea bags in a beaker using a hot plate.
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3. This equipment is called Buchner filtration. We attached it to taps to create suction.
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4. Filtering
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5. We filtered our stewed tea to remove any bits.
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6. I cooled down the filtrate using an ice bowl.
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7. I added the solution to a separating funnel with an organic solvent.
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8. We shook the funnel and released the gas, pointing at the wall.
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9. I ran off the bottom layer of solution containing the caffeine and dichloromethane solvent.
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10. I used a rotary evaporator to leave the solid in my flask. Expensive machine!
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11. This is our caffeine.
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12. I scraped out the solid caffeine.
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13. We tested the purity on a melting point machine.
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14. Caffeine extracted.
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