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Published byClaire Lambert Modified over 9 years ago
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Genva, January 23, 2001H.-G. Moser MPI, Munich A quick and clean method to measure thermal conductivity Application: QA and QC of spines Standard Method: T between heat source and heat sink Disadvatage: depends on thermal coupling of heaters, sensors etc....
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Genva, January 23, 2001H.-G. Moser MPI, Munich Ballistic Method heater pt100 T t T t Measure reponse T(t): time constant depends on c/ck (c: specific heat, ck: thermal conductivity)
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Genva, January 23, 2001H.-G. Moser MPI, Munich Ballistic Method heater pt100 t=0: T 0 t>0: T r T(t,x)=T r -(T r -T 0 ) c i exp(- ² t/L²)cos[ (x-L)/L] i = /2, 3/2 , 5/2 c i =4 sin( i )/[2 i sin(2 i )] =c k /c L X=0
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Genva, January 23, 2001H.-G. Moser MPI, Munich TPG bar 12 cm Theoretical solution for T=const boundary condition!
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Genva, January 23, 2001H.-G. Moser MPI, Munich Measurements In practice: use heater (constant power) instead of constant temperature bath Spine is a composite object => Calibration necessary
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Genva, January 23, 2001H.-G. Moser MPI, Munich TPG/Cu TPG bar Copper bar Ln[(T-Tmin)/(Tmin-Tmax)]
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Genva, January 23, 2001H.-G. Moser MPI, Munich Effect of different power One practical problem is bad reproducibility of the coupling heater/sample (and sensor/sample) Can be checked by varying the heater power 1.7, 3.2, 6.6 W Ln[(T-Tmax)/(Tmin-Tmax)]
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Genva, January 23, 2001H.-G. Moser MPI, Munich Conclusions Time constant (almost) independent of heater power, coupling of heaters and sensors Fast response: small effect of ambient temperature Robust and reproducible measurement of C k -> develop a simple QC setup for spine
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