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Electrical measurements of sputtered NiCr on grid spacers (GS2mm) 07-11-2011 Dean Walters, Anil Mane Guy Harris, Jeff Elam
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Objective To deposit NiCr layer(150-200nm/side) on grid spacers for better electrical contact. 2 As receivedAfter NiCr coating Appearance of NiCr coated grid looks good
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Photograph after NiCr electrode 3 NiCr Glass Grid edges are sharp but much better than previous vender Overall deposition looks great.
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Thickness values based on Resistance on the grid spacer 4 Considered Bulk rho of NiCr Pt #Resistance (ohm)Thickness (nm) 1625.34 22215.04 3645.17 41522.07 51522.07 61423.64 71917.42 81719.47 9936.78 101130.09 111818.39 121522.07 131227.58 14 23.64 15575.81 162016.55 17684.87 123123 4 5 6 7 8 9 10 11 12 13 14 1516 17 Thickness non-uniformity on the grid spacer We need to improve the Thickness NU and then we can target thickness= 50nm I think 50nm uniform thickness of NiCr will be sufficient for good electrical contact? Similar number and trend observed for other side of the grid spacer
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Rings of Equal Thickness (nm) – Anil’s data 5
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3D Plot and Diagonal Cut Making a cut through the data using both diagonals a cross section plot was made. 6 All measurements 18.6Average 9.21Std Dev
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Four groups of glass samples were coated while being taped onto the surface of the tooling. They were in locations 4, 12, 6, 14 for each set. 7 Sample ID Sheet resistance Thickness from Rs ohm/sq bulk NiCr resistivity (nm) A20.767.6 B24.756.7 C22.861.3 D25.954.1 E14.695.6 F16.684.4 G17.679.6 H18.475.9 I10.6132 J11.6121.1 K12.1115.7 L10.8129.8 M22.163.4 N22.562.3 O21.664.9 Grp 4 Grp 2 Grp 3 QCM=30 Avg59.93 Std Dev5.92 Avg83.88 Std Dev8.56 Avg124.65 Std Dev7.60 Avg63.53 Std Dev1.31 QCM=20 Grp 1 QCM=40 QCM=20
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Conclusion Grid Data –Average of the data was 18 nm –Maximum of data was 36.8 nm Data from Flat Glass Samples –Average of Group #1 is 60 nm –Average of Group #2 is 84 nm –Average of Group #3 is 125 nm The setup for Group #1 (& #4) were the same as the grid data. There is nearly a 4X difference between those averages and the is a 2X difference the maximum point and the samples. 8
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