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Gravimetric Analysis. Quantitative Analysis Process of determining how much of one or more constituents are present in a sample Two Types of Quantitative.

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Presentation on theme: "Gravimetric Analysis. Quantitative Analysis Process of determining how much of one or more constituents are present in a sample Two Types of Quantitative."— Presentation transcript:

1 Gravimetric Analysis

2 Quantitative Analysis Process of determining how much of one or more constituents are present in a sample Two Types of Quantitative Analysis: 1) Gravimetric Analysis – Uses weights 2) Volumetric Analysis – Uses volumes

3 Gravimetric Analysis Dissolves the sample Precipitates out one of the constituents Collects and weighs the precipitate Determines the weight of the constituent Calculates the percent of the constituent in the original sample

4 Example A unknown chloride salt of mass 0.1567g is dissolved in water. Silver nitrate is added and 0.2516g of AgCl precipitate is formed. What is the percent of chlorine in the original sample?

5 Statistics Used to analyze results Experiments are repeated several times It is important that the results are repeatable and not just random (there is precision)

6 Mean Average of the measurements mean = sum of results number of results

7 Deviation How much a result is different from the mean d = result - mean

8 Standard Deviation Gives an indication of the precision of the measurement s.d. = sum of the squares of deviations number of results - 1

9 Example An experiments results are 1, 3, and 5. Calculate the mean, the deviations from the mean, and the standard deviation.

10 What does it tell you? Any result more than two standard deviations from the mean is meaningless and should be discarded


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