1. MASS SPECTROMETRY

3. Intro to Spectroscopy, 3 rd ed., Pavia et al. Mass Spec – Ionization

4. Table 8.2, p 399 Intro to Spectroscopy, 3 rd ed., Pavia et al. Mass Spec – Molecular Formula

5. Table 8.3, p 401 Intro to Spectroscopy, 3 rd ed., Pavia et al. Mass Spec – Molecular Formula

7. Unknown: Contains C, H and one other element. Determine the MF and propose a structure.

8. Table 8.6, p 403 Intro to Spectroscopy, 3 rd ed., Pavia et al. Mass Spec – Molecular Formula

9. Unknown: Contains C, H and one other element. Determine the MF and propose a structure.

10. Mass Spec – Fragmentation

11. Appendices p A39-A44, Intro to Spectroscopy, 3 rd ed., Pavia et al.

12. Mass Spec – Functional Groups Intro to Spectroscopy, 3 rd ed., Pavia et al., p. 406

13. Mass Spec – Alkanes

14. Mass Spec – Alkenes

15. Mass Spec – Alkynes

16. Mass Spec – Aromatic Hydrocarbons

17. MS – Aromatic Hydrocarbons

18. McLafferty Rearrangement Intro to Spectroscopy, 3 rd ed., Pavia et al., p. 416 McLafferty ion

19. C 9 H 12 - Unknown monosubstituted aromatic hydrocarbons.

20. MS – Aldehydes

21. MS – Ketones

22. MS – Ketones: 1-phenyl-1-butanone vs 1-phenyl-2-butanone

23. MS – Esters

25. Unknown: C 8 H 16 O 2 Propose a structure and draw structures for defining fragment ions

26. MS – Carboxylic Acids

27. MS-Amines

28. MS - Amides

29. MS – Unknown Aldehyde