1. Supervised by: Prof. Mohamed Fahim Eng. Yusuf Ismail Done by: Mutlaq Al_Shammari

2. - Distillation column design. - Storage tanks design. - Air cooler design.

3. Introduction : Distillation column is used to separate components according to their boiling point temperature. Objective : To produce high purity of ethyl benzene and distillate product.

4. Assumptions: For c-203 - Sieve plate. - Material of the distillation is carbon steel - Column Efficiency =77.7%. - Tray spacing = 0.64. - Flooding Percentage=85%. - Down Comer Area=12%. - Hole area( 0.1 of Active area). - Weir height ( 50mm). - Hole diameter (5mm). - Plate Thickness (5mm). - Turn down Percentage (70%)

5. - Specify the properties of outlets streams for both vapor and liquid from HYSYS. - Calculating actual no. of stages: - Actual Number of stage = Nm/ efficiency Where, Nm : no of theoretical stages Efficiency = 77.7%

6. - Column diameter:

7. - Liquid flow pattern:

8. - Provisional plate design: Where lw, the weir length

9. - Checking Weeping: Where; h ow is the weir crest liquid in (mm). u h is the liquid velocity in (m/s). u vapor is the vapor velocity in (m/s)

10. - Residence time: - Entrainment:

11. - Number of holes: where, Ah: the total area of the holes Dh: the hole diameter

12. - Thickness calculation: where, - D is the column diameter in m - rj is internal radius in (in). - P is the operating pressure in psi - S is the working stress (psi). - E is the joint efficiency - Cc is the allowance for corrosion (in). - T is thickness of the column in (in).

13. - Cost estimation: where, H: column height V: volume of the column M: mass of the column

14. Introduction : Tanks are basically was made to hold, transport or store fluid and solid.

15.  Volume of the liquid= Total mass flow rate in* time hold-up  Time hold-up: the time where the liquid is hold inside the tank  Volume of cylinder = π R 2 H … (1)  Get the volume of the liquid (assume H=0.2D)  To determine vapor pressure Antoine equation is used:  Log 10 P* = A- (B/C+T) … (2)  T: the temperature in ˚C  The values of A, B, and C is taken from table Antoine equation constant  At this vapor pressure the top space in the tank can be determined.  the total volume=volume of liquid/0.12 … (3)  Diameter 3 = (5*total volume)/ П  Height = 0.2diameter  Area of the tank = total volume/ height … (4)  Thickness  t = (P r i / S E - 0.6P) + Cc …(5)

16. What is air cooler? Air coolers are devices to reject heat from a process fluid directly to ambient air.

17. 1-calculate the heat duty : Q= m Cp Δ T Where, Q: heat duty m: mass flow rate Cp: heat capacity Δ T : Temperature difference

18. 2- CALCULATE OVERALL HEAT TRANSFER COEFFICIENT 3-CALCULATE MEAN TEMPERATURE DIFFERENCE

19. 4-Calculate correction on mean temperature difference 5- Calculate Area Δ Tm=lMTD*Ft Q=UA Δ Tm A=Q/(U Δ Tm)

21. 7- # tube Nt=A/A assume 8-Calculate horse power requirement HP=mcp Δ T*1.34 9- Cost (from matche.com)

22. Distillation c-203Equipment Name To separate EB from PEB& heviesObjective c-203Equipment Number Mutlaq Al_ShammariDesigner Tray columnType EB productionLocation carbon steelMaterial of Construction Mineral woolInsulation 1300000Cost ($)

23. Column Flow Rates ----Recycle (kgmole/hr)682.3Feed (kgmole/hr) 59.13Bottoms(kgmole/hr)623.2Distillate (kgmole/hr) Dimensions 45.717 Height (m) 5.668Diameter (m) 4.81 Reflux Ratio 63Number of Trays Sieve tray Type of tray 0.6357Tray Spacing ------- Number of Caps/Holes 97683Number of Holes Cost 69300$Trays605000$Vessel 277100 $Reboiler303600$Condenser Unit

24. volume of liquid(m3)time hold(hr)Flow rate(m3/hr)Storage no. 840.46550.547 1536.5 T_151 227.54162.7283.655T_201 A&B Area(m2) ActD(t ank)m D^3 Total Volume(m3)Storage no. cost=2655001567.40894.46844410122.342220511152.673837003.879167T_151 cost=109200655.958342.89070185814.453509293019.3949041896.18T_201 A&B t(m)Cc(m)S(kpa)E(m)ri(m)P(kpa)Storage no. 0.1868780.003175945000.8511.171110251308T_151 0.0068950.003175945000.85 7.22675464 541.34T_201 A&B T©CBAp(mmhg)p*(atm)Storage no. 200219.8881203.5316.892722339039.1683077.683115T_151 105.1213.0911423.5436.95651935551.6022546.778423T_201 A&B

25. Heat exchanger Equipment Name Decrease Temperature of vent gas Objective E-106 Equipment Number Mutlaq Al Shammari Designer Air cooler Type After k_101 Location Carbon steel Material of Construction 14600$ Cost ($)

26. Operating Condition Air Side 33 Outlet temperature ( o C) 30 Inlet temperature ( o C) Tube Side 390 Outlet temperature ( o C) 422.4 Inlet temperature ( o C) 13.62Number of Tubes- Number of Tube Rows - Shell Diameter (m)- Tube bundle Diameter (m) 374.5 LMTD ( o C) 225.9199188 Q total (KJ/s) 73.3 Heat Exchanger Area (ft 2 ) 88.6 U ( W/m2 C )

27. Heat exchanger Equipment Name Decrease Temperature of vent gas Objective E-112 Equipment Number Mutlaq Al Shammari Designer Air cooler Type After vlv_103 Location Carbon steel Material of Construction 14400$ Cost ($)

28. Operating Condition Air Side 38.5 Outlet temperature ( o C) 30 Inlet temperature ( o C) Tube Side 300Outlet temperature ( o C) 389.4 Inlet temperature ( o C) 13.04 Number of Tubes- Number of Tube Rows -Shell Diameter (m)- Tube bundle Diameter (m) 308.69 LMTD ( o C) 604.2898683 Q total (KJ/s) 70.18Heat Exchanger Area (ft 2 ) 300.1 U ( W/m2 C )

29. Thank you for listening