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MPRI Centralised Laboratories Gerrard Peters School of Physics 1
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Introduction Centralised laboratories houses similar pieces of equipment – Better accessibility of equipment to researchers – Provides a wider scope for preparing and analysing materials MPRI Centralised Laboratories – Thin Films Lab – Furnace Lab – Sample Preparation Lab Research labs are utilised by : – Physics researchers and post graduate students – Students from other schools and faculties including; Chemistry Biology Metallurgical Engineering Mechanical Engineering 2
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Thin Films Laboratory Houses various deposition systems Can deposit ~100nm thick layers of most metals (Al, Au, Cr etc,), and Organic thin film layers: pentacene 3
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Thin Films Laboratory 4 PLD (pulsed laser deposition) system Hard coatings and protective layers - Transition metal Carbides and nitrides B4C, TiC, NbC, NbN, RF Sputtering system Single/Multi metallic layers, nano particles, Ti, Nb, Hf, diamond like carbon: doped & pristine Compounds: Oxides- BiFeO 3, carbides, nitrides, oxynitrides, composite oxides
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Thin Films Laboratory 5 DC Sputtering system transparent conducting oxides reactive sputtering of composite oxides and oxynitrides Modification: multi-layer thin films Thermal evaporation system High vapor pressure materials Al, Au, Cr, Organic thin film layers
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Thin Films Laboratory SEM (Scanning Electron Microscope) with EDS attachment Large chamber (sample size up to 60mm dia x 40mm height) 50nm resolution (W-filament) Elemental surface analysis 6 I-V (electrical measurement) system two point and 4 point in air and at 50K - 325K Photoconductive experiments Photovoltaic materials: low cost Pulse measurements: C-V-t
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Furnace Laboratory Carbolite tube furnace (max temp. ~1100°C) Carbolite tube furnace(max temp. ~1700°C) Sentro Tech tube furnace – 2 zone (max temp. ~1700°C) RF furnace (max temp. ~1400°C) Drying ovens 7
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Sample Preparation Laboratory Precision cutting saws Metallographic polishing machines Variety of optical and stereo microscopes Facilities for working with chemicals 8
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Sample Preparation Laboratory Low speed diamond saw diamond wire saw 9
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Sample Preparation Laboratory Metallographic polisher Optical/stereo microscopes 10
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11 Contact information For use of the Centralised facilities all initial contact to be made with Prof. Elias Haddad For more information on the facilities ; Thin Films Laboratory : Dr. Daniel Wamwangi Furnace Laboratory : Gerrard Peters Sample Prep. Laboratory : Gerrard Peters
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